iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
ASTM

ASTM D1135-86(2020)

(Test Method)

Standard Test Methods for Chemical Analysis of Blue Pigments

Standard Test Methods for Chemical Analysis of Blue Pigments

SIGNIFICANCE AND USE
3.1 These test methods are suitable for determining if impurities are present and establishing that the required pigments are present. These test methods may be used for manufacturing quality control.
SCOPE
1.1 These test methods cover procedures for the chemical analysis of blue pigments known commercially as iron blue, copper phthalocyanine blue, and ultramarine blue.  
1.2 The analytical procedures appear in the following order:    
Sections  
IRON BLUE PIGMENTS  
Identification  
6  
Moisture by the Brabender Moisture Tester  
7 and 8  
Moisture by Toluene Distillation  
9  
Water-Soluble Matter by Extraction  
10  
Water-Soluble Salts by Electrical Conductivity  
11  
Detection of Acid-Insoluble Extenders  
12 and 13  
Detection of Acid-Soluble Extenders  
14 to 17  
Detection of Organic Colors and Lakes  
18  
COPPER PHTHALOCYANINE BLUE PIGMENTS  
Identification  
19  
Moisture and Other Volatile Matter  
20  
Detection of Basic Dye Derivatives  
21  
Detection of Other Organic Coloring Matter  
22  
Detection of Ultramarine Blue  
23  
Detection of Iron Blue  
24  
ULTRAMARINE BLUE  
Identification  
25  
Moisture and Other Volatile Matter  
26  
Water-Soluble Matter  
27  
Detection of Basic Dye Derivatives  
28  
Detection of Other Organic Coloring Matter  
29  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-May-2020
ICS
87.060.10 - Pigments and extenders
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.31 - Pigment Specifications
Current Stage
Ref Project

Relations

Referred By
ASTM D4139-04(2020) - Standard Guide for Determining Volatile and Nonvolatile Content of Pigments
Effective Date
01-Jun-2020

Buy Standard

ASTM D1135-86(2020) - Standard Test Methods for Chemical Analysis of Blue PigmentsASTM D1135-86(2020) - Standard Test Methods for Chemical Analysis of Blue Pigments
PreviousNext
Standard
ASTM D1135-86(2020) - Standard Test Methods for Chemical Analysis of Blue Pigments
English language
6 pages
sale 15% off
Preview
sale 15% off
Preview

Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D1135 − 86 (Reapproved 2020)
Standard Test Methods for
1
Chemical Analysis of Blue Pigments
This standard is issued under the fixed designation D1135; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 1.5 This international standard was developed in accor-
dance with internationally recognized principles on standard-
1.1 These test methods cover procedures for the chemical
ization established in the Decision on Principles for the
analysis of blue pigments known commercially as iron blue,
Development of International Standards, Guides and Recom-
copper phthalocyanine blue, and ultramarine blue.
mendations issued by the World Trade Organization Technical
1.2 The analytical procedures appear in the following order:
Barriers to Trade (TBT) Committee.
Sections
2. Referenced Documents
IRON BLUE PIGMENTS
2
2.1 ASTM Standards:
Identification 6
D280 Test Methods for Hygroscopic Moisture (and Other
Moisture by the Brabender Moisture Tester 7 and 8
Matter Volatile Under the Test Conditions) in Pigments
Moisture by Toluene Distillation 9
Water-Soluble Matter by Extraction 10
D1193 Specification for Reagent Water
Water-Soluble Salts by Electrical Conductivity 11
D1208 Test Methods for Common Properties of Certain
Detection of Acid-Insoluble Extenders 12 and 13
Pigments
Detection of Acid-Soluble Extenders 14 to 17
Detection of Organic Colors and Lakes 18
D2448 Test Method for Water-Soluble Salts in Pigments by
Measuring the Specific Resistance of the Leachate of the
COPPER PHTHALOCYANINE BLUE PIGMENTS
Pigment
Identification 19
E11 Specification for Woven Wire Test Sieve Cloth and Test
Moisture and Other Volatile Matter 20
Sieves
Detection of Basic Dye Derivatives 21
Detection of Other Organic Coloring Matter 22
Detection of Ultramarine Blue 23
3. Significance and Use
Detection of Iron Blue 24
3.1 These test methods are suitable for determining if
ULTRAMARINE BLUE
impurities are present and establishing that the required pig-
ments are present. These test methods may be used for
Identification 25
Moisture and Other Volatile Matter 26
manufacturing quality control.
Water-Soluble Matter 27
Detection of Basic Dye Derivatives 28
4. Purity of Reagents and Water
Detection of Other Organic Coloring Matter 29
4.1 Purity of Reagents—Unless otherwise indicated, it is
1.3 The values stated in SI units are to be regarded as
intended that all reagents shall conform to the specifications of
standard. No other units of measurement are included in this
theCommitteeonAnalyticalReagentsoftheAmericanChemi-
standard.
3
cal Society, where such specifications are available. Other
1.4 This standard does not purport to address all of the
grades may be used, provided it is first ascertained that the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
priate safety, health, and environmental practices and deter-
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
mine the applicability of regulatory limitations prior to use.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
1 3
These test methods are under the jurisdiction of ASTM Committee D01 on ACS Reagent Chemicals, Specifications and Procedures for Reagents and
Paint and Related Coatings, Materials, and Applications and are the direct Standard-Grade Reference Materials, American Chemical Society, Washington,
responsibility of Subcommittee D01.31 on Pigment Specifications. DC. For suggestions on the testing of reagents not listed by theAmerican Chemical
Current edition approved June 1, 2020. Published June 2020. Originally Society, see Analar Standards for Laboratory Chemicals, BDH Ltd., Poole, Dorset,
approved in 1950. Last previous edition approved in 2014 as D1135 – 86 (2014). U.K., and the United States Pharmacopeia and National Formulary, U.S. Pharma-
DOI: 10.1520/D1135-86R20. copeial Convention, Inc. (USPC), Rockville, MD.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D1135 − 86 (2020)
reagent is of sufficiently high purity to permit its use without 5.2 Grind extracted pigments to pass a No.
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

ASTM
ASTM D6131-17(2023)(Test Method)
Standard Test Method for Evaluating the Relative Tint Undertone of Titanium Dioxide Pigments

SIGNIFICANCE AND USE
5.1 This test method allows the user to make a determination of the blueness or yellowness of the tint undertone of titanium dioxide pigments, versus a reference pigment agreed upon by the parties to the test. This is an important measure of tone, since it gives both a measure of effective particle size, and quick approximation of the blue/yellow undertone that can be expected when a coating containing the titanium dioxide is tinted.  
5.2 Such matters as the vehicle for preparing the dispersions and the mechanical method of preparing the dispersion are left to the user. However, variation in these practices will lead to increased variance in the results, so users ought to fix these parameters, in-so-far as is possible, within any one laboratory. This will lead to reduced uncertainty of the results within that laboratory, and it is seldom that interlaboratory comparisons of this test result is needed.  
5.3 Each user must decide whether the loss of accuracy in his measurements due to variation of these parameters is negligibly small for the purpose for which the data are obtained.
SCOPE
1.1 This test method is intended to be used to determine the tint undertone (blue or yellow) of titanium dioxide pigments. This relates to the effective particle size of the pigment  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D6580-17(2023)(Test Method)
Standard Test Method for The Determination of Metallic Zinc Content in Both Zinc Dust Pigment and in Cured Films of Zinc-Rich Coatings

SIGNIFICANCE AND USE
4.1 This test method is useful for determining the amount of metallic zinc in zinc dust pigment, and also in dried films of both inorganic and organic zinc-rich coatings. Test Methods D521 is an appropriate method for analyzing zinc dust, but has shortcomings when applied to samples of cured coatings.
SCOPE
1.1 This test method covers the determination by differential scanning calorimetry of the metallic zinc content of both zinc-dust pigment, and of dried films of zinc-rich coatings. This test method is applicable to both inorganic and organic zinc-rich coatings.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    3 pages
    English language
    sale 15% off
ASTM
ASTM D2745-00(2023)(Test Method)
Standard Test Method for Relative Tinting Strength of White Pigments by Reflectance Measurements

SIGNIFICANCE AND USE
4.1 Tinting strength is one of the most important properties of a white pigment. This test method provides a means of testing this property for quality control.  
4.2 This test method is a referee method, and the vehicle for preparing the dispersion and the black for tinting are suggested, but others may be used provided both the purchaser and the seller agree to the changes.  
4.3 The results obtained with a muller do not necessarily agree with industrial situations where different dispersing conditions exist. However, dispersing with a muller is a fast, relatively inexpensive way of testing tinting strength for routine quality control.
SCOPE
1.1 This test method describes the procedure for determining the relative tinting strength of white pigments by reflectance measurements of black tints.  
1.2 This test method is applicable only for comparing the test pigment with a reference standard of the same type and grade.  
Note 1: Test Method D332 describes a procedure for visual assessment of blue-tinted samples.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    3 pages
    English language
    sale 15% off
ASTM
ASTM D185-07(2023)(Test Method)
Standard Test Methods for Coarse Particles in Pigments

SIGNIFICANCE AND USE
3.1 In production of paints, smoothness of the paint film is of paramount importance. Agglomerates or coarse particles larger than 45 μm are difficult to disperse and may prevent obtaining a smooth film. These test methods are a valuable quality control test for grading raw materials.
SCOPE
1.1 These test methods cover the determination of the amount of coarse particles in dry pigments.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D6619-00(2023)(Practice)
Standard Practice for Incorporating Pigments by High Speed Dispersion

SIGNIFICANCE AND USE
3.1 High speed dispersion is a commonly used dispersion method in the coatings industry. For the purpose of this practice, “high speed” would normally be understood to be a range of RPM between 3 000 and 10 000. This practice provides a reference for its use, so that a producer and user can standardize on an incorporation technique. This will minimize differences in the millbase, and allow the interested parties to concentrate on the physical, chemical, or optical methods to be run.
SCOPE
1.1 This practice covers the dispersion of pigments using a laboratory size high-speed impeller mill. It is similar in technical content to ISO 8780-3.
Note 1: This practice is restricted to mill bases of moderately high viscosity due to either high vehicle concentration or high pigment concentration, or both, which can produce high shear force. It is not intended to provide a means of formulating either pilot plant or full-scale mill base compositions (scaling up the process from laboratory equipment to factory mills is not simple).  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    3 pages
    English language
    sale 15% off
ASTM
ASTM D50-90(2023)(Test Method)
Standard Test Methods for Chemical Analysis of Yellow, Orange, Red, and Brown Pigments Containing Iron and Manganese

SIGNIFICANCE AND USE
3.1 These test methods compile in one place, recommended procedures for analyzing inorganic colored pigments. These pigments are used extensively in paints, and for this reason their compositions are important to the formulators and user.
SCOPE
1.1 These test methods cover procedures for the chemical analysis of yellow, orange, red, and brown pigments containing iron and manganese. The test methods apply specifically to the following pigments: synthetic hydrated yellow iron oxide, yellow ocher, red and brown iron oxides, raw and burnt umber, raw and burnt sienna, and venetian red.  
1.2 The analytical procedures appear in the following order:    
ASTM  
Method  
Refer-  
Dry Pigments
Sections  
ences  
Moisture and Other Volatile Matter  
6  
D280  
Loss on Ignition  
7  
Coarse Particles  
8  
D185  
Matter Soluble in Water  
9  
D1208  
Organic Coloring Matter  
10  
Iron Oxide  
11 and 12  
Calcium Compounds (Reported as CaO)  
13 and 14  
Sulfates Soluble in Hydrochloric Acid  
15 and 16  
Lead Chromate (in Ochers)  
17  
Calcium Carbonate (in Venetian Red)  
18  
C25  
Manganese (in Siennas and Umbers)  
19 and 20  
Pigment Pastes in Oil  
Pigment Content  
21  
D1208  
Moisture and Other Volatile Matter  
22  
D1208  
Nonvolatile Matter in Vehicle  
23  
Moisture by Distillation  
24  
D1208  
Coarse Particles and Skins  
25  
D185  
Consistency (Stormer)  
26  
D562  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to us.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    5 pages
    English language
    sale 15% off
ASTM
ASTM D210-05(2023)(Specification)
Standard Specification for Bone Black Pigment

ABSTRACT
This specification covers bone black, ivory black, or drop black pigment. The pigment may be in dry form or in aqueous dispersion. Dry pigment shall be made by the calcinations of bones, unmixed with any other substance. Dry pigment shall compose of ash, ash insoluble in acids, and coarse particles. Pigment in aqueous dispersion shall be made by grinding the pigment with water, dispersing agent, biocide, fungicide, pH stabilizer, and defoamer. ASTM test methods shall be conducted for coarse particles, pigment and linseed oil in paste in oil, and mass color and tinting strength.
SCOPE
1.1 This specification covers the pigment commercially known as bone black, ivory black, or drop black. The pigment may be purchased in the dry form or as an aqueous dispersion.  
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Technical specification
    2 pages
    English language
    sale 15% off
ASTM
ASTM D126-87(2023)(Test Method)
Standard Test Methods for Analysis of Yellow, Orange, and Green Pigments Containing Lead Chromate and Chromium Oxide Green

SIGNIFICANCE AND USE
4.1 These test methods are for analysis designed as an aid in quality of yellow, orange, and green pigments containing lead chromate and chromium oxide green. Some sections may be applicable to analysis of these pigments when extracted from whole paints.
SCOPE
1.1 These test methods cover procedures for the chemical analysis of yellow, orange, and green pigments containing lead chromate and chromium oxide green.  
1.2 The analytical procedures appear in the following order:    
Sections  
Chrome  Yellow, Chrome Orange, and Molybdate Orange  
Organic Colors and Lakes  
7  
Moisture and Other Volatile Matter  
8  
Matter Soluble in Water  
9  
Lead Chromate  
10 and 11  
Total Lead  
12  
Sulfate  
13 and 14  
Carbon Dioxide  
15  
Molybdenum  
16 and 17  
Extenders  
18 – 22  
Calculation of Substances Other than Insoluble Lead
Compounds  
23 and 24  
Pure  Chrome Green and Reduced Chrome Green  
Organic Colors and Lakes  
25  
Moisture and Other Volatile Matter  
26  
Matter Soluble in Water  
27  
Iron Blue  
28  
Lead Chromate  
29 and 30  
Barium Sulfate and Insoluble Siliceous Material  
31  
Total Lead  
32  
Sulfate  
33  
Calcium Oxide Soluble in Acid  
34 and 35  
Extenders  
36  
Calculation of Insoluble Lead Compounds  
37  
Chromium Oxide Green  
Organic Colors and Lakes  
38  
Moisture and Other Volatile Matter  
39  
Matter Soluble in Water  
40  
Total Chromium as Chromium Oxide  
41  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Note 3.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    8 pages
    English language
    sale 15% off
ASTM
ASTM D1483-12(2023)(Test Method)
Standard Test Method for Oil Absorption of Pigments by Gardner-Coleman Method

SIGNIFICANCE AND USE
4.1 The oil absorption value obtained by this test method provides information about the vehicle demand of the pigment when it is used in a pigment paste. Oil absorption values can be used to characterize batches of a given pigment.  
4.2 This test method differs from Test Method D281 in that D281 requires a vigorous rubbing action whereas this test method involves only a gentle stirring and folding of the pigment. Because the end points are different, the values obtained from the two test methods generally differ.
SCOPE
1.1 This test method covers the determination of oil absorption of pigments by the Gardner-Coleman procedure.2  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D280-01(2023)(Test Method)
Standard Test Methods for Hygroscopic Moisture (and Other Matter Volatile Under the Test Conditions) in Pigments

ABSTRACT
These test methods establish the standard procedures for determining the hygroscopic moisture (and other matter volatile under the test conditions) in pigments. Method A shall be performed on pigments that do not decompose at a specified temperature. This method shall require the use of a wide-mouth cylindrical glass weighing bottle, an oven, and an analytical balance. Method B, on the other hand, shall be used for pigments that decompose at the same specified temperature. This method shall also need a wide-mouth cylindrical glass weighing bottle, an open-tube manometer, a glass desiccator, an oil vacuum pump, and an analytical balance.
SCOPE
1.1 These test methods cover procedures for determining hygroscopic moisture (and other matter volatile under the test conditions) in pigments.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off