ASTM D480-88(2014)

Standard Test Methods for Sampling and Testing of Flaked Aluminum Powders and Pastes

SIGNIFICANCE AND USE
3.1 Flaked aluminum pigments are produced in a variety of forms. These test methods allow the user to determine the applicability of a given product to this use.
SCOPE
1.1 These test methods cover procedures for sampling, qualitative analysis, and physical testing of flaked aluminum powders and pastes (leafing and nonleafing) for coatings.  
1.2 These test methods apply equally to leafing and nonleafing flaked aluminum powders and pastes except where noted to the contrary.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see 7.3.1.

General Information

• Status: Historical
• Publication Date: 30-Nov-2014
• ICS: 87.060.10 - Pigments and extenders
• Technical Committee: D01 - Paint and Related Coatings, Materials, and Applications
• Drafting Committee: D01.31 - Pigment Specifications

Relations

• Replaces: ASTM D480-88(2008) - Standard Test Methods for Sampling and Testing of Flaked Aluminum Powders and Pastes
• Effective Date: 01-Dec-2014
• Replaced By: ASTM D480-88(2020) - Standard Test Methods for Sampling and Testing of Flaked Aluminum Powders and Pastes
• Effective Date: 01-Jun-2020
• Referred By: ASTM B215-20 - Standard Practices for Sampling Metal Powders
• Effective Date: 01-Dec-2014
• Referred By: ASTM D962-81(2020) - Standard Specification for Aluminum Powder and Paste Pigments for Paints
• Effective Date: 01-Dec-2014
• Referred By: ASTM D4139-04(2020) - Standard Guide for Determining Volatile and Nonvolatile Content of Pigments
• Effective Date: 01-Dec-2014
• Referred By: ASTM D267-82(2020) - Standard Specification for Gold Bronze Powder
• Effective Date: 01-Dec-2014

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D480 − 88 (Reapproved 2014)
Standard Test Methods for
Sampling and Testing of Flaked Aluminum Powders and
1
Pastes
This standard is issued under the fixed designation D480; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope E34 Test Methods for Chemical Analysis of Aluminum and
Aluminum-Base Alloys
1.1 These test methods cover procedures for sampling,
E607 Test Method for Atomic Emission Spectrometric
qualitative analysis, and physical testing of flaked aluminum
Analysis Aluminum Alloys by the Point to Plane Tech-
powders and pastes (leafing and nonleafing) for coatings.
3
nique Nitrogen Atmosphere (Withdrawn 2011)
1.2 These test methods apply equally to leafing and non-
E691 Practice for Conducting an Interlaboratory Study to
leafing flaked aluminum powders and pastes except where
Determine the Precision of a Test Method
noted to the contrary.
3. Significance and Use
1.3 The values stated in SI units are to be regarded as the
3.1 Flaked aluminum pigments are produced in a variety of
standard. The values given in parentheses are for information
only. forms. These test methods allow the user to determine the
applicability of a given product to this use.
1.4 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
4. Sampling
responsibility of the user of this standard to establish appro-
4.1 Sampling is subject to mutual agreement between the
priate safety and health practices and determine the applica-
seller and the purchaser. Place each sample in a clean, dry
bility of regulatory limitations prior to use. For a specific
metal or glass container which shall be nearly filled, then close
hazard statement, see 7.3.1.
with a tight cover, seal, mark, and send to the laboratory for
testing.
2. Referenced Documents
2
4.2 When requested, duplicate samples may be taken from
2.1 ASTM Standards:
thesamecontaineranddeliveredtotheseller,andtheinspector
D185 Test Methods for Coarse Particles in Pigments
may take a third set of samples to hold for test in case of
D235 Specification for Mineral Spirits (Petroleum Spirits)
disagreement.
(Hydrocarbon Dry Cleaning Solvent)
D329 Specification for Acetone
5. Qualitative Analysis
D962 Specification for Aluminum Powder and Paste Pig-
5.1 Significance and Use—This test method determines if
ments for Paints
there are chemical impurities, other than fatty and oily matter,
D3980 Practice for Interlaboratory Testing of Paint and
3
as specified in Specification D962, to ensure the absence of
Related Materials (Withdrawn 1998)
fillers or extender pigments.
E11 Specification for Woven Wire Test Sieve Cloth and Test
Sieves
5.2 Procedure:
5.2.1 Total Impurities—Determine the total impurities by
weight in accordance with Test Methods E34 and E607 or by
1
These test methods are under the jurisdiction of ASTM Committee D01 on
atomic absorption.
Paint and Related Coatings, Materials, and Applications and are the direct
responsibility of Subcommittee D01.31 on Pigment Specifications.
5.2.2 Total Aluminum—Determine the total aluminum by
Current edition approved Dec. 1, 2014. Published December 2014. Originally
weight difference with elemental impurities in accordance with
approved in 1938. Last previous edition approved in 2008 as D480 – 88 (2008).
5.2.1.
DOI: 10.1520/D0480-88R14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
6. Leafing Properties
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
6.1 The leafing test conditions specified are selected
the ASTM website.
3
arbitrarily, and even though the numerical leafing value ob-
The last approved version of this historical standard is referenced on
www.astm.org. tained by this test method appears to be low, the pigment may
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D480 − 88 (2014)
give substantially perfect leafing under the conditions of in the glass cylinder and cover with a watch glass. Transfer
practical application in a paint. 25.0 6 1.0 mL of the vehicle to a clean container. Weigh the
required aliquot of aluminum powder or paste to the nearest
6.2 SignificanceandUse—Thisleafingtestmethodhasbeen
0.01 g and transfer to a small dish. Add about 2.5 mL of the
established to determine the percent of leafed aluminum flakes
25-mLquantityofve
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D480 − 88 (Reapproved 2008) D480 − 88 (Reapproved 2014)
Standard Test Methods for
Sampling and Testing of Flaked Aluminum Powders and
1
Pastes
This standard is issued under the fixed designation D480; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope
1.1 These test methods cover procedures for sampling, qualitative analysis, and physical testing of flaked aluminum powders
and pastes (leafing and nonleafing) for coatings.
1.2 These test methods apply equally to leafing and nonleafing flaked aluminum powders and pastes except where noted to the
contrary.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. For a specific hazard statement, see 7.3.1.
2. Referenced Documents
2
2.1 ASTM Standards:
D185 Test Methods for Coarse Particles in Pigments
D235 Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent)
D329 Specification for Acetone
D962 Specification for Aluminum Powder and Paste Pigments for Paints
3
D3980 Practice for Interlaboratory Testing of Paint and Related Materials (Withdrawn 1998)
E11 Specification for Woven Wire Test Sieve Cloth and Test Sieves
E34 Test Methods for Chemical Analysis of Aluminum and Aluminum-Base Alloys
E607 Test Method for Atomic Emission Spectrometric Analysis Aluminum Alloys by the Point to Plane Technique Nitrogen
3
Atmosphere (Withdrawn 2011)
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
3. Significance and Use
3.1 Flaked aluminum pigments are produced in a variety of forms. These test methods allow the user to determine the
applicability of a given product to this use.
4. Sampling
4.1 Sampling is subject to mutual agreement between the seller and the purchaser. Place each sample in a clean, dry metal or
glass container which shall be nearly filled, then close with a tight cover, seal, mark, and send to the laboratory for testing.
4.2 When requested, duplicate samples may be taken from the same container and delivered to the seller, and the inspector may
take a third set of samples to hold for test in case of disagreement.
1
These test methods are under the jurisdiction of ASTM Committee D01 on Paint and Related Coatings, Materials, and Applications and are the direct responsibility of
Subcommittee D01.31 on Pigment Specifications.
Current edition approved July 1, 2008Dec. 1, 2014. Published July 2008. December 2014. Originally approved in 1938. Last previous edition approved in 20032008 as
D480 – 88 (2003).(2008). DOI: 10.1520/D0480-88R08.10.1520/D0480-88R14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Standards
volume information, refer to the standard’sstandard’s Document Summary page on the ASTM website.
3
The last approved version of this historical standard is referenced on www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D480 − 88 (2014)
5. Qualitative Analysis
5.1 Significance and Use—This test method determines if there are chemical impurities, other than fatty and oily matter, as
specified in Specification D962, to ensure the absence of fillers or extender pigments.
5.2 Procedure:
5.2.1 Total Impurities—Determine the total impurities by weight in accordance with Test Methods E34 and E607 or by atomic
absorption.
5.2.2 Total Aluminum—Determine the total aluminum by weight difference with elemental impurities in accordance with 5.2.1.
6. Leafing Properties
6.1 The leafing test conditions specified are selected arbitrarily, and even though the numerical leafing value obtained by this
test method appears to be low, the pigment may give substantially perfect leafing under the conditions of practical application in
a paint.
6.2
...