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ASTM D6572-06

(Test Method)

Standard Test Methods for Determining Dispersive Characteristics of Clayey Soils by the Crumb Test

Standard Test Methods for Determining Dispersive Characteristics of Clayey Soils by the Crumb Test

SIGNIFICANCE AND USE
The crumb test method provides a simple, quick method for field or laboratory identification of a dispersive clay soil. The internal erosion failures of a number of homogeneous earth dams, erosion along channel or canal banks, and rainfall erosion of earthen structures have been attributed to colloidal erosion along cracks or other flow channels formed in masses of dispersive clay (5).
The crumb test method, as originally developed by Emerson (6), was called the aggregate coherence test and had seven different categories of soil-water reactions. Sherard (5) later simplified the test by combining some soil-water reactions so that only four categories, or grades, of soil dispersion are observed during the test. The crumb test is a relatively accurate positive indicator of the presence of dispersive properties in a soil. The crumb test, however, is not a completely reliable negative indicator that soils are not dispersive. The crumb test, can seldom be relied upon as a sole test method for determining the presence of dispersive clays. The double-hydrometer test (Test Method D 4221) and pinhole test (Test Method D 4647) are test methods that provide valuable additional insight into the probable dispersive behavior of clay soils.
Note 2—The quality of the result produced by these test methods is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D 3740 are generally considered capable of competent and objective testing. Users of these test methods are cautioned that compliance with Practice D 3740 does not in itself ensure reliable testing. Reliable testing depends on several factors; Practice D 3740 provides a means of evaluating some of those factors.
SCOPE
1.1 These test methods provide a qualitative indication of the natural dispersive characteristics of clayey soils.
1.2 These test methods are not applicable for soils with less than 12 % fraction finer than 0.005 mm and with a plasticity index less than or equal to 8.
1.3 The crumb test method has some limitations in its usefulness as an indicator of dispersive clay. A dispersive soil may sometimes give a nondispersive reaction in the crumb test. Soils containing kaolinite with known field dispersion problems have shown nondispersive reactions in the crumb test (). However, if the crumb test indicates dispersion, the soil is probably dispersive.
1.4 Oven-dried soil should not be used to prepare crumb test specimens, as irreversible changes could occur to the soil pore-water physicochemical properties responsible for dispersion ().
1.5 The crumb test method, while a good quick indication of dispersive clay, should usually be run in conjunction with a pinhole test and a double hydrometer test, Test Methods D 4647 and D 4221, respectively.Note 1
In some cases, the results of the pinhole, crumb, and double-hydrometer test methods may disagree. Crumb test methods are a better indicator of dispersive clays than of nondispersive clays ().
1.6 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Oct-2006
ICS
13.080.20 - Physical properties of soils
Technical Committee
D18 - Soil and Rock
Drafting Committee
D18.06 - Physical-Chemical Interactions of Soil and Rock
Current Stage
Ref Project

Relations

Replaces
ASTM D6572-00 - Standard Test Methods for Determining Dispersive Characteristics of Clayey Soils by the Crumb Test
Effective Date
01-Nov-2006
Replaced By
ASTM D6572-12 - Standard Test Methods for Determining Dispersive Characteristics of Clayey Soils by the Crumb Test
Effective Date
01-Nov-2012
Referred By
ASTM D4221-18 - Standard Test Method for Dispersive Characteristics of Clay Soil by Double Hydrometer
Effective Date
01-Nov-2006

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ASTM D6572-06 - Standard Test Methods for Determining Dispersive Characteristics of Clayey Soils by the Crumb TestASTM D6572-06 - Standard Test Methods for Determining Dispersive Characteristics of Clayey Soils by the Crumb Test
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ASTM D6572-06 - Standard Test Methods for Determining Dispersive Characteristics of Clayey Soils by the Crumb Test
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D6572 − 06
StandardTest Methods for
Determining Dispersive Characteristics of Clayey Soils by
1
the Crumb Test
This standard is issued under the fixed designation D6572; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
3
1.1 These test methods provide a qualitative indication of
2.1 ASTM Standards:
the natural dispersive characteristics of clayey soils.
D653 Terminology Relating to Soil, Rock, and Contained
Fluids
1.2 These test methods are not applicable for soils with less
D1193 Specification for Reagent Water
than 12 % fraction finer than 0.005 mm and with a plasticity
D2216 Test Methods for Laboratory Determination of Water
index less than or equal to 8.
(Moisture) Content of Soil and Rock by Mass
1.3 The crumb test method has some limitations in its
D3740 Practice for Minimum Requirements for Agencies
usefulness as an indicator of dispersive clay. A dispersive soil
Engaged in Testing and/or Inspection of Soil and Rock as
maysometimesgiveanondispersivereactioninthecrumbtest.
Used in Engineering Design and Construction
Soils containing kaolinite with known field dispersion prob-
D4221 Test Method for Dispersive Characteristics of Clay
lems have shown nondispersive reactions in the crumb test
Soil by Double Hydrometer
2
(1) . However, if the crumb test indicates dispersion, the soil is
D4318 Test Methods for Liquid Limit, Plastic Limit, and
probably dispersive.
Plasticity Index of Soils
1.4 Oven-driedsoilshouldnotbeusedtopreparecrumbtest
D4647 Test Method for Identification and Classification of
specimens, as irreversible changes could occur to the soil
Dispersive Clay Soils by the Pinhole Test
pore-water physicochemical properties responsible for disper-
D6026 Practice for Using Significant Digits in Geotechnical
sion (2).
Data
E1 Specification for ASTM Liquid-in-Glass Thermometers
1.5 Thecrumbtestmethod,whileagoodquickindicationof
E11 Specification for Woven Wire Test Sieve Cloth and Test
dispersive clay, should usually be run in conjunction with a
Sieves
pinholetestandadoublehydrometertest,TestMethodsD4647
and D4221, respectively.
3. Terminology
NOTE 1—In some cases, the results of the pinhole, crumb, and
3.1 Definitions:
double-hydrometer test methods may disagree. Crumb test methods are a
better indicator of dispersive clays than of nondispersive clays (3).
3.1.1 dispersive clays—soils that disperse (deflocculate)
easily and rapidly without significant mechanical assistance in
1.6 The values stated in SI units are to be regarded as the
water of low-salt concentration.
standard. The values given in parentheses are for information
only.
3.1.1.1 Discussion—Such soils usually have a high propor-
tion of their adsorptive capacity saturated with sodium cations
1.7 This standard does not purport to address all of the
althoughadsorbedlithiumandmagnesiummayalsoplayarole
safety concerns, if any, associated with its use. It is the
(4). Such soils also generally have a high shrink-swell
responsibility of the user of this standard to establish appro-
potential, have low resistance to erosion, and have low
priate safety and health practices and determine the applica-
permeability in an intact state.
bility of regulatory limitations prior to use.
3.2 Fordefinitionsofothertermsusedinthesetestmethods,
refer to Terminology D653.
1
These test methods are under the jurisdiction ofASTM Committee D18 on Soil
and Rock and are the direct responsibility of Subcommittee D18.06 on Physical-
Chemical Interactions of Soil and Rock
3
Current edition approved Nov. 1, 2006. Published December 2006. DOI: For referenced ASTM standards, visit the ASTM website, www.astm.org, or
10.1520/D6572-06. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
2
The boldface numbers in parentheses refer to the list of references at the end of Standards volume information, refer to the standard’s Document Summary page on
this standard. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D6572 − 06
4. Summary of Test Method from the water surface can cause excessive slaking and may
result in erroneous interpretation of the dispersion grade.
5
4.1 A cube of remolded soil approximately 15 mm ( ⁄8 in.)
on each side (about the size of a single die in a pair of dice) or 6.4 Jarring or moving the soil specimen or porcelain dish
once the test method has begun can cause excessive turbidity
a natural soil crumb of approximately similar volume is placed
on t
...

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1.1.1 For limitations see Section 5 on Interferences.  
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5.1 The ring shear test is suited to the relatively rapid determination of drained residual shear strength because of the short drainage path through the thin specimen, the constant cross-sectional area of the shear surface during shear, unlimited rotational displacement in one direction, and the capability of testing one specimen under different effective normal stresses to obtain clay particles that are oriented parallel to the direction of shear to obtain residual shear strength envelope.  
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1.1 Fine-grained soils in this Test Method are restricted to soils containing no more than 15 % fine sand (100 % passing the 425 μm (No. 40) sieve and no more than 15 % retained on the 75 μm (No. 200) sieve).A Summary of Changes section appears at the end of this standard.  
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1.5 A shear stress-displacement relationship may be obtained from this test method. However, a shear stress-strain relationship or any associated quantity, such as modulus, cannot be determined from this test method because the height of the shear zone unknown, so an accurate or representative shear strain cannot be determined.  
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ASTM D7830/D7830M-14(2021)e1(Test Method)
Standard Test Method for In-Place Density (Unit Weight) and Water Content of Soil Using an Electromagnetic Soil Density Gauge

SIGNIFICANCE AND USE
5.1 The method described determines wet density and gravimetric water content by correlating complex impedance measurement data to an empirically developed model. The empirical model is generated by comparing the electrical properties of typical soils encountered in civil construction projects to their wet densities and gravimetric water contents determined by other accepted methods.  
5.2 The test method described is useful as a rapid, non-destructive technique for determining the in-place total density and gravimetric water content of soil and soil-aggregate mixtures and the determination of dry density.  
5.3 This method may be used for quality control and acceptance of compacted soil and soil-aggregate mixtures as used in construction and also for research and development. The non-destructive nature allows for repetitive measurements at a single test location and statistical analysis of the results.
Note 2: The quality of the result produced by this standard test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the requirements of Practice D3740 are generally considered capable of competent and objective sampling/testing/inspection, and the like. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluation some of those factors.
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1.1.1 The method and device described in this test method are intended for in-process quality control of earthwork projects. Site or material characterization is not an intended result.  
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Standard Test Method for Particle-Size Distribution (Gradation) of Fine-Grained Soils Using the Sedimentation (Hydrometer) Analysis

SIGNIFICANCE AND USE
5.1 Particle-size distribution (gradation) is a descriptive term referring to the proportions by dry mass of a soil distributed over specified particle-size ranges. The gradation curve generated using this method yields the distribution of silt and clay size fractions present in the soil based on size definitions, not mineralogy or Atterberg limit classification.  
5.2 Unless the sedimentation sample is representative of the entire sample, the sedimentation results must be combined with a sieve analysis to obtain the complete particle size distribution.  
5.3 The clay size fraction is material finer than 2 µm. The clay size fraction is used in combination with the Plasticity Index (Test Methods D4318) to compute the activity, which provides an indication of the mineralogy of the clay fraction.  
5.4 The gradation of the silt and clay size fractions is an important factor in determining the susceptibility of fine-grained soils to frost action.  
5.5 The gradation of a soil is an indicator of engineering properties such as hydraulic conductivity, compressibility, and shear strength. However, soil behavior for engineering and other purposes is dependent upon many factors, such as effective stress, mineral type, structure, plasticity, and geological origin, and cannot be based solely upon gradation.  
5.6 Some types of soil require special treatment in order to correctly determine the particle sizes. For example, chemical cementing agents can bond clay particles together and should be treated in an effort to remove the cementing agents when possible. Hydrogen peroxide and moderate heat can digest organics. Hydrochloric acid can remove carbonates by washing and Dithionite-Citrate-Bicarbonate extraction can be used to remove iron oxides. Leaching with test water can be used to reduce salt concentration. All of these treatments, however, add significant time and effort when performing the sedimentation test and are allowable but outside the scope of this test method. ...
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1.1 This test method covers the quantitative determination of the distribution of particle sizes of the fine-grained portion of soils. The sedimentation by hydrometer method is used to determine the particle-size distribution (gradation) of the material that is finer than the No. 200 (75-µm) sieve and larger than about 0.2-µm. The test is performed on material passing the No. 10 (2.0-mm) or finer sieve and the results are presented as the mass percent finer of this fraction versus the log of the particle diameter.  
1.2 This method can be used to evaluate the fine-grained fraction of a soil with a wide range of particle sizes by combining the sedimentation results with results from a sieve analysis using D6913 to obtain the complete gradation curve. The method can also be used when there are no coarse-grained particles or when the gradation of the coarse-grained material is not required or not needed.
Note 1: The significant digits recorded in this test method preclude obtaining the grain size distribution of materials that do not contain a significant amount of fines. For example, clean sands will not yield detectable amounts of silt and clay sized particles, and therefore should not be tested with this method. The minimum amount of fines in the sedimentation specimen is 15 g.  
1.3 When combining the results of the sedimentation and sieve tests, the procedure for obtaining the material for the sedimentation analysis and calculations for combining the results will be provided by the more general test method, such as Test Methods D6913 (Note 2).
Note 2: Subcommittee D18.03 is currently developing a new test method “Test Method for Particle-Size Analysis of Soils Combining the Sieve and Sedimentation Techniques.”  
1.4 The terms “soil” and “material” are used interchangeably throughout the standard.  
1.5 The sedimentation analysis is based on the concept that larger particles will fall through a fluid faster than...

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ASTM D6572-21(Test Method)
Standard Test Methods for Determining Dispersive Characteristics of Clayey Soils by the Crumb Test

SIGNIFICANCE AND USE
5.1 The crumb test provides a simple, quick method for field or laboratory identification of a dispersive clayey soil. The internal erosion failures of a number of homogeneous earth dams, erosion along channel or canal banks, and rainfall erosion of earthen structures have been attributed to colloidal erosion along cracks or other flow channels formed in masses of dispersive clay (5).  
5.2 The crumb test, as originally developed by Emerson (6), was called the aggregate coherence test and had seven different categories of soil-water reactions. Sherard (5) later simplified the test by combining some soil-water reactions so that only four categories, or grades, of soil dispersion are observed during the test. The crumb test is a relatively accurate positive indicator of the presence of dispersive properties in a soil. The crumb test, however, is not a completely reliable negative indicator that soils are not dispersive. The crumb test can seldom be relied upon as a sole test method for determining the presence of dispersive clays. The double-hydrometer test (Test Method D4221) and pinhole test (Test Method D4647/D4647M) are test methods that provide valuable additional insight into the probable dispersive behavior of clay soils.
Note 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depends on several factors; Practice D3740 provides a means of evaluating some of those factors.
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1.1 Two test methods are provided to give a qualitative indication of the natural dispersive characteristics of clayey soils: Method A and Method B.  
1.1.1 Method A—Procedure for Natural Soil Crumbs described in 10.1.  
1.1.2 Method B—Procedure for Remolded Soil Crumbs described in 10.2.  
1.2 The crumb test, while a good, quick indication of dispersive soil, should usually be run in conjunction with a pinhole test and a double hydrometer test, Test Methods D4647/D4647M and D4221, respectively. Since this test method may not identify all dispersive clay soils, other tests such as, pinhole dispersion (Test Methods D4647/D4647M), double hydrometer (Test Method D4221) and the analysis of pore water extraction (Test Methods D4542) may be performed individually or used together to help verify dispersion.  
1.3 The crumb test has some limitations in its usefulness as an indicator of dispersive soil. A dispersive soil may sometimes give a non-dispersive reaction in the crumb test. Soils containing kaolinite with known field dispersion problems, have shown non-dispersive reactions in the crumb test (1).2 However, if the crumb test indicates dispersion, the soil is probably dispersive.  
1.4 These test methods are applicable only to soils where the position of the plasticity index versus liquid limit plots (Test Methods D4318) falls on or above the “A” line (Practice D2487) and more than 12 % of the soil fraction is finer than 2-μm as determined in accordance with Test Method D7928.  
1.5 Oven-dried soil should not be used to prepare crumb test specimens, as irreversible changes could occur to the soil pore-water physicochemical properties responsible for dispersion (2).
Note 1: In some cases, the results of the pinhole, crumb, and double-hydrometer test methods may disagree. The crumb test is a better indicator of dispersive soils than of non-dispersive soils (3).  
1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.7 All observed and calculated values shall conform to the guidelines for significant digits and rounding establish...

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ASTM
ASTM D7698-21(Test Method)
Standard Test Method for In-Place Estimation of Density and Water Content of Soil and Aggregate by Correlation with Complex Impedance Method

SIGNIFICANCE AND USE
5.1 CIMI measurements as described in this Standard Test Method are applicable to measurements of compacted soils intended for roads and foundations.  
5.2 The test method is used for estimating in-place values of density and water content of soils and soil-aggregates based on electrical measurements.  
5.3 The test method may be used for quality control and acceptance testing of compacted soil and soil aggregate mixtures as used in construction and also for research and development. The minimal disturbance nature of the methodology allows repetitive measurements in a single test location and statistical analysis of the results.  
5.4 Limitations:  
5.4.1 This test method provides an overview of the CIMI measurement procedure using a controlling console connected to a soil sensor unit which applies a 3.0 MHz RF voltage to an in-place soil via metallic probes that are driven into the soil at a prescribed distance apart. This test method does not discuss the details of the CIMI electronics, computer, or software that utilize on-board algorithms for estimating the soil density and water content  
5.4.2 It is difficult to address an infinite variety of soils in this standard. However, data presented in X3.1 provides a list of soil types that are applicable for the CIMI use.  
5.4.3 The procedures used to specify how data are collected, recorded, or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures prescribed in this standard do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.
Note 1: Notwithstanding th...
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1.1 Purpose and Application—This test method describes the procedure, equipment, and interpretation methods for estimating in-place soil dry density and water content using a Complex-Impedance Measuring Instrument (CIMI).  
1.1.1 The purpose and application of this test method is for testing porous material such as used in roadway base or building foundations that may be deployed in the field at various test sites. The test apparatus includes electrodes that contact the porous material under test and a sensor unit that supplies electromagnetic signals to the porous material. Response signals reveal electrical parameters such as complex impedance which can be equated to material properties such as density and moisture content.  
1.1.2 CIMI measurements as described in this test method are applicable to measurements of compacted soils intended for roads and foundations.  
1.1.3 This test method describes the procedure for estimating in-place density and water content of soils and soil-aggregates by use of a CIMI. The electrical properties of the soil are measured using a radio frequency (RF) voltage source connected to soil electrical probes driven into the soils and soil-aggregates to be tested, in a prescribed pattern and depth. Certain algorithms of these properties are related to wet density and water content. This correlation between electrical measurements, and density and water content is accomplished using a calibration methodology. In the calibration methodology, density and water content are determined by other ASTM Test Standards that measure soil density and water content, thereafter correlating the corresponding measured electrical properties to the soil physical properties.  
1.2 Units—The values stated in SI units are to be regarded as standard. The inch-pound units given in parentheses are mathematical conversions which are provided for information purposes only and are not considered standard.  
1.2.1...

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ASTM
ASTM D7263-21(Test Method)
Standard Test Methods for Laboratory Determination of Density and Unit Weight of Soil Specimens

SIGNIFICANCE AND USE
5.1 Density is a key element in the phase relations, phase relationships, or mass-volume relationships of soil and rock (Appendix X1). When particle density, that is, specific gravity (Test Methods D854) is also known, dry density can be used to calculate porosity and void ratio (see Appendix X1). Dry density measurements are also useful for determining degree of soil compaction. Since water content is variable, total/moist soil density provides little useful information except to estimate the weight of soil per unit volume, for example, grams per cubic centimeter, at the time of sampling. Since soil volume shrinks with drying of swelling soils, total density will vary with water content. Hence, the water content of the soil should be determined at the time of sampling.  
5.2 Densities and unit weights of remolded/reconstituted specimens are commonly used to evaluate the degree of compaction of earthen fills, embankments, and the like. Dry density values are used to calculate dry unit weight values to create a compaction curve (Test Methods D698 and D1557).
Note 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on several factors; Practice D3740 provides a means of evaluating some of these factors.
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1.1 These test methods describe two ways of determining the total/moist/bulk density, dry density, and dry unit weight of intact, disturbed, remolded, and reconstituted (compacted) soil specimens (Note 1). Intact specimens may be obtained from thin-walled sampling tubes, block samples, or clods. Specimens that are remolded by dynamic or static compaction procedures are also measured by these methods. These methods apply to soils that will retain their shape during the measurement process and may also apply to other materials such as soil-cement, soil-lime, soil-bentonite or solidified soil-bentonite-cement slurries. It is common for the density to be less than the value based on tube or mold volumes, or of in situ conditions after removal of the specimen from sampling tubes and compaction molds. This change is due to the specimen swelling after removal of lateral pressures.
Note 1: The adjectives total, moist, wet or bulk are used to represent the density condition. In some professions, such as Soil Science and Geology, the term “bulk density” usually has the same meaning as dry density. In the Geotechnical and Civil Engineering professions, the preferred adjective is total over moist and bulk when referring to the total mass of partially saturated or saturated soil or rock per unit total volume. For more detailed information regarding the term density, refer to Terminology D653.  
1.1.1 Method A (Water Displacement)—A specimen is coated in wax and then placed in water to measure the volume by determining the quantity of water displaced. The density and unit weight are then calculated based on the mass and volume measurements. Do not use this method if the specimen is susceptible to surface wax intrusion.  
1.1.2 Method B (Direct Measurement)—The dimensions and mass of a specimen are measured. The density and unit weight are then calculated using these direct measurements. Usually, the specimen has a cylindrical or cuboid shape. Intact and reconstituted/remolded specimens may be tested by this method in conjunction with strength, permeability/hydraulic conductivity (air/water) and compressibility determinations.  
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard. ...

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