Standard Test Method for Acid Resistance of Ceramic Decorations on Architectural-Type Glass

SIGNIFICANCE AND USE
This test method evaluates the quality and serviceability of a ceramic decoration on architectural type glass. The degree of attack is determined using an acidic solution both quantitatively and qualitatively.  
This test method provides a convenient control test during the manufacture of the ware.
This test method is suitable for specification acceptance.
SCOPE
1.1 This test method covers qualitative determination of the acid resistance of the ceramic decoration on architectural glass.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
28-Feb-2010
Technical Committee
Drafting Committee
Current Stage
Ref Project

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ASTM C724-91(2010) - Standard Test Method for Acid Resistance of Ceramic Decorations on Architectural-Type Glass
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C724 − 91 (Reapproved2010)
Standard Test Method for
Acid Resistance of Ceramic Decorations on Architectural-
Type Glass
This standard is issued under the fixed designation C724; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope all reagents shall conform to the specifications of the Commit-
tee onAnalytical Reagents of theAmerican Chemical Society,
1.1 This test method covers qualitative determination of the
where such specifications are available. Other grades may be
acid resistance of the ceramic decoration on architectural glass.
used, provided it is first ascertained that the reagent is of
1.2 The values stated in SI units are to be regarded as
sufficiently high purity to permit its use without lessening the
standard. No other units of measurement are included in this
accuracy of the determination.
standard.
5.2 Citric Acid Solution(1+9) —Add 10 parts by mass of
1.3 This standard does not purport to address all of the
reagent grade citric acid to 90 parts by mass of distilled water.
safety concerns, if any, associated with its use. It is the
Prepare fresh for each determination.
responsibility of the user of this standard to establish appro-
5.3 Hydrochloric Acid Solution (1 + 9)—Add 10 parts by
priate safety and health practices and determine the applica-
mass of reagent grade concentrated hydrochloric acid (HCl)
bility of regulatory limitations prior to use.
(36 to 38 %) to 90 parts by mass of distilled water.
2. Terminology
6. Procedure
2.1 Definitions:
2.1.1 architectural glass—glass used in the building indus-
6.1 Place four drops of each acid solution on a separate
try.
location on the surface of the ceramic decoration of the
architectural glass to be tested. Cover each spot with a
3. Summary of Test Method
watchglass to retard evaporation and prevent contamination.
3.1 This test method qualitatively determines, by visual
Acid should remain on the surface of the test specimen for 15
inspection, the degree of attack upon a ceramic decoration by min at 20 62°C.
a 10 % citric acid solution and a nominal 3.7 % hydrochloric
6.2 After 15 min of exposure, wash the acid solutions
acid solution.
(1 + 9) from the test specimen with tap water and allow it to air
dry.
4. Significance and Use
4.1 This test method evaluates the quality and serviceability
7. Report
of a ceramic decoration on architectural type glass. The degree
7.1 Report the following information:
of attack is determined using an acidic solution both quantita-
7.1.1 The degree of attack by visual observation by grading
tively and qualitatively.
as follows:
4.2 This test method provides a convenient control test
Grade 1—No attack apparent
during the manufacture of the ware.
Grade 2—Appearance of iridescence or visible stain on the
4.3 This test method is suitable for specification acceptance. exposed surface when viewed at a 45° angle but not apparent
at angles less than 30°
5. Reagent
Grade 3—A definite stain which does not blur reflected
5.1 Purity of Reagents— Reagent
...

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