ASTM D2916-09
(Specification)Standard Specification for Isophorone
Standard Specification for Isophorone
ABSTRACT
This specification covers isophorone volatile solvents used in paints, varnishes, lacquers, and related products. Isoprophone should conform to the specified requirements on apparent specific gravity, color, distillation, purity, acidity as acetic acid, and water content.
SCOPE
1.1 This specification covers isophorone (98 % grade) for use in paint, varnish, lacquer, and related products.
1.2 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E 29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 For specific hazard information and guidance, see the supplier's Material Safety Data Sheet for materials listed in this specification.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D2916 −09
Standard Specification for
1
Isophorone
This standard is issued under the fixed designation D2916; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* Fischer Reagent Titration Method)
2
D1613 Test Method for Acidity in Volatile Solvents and
1.1 This specification covers isophorone (98 % grade) for
Chemical Intermediates Used in Paint, Varnish, Lacquer,
use in paint, varnish, lacquer, and related products.
and Related Products
1.2 The following applies to all specified limits in this
D2192 Test Method for Purity of Aldehydes and Ketones
standard; for purposes of determining conformance with this
D4052 Test Method for Density, Relative Density, and API
standard, an observed value or a calculated value shall be
Gravity of Liquids by Digital Density Meter
rounded off “to the nearest unit” in the last right-hand digit
D5386 Test Method for Color of Liquids Using Tristimulus
used in expressing the specification limit, in accordance with
Colorimetry
the rounding-off method of Practice E29.
E29 Practice for Using Significant Digits in Test Data to
1.3 The values stated in SI units are to be regarded as Determine Conformance with Specifications
E300 Practice for Sampling Industrial Chemicals
standard. No other units of measurement are included in this
4
standard.
2.2 U.S. Federal Specification:
PPP-C-2020 Chemicals, Liquid, Dry, and Paste: Packaging
1.4 For specific hazard information and guidance, see the
of
supplier’sMaterialSafetyDataSheetformaterialslistedinthis
specification.
3. Properties
1.5 This standard does not purport to address all of the
3.1 Isophoroneshallconformtothefollowingrequirements:
safety concerns, if any, associated with its use. It is the
Apparent specific gravity:
responsibility of the user of this standard to establish appro-
20/20°C 0.921 to 0.923
priate safety and health practices and determine the applica-
or
bility of regulatory limitations prior to use.
25/25°C 0.918 to 0.920
Color, Pt-Co scale, max (Note 1) 100
Distillation, °C
2. Referenced Documents
Initial boiling point, min 210
3
95 % point, max 218
2.1 ASTM Standards:
Purity, weight % min 98
D268 Guide for Sampling and Testing Volatile Solvents and
Acidity as acetic acid, weight %, max 0.02
Chemical Intermediates for Use in Paint and Related
Water, weight %, max 0.1
Coatings and Material
NOTE 1—Instrumental Pt-Co color determined by Test Method D5386
D1078 Test Method for Distillation Range of Volatile Or-
have been shown to have no statistically significant difference from Pt-Co
ganic Liquids
color determined by Test Method D1209. However, it is not known
whether isophorone was part of the sample set included in the interlabo-
D1209 Test Method for Color of Clear Liquids (Platinum-
ratory study.
Cobalt Scale)
D1364 Test Method for Water in Volatile Solvents (Karl
4. Sampling
4.1 Sample the material in accordance with Practice E300.
1
This specification is under the jurisdiction of ASTM Committee D01 on Paint
and Related Coatings, Materials, andApplications and is the direct responsibility of
5. Test Methods
Subcommittee D01.35 on Solvents, Plasticizers, and Chemical Intermediates.
5.1 The properties enumerated in this specification shall be
Current edition approved June 1
...
This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D2916–04 Designation: D 2916 – 09
Standard Specification for
1
Isophorone
This standard is issued under the fixed designation D 2916; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
2
1.1 This specification covers isophorone (98 % grade) for use in paint, varnish, lacquer, and related products.
1.2The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3The following applies to all specified limits in this standard; for purposes of determining conformance with this standard, an
observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the
specification limit, in accordance with the rounding-off method of Practice E29.
1.4
1.2 The following applies to all specified limits in this standard; for purposes of determining conformance with this standard,
an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing
the specification limit, in accordance with the rounding-off method of Practice E 29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 For specific hazard information and guidance, see the supplier’s Material Safety Data Sheet for materials listed in this
specification.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
1.5For specific hazard information and guidance, see the supplier’s Material Safety Data Sheet for materials listed in this
specification.
2. Referenced Documents
3
2.1 ASTM Standards:
D 268 Guide for Sampling andTestingVolatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and
Material
D 1078 Test Method for Distillation Range of Volatile Organic Liquids
D 1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D 1364 Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method)
D 1613 TestMethodforAcidityinVolatileSolventsandChemicalIntermediatesUsedIninPaint,Varnish,Lacquer,andRelated
Products
D 2192 Test Method for Purity of Aldehydes and Ketones
D 4052 Test Method for Density and Relative Density of Liquids by Digital Density Meter
D 5386 Test Method for Color of Liquids Using Tristimulus Colorimetry
E1Specification for ASTM Thermometers
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E 300 Practice for Sampling Industrial Chemicals
4
2.2 U.S. Federal Specification:
PPP-C-2020 Chemicals, Liquid, Dry, and Paste: Packaging of
1
This specification is under the jurisdiction ofASTM Committee D01 on Paint and Related Coatings, Materials, and MaterialsApplications and is the direct responsibility
of Subcommittee D01.35 on Solvents, Plasticizers, and Chemical Intermediates.
Current edition approved June 1, 2004.2009. Published June 2004.2009. Originally approved in 1970. Last previous edition approved in 19882004 as
D2916–88(2001).D 2916 – 04.
2
This compound is also known under the name 3,5,5-trimethyl-2-cyclohexene-1-one.
3
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
4
Available from Standardization Documents Order Desk, DODSSP, Bldg. 4, Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http://www.dodssp.daps.mil.
*ASummary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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D2916–09
3. Properties
3.1 Isophorone shall conform to the following requirements:
Apparent specific gravity:
20/20°C 0.921 to 0.923
or
25/25°C 0.918 to 0.920
Color, Pt-Co scale, max 100
Color, Pt-Co scale, max (Note 1) 100
Distillation, °C
Initial boiling point, min 210
95 % point, max 218
Purity, weight % min 98
Acidity as a
...
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