Standard Practice for Sampling of Green Petroleum Coke

SCOPE
1.1 This practice primarily references Practice D2234/D2234M and applies its sampling principles to green petroleum coke. Green petroleum coke is typically more homogeneous than coal and this practice provides specific guidance for the application of D05.05 coal standards to the sampling of green petroleum coke.  
1.1.1 Practice D2234/D2234M references the four conditions of collecting sample increments: Condition A (Stopped Belt Cut), Condition B (Full-stream Cut), Condition C (Part-stream Cut), and Condition D (Stationary Sampling). This practice directs the user to the appropriate coal standard to apply to each condition, as well as key considerations.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Historical
Publication Date
30-Apr-2018
Current Stage
Ref Project

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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D8145 − 18
Standard Practice for
1
Sampling of Green Petroleum Coke
This standard is issued under the fixed designation D8145; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
Green petroleum coke is a byproduct of certain oil refining technologies but has multiple uses, such
as a solid mineral fuel or a key constituent of making anodes. The chemical and physical
characteristics of green petroleum coke, particularly the moisture content, are not always distributed
equally in the different sized particles.As such, the sampling of green petroleum coke must follow the
generalsamplingprincipalsofcapturingtheparticlesizedistributionoftheconsignmentintothegross
sample that is collected to represent it.
Green petroleum coke sampling has relied on the sampling standards for Coal and Coke under
ASTM Subcommittee D05.05 for guidance on how to collect and prepare samples, in particular,
Practice D2234/D2234M for the Collection of a Gross Sample of Coal, Practice D2013/D2013M for
the Preparation of Coal Samples for Analysis, and Practice D346 for the Collection and Preparation
of Coke Samples for Laboratory Analysis have been used, among others. With the growing use of
mechanicalsamplingequipment,PracticeD7430fortheMechanicalSamplingofCoalhasbeenadded
to the mix. The above cited standards are useful, but do not account for some of the unique
characteristics of petroleum coke, which has led to widespread confusion as to which parts are
applicable, especially Practice D346, which is really used for coke made from coal and not from
petroleum refining.
This practice gives guidelines for the user on how to sample green petroleum coke.The intent is not
to write a standalone standard for green petroleum coke but to direct the user as to how to apply the
D05.05 coal standards already in existence.
1. Scope priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
1.1 This practice primarily references Practice D2234/
1.3 This international standard was developed in accor-
D2234M and applies its sampling principles to green petro-
dance with internationally recognized principles on standard-
leum coke. Green petroleum coke is typically more homoge-
ization established in the Decision on Principles for the
neous than coal and this practice provides specific guidance for
Development of International Standards, Guides and Recom-
the application of D05.05 coal standards to the sampling of
mendations issued by the World Trade Organization Technical
green petroleum coke.
Barriers to Trade (TBT) Committee.
1.1.1 Practice D2234/D2234M references the four condi-
tions of collecting sample increments: Condition A (Stopped
2. Referenced Documents
Belt Cut), Condition B (Full-stream Cut), Condition C (Part-
2
2.1 ASTM Standards:
stream Cut), and Condition D (Stationary Sampling). This
D121 Terminology of Coal and Coke
practice directs the user to the appropriate coal standard to
D346 Practice for Collection and Preparation of Coke
apply to each condition, as well as key considerations.
Samples for Laboratory Analysis
1.2 This standard does not purport to address all of the
D2013/D2013M Practice for Preparing Coal Samples for
safety concerns, if any, associated with its use. It is the
Analysis
responsibility of the user of this standard to establish appro-
D2234/D2234M Practice for Collection of a Gross Sample
of Coal
1
This practice is under the jurisdiction of ASTM Committee D02 on Petroleum
2
Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcom- For referenced ASTM standards, visit the ASTM website, www.astm.org, or
mittee D02.05 on Properties of Fuels, Petroleum Coke and Carbon Material. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Current edition approved May 1, 2018. Published July 2018. DOI: 10.1520/ Standards volume information, refer to the standard’s Document Summary page on
D8145-18. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D8145 − 18
D5709 Test Method for Sieve Analysis of Petroleum Coke sample results obtained using probability sampling, the prob-
D6609 Guide for Part-Stream Sampling of Coal ability distribution of sampling errors can be estimated.
D6883 Practice for Ma
...

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D8145 − 18
Standard Practice for
1
Sampling of Green Petroleum Coke
This standard is issued under the fixed designation D8145; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
Green petroleum coke is a byproduct of certain oil refining technologies but has multiple uses, such
as a solid mineral fuel or a key constituent of making anodes. The chemical and physical
characteristics of green petroleum coke, particularly the moisture content, are not always distributed
equally in the different sized particles. As such, the sampling of green petroleum coke must follow the
general sampling principals of capturing the particle size distribution of the consignment into the gross
sample that is collected to represent it.
Green petroleum coke sampling has relied on the sampling standards for Coal and Coke under
ASTM Subcommittee D05.05 for guidance on how to collect and prepare samples, in particular,
Practice D2234/D2234M for the Collection of a Gross Sample of Coal, Practice D2013/D2013M for
the Preparation of Coal Samples for Analysis, and Practice D346 for the Collection and Preparation
of Coke Samples for Laboratory Analysis have been used, among others. With the growing use of
mechanical sampling equipment, Practice D7430 for the Mechanical Sampling of Coal has been added
to the mix. The above cited standards are useful, but do not account for some of the unique
characteristics of petroleum coke, which has led to widespread confusion as to which parts are
applicable, especially Practice D346, which is really used for coke made from coal and not from
petroleum refining.
This practice gives guidelines for the user on how to sample green petroleum coke. The intent is not
to write a standalone standard for green petroleum coke but to direct the user as to how to apply the
D05.05 coal standards already in existence.
1. Scope priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
1.1 This practice primarily references Practice D2234/
1.3 This international standard was developed in accor-
D2234M and applies its sampling principles to green petro-
dance with internationally recognized principles on standard-
leum coke. Green petroleum coke is typically more homoge-
ization established in the Decision on Principles for the
neous than coal and this practice provides specific guidance for
Development of International Standards, Guides and Recom-
the application of D05.05 coal standards to the sampling of
mendations issued by the World Trade Organization Technical
green petroleum coke.
Barriers to Trade (TBT) Committee.
1.1.1 Practice D2234/D2234M references the four condi-
tions of collecting sample increments: Condition A (Stopped
2. Referenced Documents
Belt Cut), Condition B (Full-stream Cut), Condition C (Part-
2
2.1 ASTM Standards:
stream Cut), and Condition D (Stationary Sampling). This
D121 Terminology of Coal and Coke
practice directs the user to the appropriate coal standard to
D346 Practice for Collection and Preparation of Coke
apply to each condition, as well as key considerations.
Samples for Laboratory Analysis
1.2 This standard does not purport to address all of the
D2013/D2013M Practice for Preparing Coal Samples for
safety concerns, if any, associated with its use. It is the
Analysis
responsibility of the user of this standard to establish appro-
D2234/D2234M Practice for Collection of a Gross Sample
of Coal
1
This practice is under the jurisdiction of ASTM Committee D02 on Petroleum
2
Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcom- For referenced ASTM standards, visit the ASTM website, www.astm.org, or
mittee D02.05 on Properties of Fuels, Petroleum Coke and Carbon Material. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Current edition approved May 1, 2018. Published July 2018. DOI: 10.1520/ Standards volume information, refer to the standard’s Document Summary page on
D8145-18. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D8145 − 18
D5709 Test Method for Sieve Analysis of Petroleum Coke sample results obtained using probability sampling, the prob-
D6609 Guide for Part-Stream Sampling of Coal ability distribution of sampling errors can be estimated.
D6883 Practice for Manual Sampling of Stationary Coal
3.2.8 sample, n—a quantity of material taken from a larger
from Railroad Cars, Barges, Truc
...

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