ASTM E785-81(2006)
(Specification)Standard Specification for Crucibles, Ignition, Laboratory, Metal
Standard Specification for Crucibles, Ignition, Laboratory, Metal
ABSTRACT
This specification covers two types of metal ignition crucibles, nickel or platinum, complete with covers, for laboratory use. Two types of crucibles shall be classified according to their capacities: Type I is nickel with capacities of 100 mL and 250 mL and Type II is platinum with capacity of 20 mL. Type I are crucibles and covers which shall be made from 99.4% nickel, spun and hardened and Type II are crucibles and covers which shall be made from 99.9% platinum plus iridium, with the iridium content of not more than 0.4%. The crucibles shall have a standard shape with a flat base to give a firm and stable resting surface. The side wall shall form a sloping and convex surface extending up to the brim. Crucibles shall be of one-piece construction. Covers shall be flat, sunken in the center, and shall have an extension to serve as a handle. The sunken area in the center shall fit inside the crucible.
SCOPE
1.1 This specification covers two types of metal ignition crucibles, nickel or platinum, complete with covers, for laboratory use.
General Information
Relations
Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
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Designation: E785 – 81 (Reapproved 2006)
Standard Specification for
Crucibles, Ignition, Laboratory, Metal
This standard is issued under the fixed designation E785; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 3.1.2 Type II—Platinum.
Capacity: 20 mL
1.1 This specification covers two types of metal ignition
crucibles, nickel or platinum, complete with covers, for labo-
4. Materials
ratory use.
4.1 Type I—Crucibles and covers shall be made from
2. Referenced Documents 99.4 % nickel, spun and hardened in conformance with Speci-
2 fication B162.
2.1 ASTM Standards:
4.2 Type II—Crucibles and covers shall be made from
B162 Specification for Nickel Plate, Sheet, and Strip
3 99.9 % platinum plus iridium, with the iridium content of not
2.2 Federal Standards:
more than 0.4 %.
Fed. Std. No. 123 Marking for Shipment (Civil Agencies)
2.3 Military Standards:
5. Physical Requirements
MIL-STD-105 Sampling Procedures and Tables for Inspec-
5.1 Crucibles shall have a standard shape with a flat base to
tion by Attributes
give a firm and stable resting surface. The side wall shall form
MIL-STD-129 Marking for Shipment and Storage
a sloping and convex surface extending up to the brim.
MIL-STD-1188 Commercial Packaging of Supplies and
Crucibles shall be of one-piece construction.
Equipment
5.2 Covers shall be flat, sunken in the center, and shall have
3. Classification an extension to serve as a handle.The sunken area in the center
shall fit inside the crucible.
3.1 Types and Capacities—The crucibles shall be furnished
in one or more of the following types or capacities as specified
6. Dimensions, Mass, and Permissible Variations
(see S2.1).
6.1 Type I crucibles and covers shall conform to the re-
3.1.1 Type I—Nickel.
quirements of Table 1.
Capacity: 100 mL
6.2 Type II Crucibles and Covers:
250 mL
6.2.1 Type II crucibles shall conform to the requirements of
Table 2.
6.2.2 Type II covers shall conform to the requirements of
This specification is under the jurisdiction of ASTM Committee E41 on
Table 3.
Laboratory Apparatus and is the direct responsibility of Subcommittee E41.01 on
Apparatus.
7. Workmanship
Current edition approved Nov. 1, 2006. Published December 2006. Originally
approved in 1981. Last previous edition approved in 2001 as E785 – 81 (2001).
7.1 Crucibles and covers shall be free of defects (scratches,
DOI: 10.1520/E0785-81R06.
2 dents, discolorations) or contamination (grease, oil, foreign
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
matter) that detract from their appearance or that impair their
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
serviceability.
the ASTM website.
Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,
8. Keywords
Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098, http://
www.dodssp.daps.mil. 8.1 crucibles; ignition; nickel; platinum
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
E785 – 81 (2006)
TABLE 1 Crucible Dimensions (Type I)
A
Outside Wall OD
A A B
Capacity, Bottom OD , Length incl. Inside Diameter of
B A
Diameter, Height, mm Thickness , Exclusive of Wall Thickness, mm
mL mm Handle, mm Sunken Section, mm
mm mm Handle, mm
100 60 30 64 0.625 67 92 58 0.625
250 83 50 83 0.625 92 116 83 0.625
A
Tolerance 6 2 mm.
B
Tolerance 6 0.25 mm.
TABLE 2 Crucible Dimensions (Type II)
Capacity, Top Inside Bottom Inside Thickness of Thickness of
Height, mm Weight, g
mL Diameter, mm Diameter, mm Side, mm Bottom, mm
20 32.4 6 0.8 19 6 1.0 34.5 6 2.0 0.22 6 0.05 0.25 6 0.05 16 6 1.0
TABLE 3 Cover Requirements (Type II)
Outside Diameter
Length Including Diameter of Sun- Depth of Sunken
Thickness, mm Excluding Handle, Weight, g
Handle, mm ken Section, mm Section, mm
mm
0.137 6 0.01 36.4 6 0.2 47 6 0.5 31.5 6 0.5 3.0 6 0.3
SUPPLEMENTARY REQUIREMENTS
The following supplementary requirements are binding when this specification is used by the
Department of Defense and the Federal Government for the procurement of platinum evaporating
dishes.
S1. Sampling S2.3.2 TypeII–Platinum.Nottakenbyfreight.ShipviaUPS
or parcel post.
S1.1 Sampling for nondestructive examination shall be
conducted in accordance with MIL-STD-105.
S3. Lotting and Sampling
S2. Ordering Information
S3.1 A lot shall consist of the crucibles and covers of the
same type and capacity offered for acceptance at one time,
S2.1 Procurement documents should specify the following:
which has been produced by one manufacturer under essen-
S2.1.1 Title, number, and date o
...
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