Standard Practice for Evaluating Absorptive Solar Receiver Materials When Exposed to Conditions Simulating Stagnation in Solar Collectors With Cover Plates

SIGNIFICANCE AND USE
Although this practice is intended for evaluating solar absorber materials and coatings used in flat-plate collectors, no single procedure can duplicate the wide range of temperatures and environmental conditions to which these materials may be exposed during in-service conditions.
This practice is intended as a screening test for absorber materials and coatings. All conditions are chosen to be representative of those encountered in solar collectors with single cover plates and with no added means of limiting the temperature during stagnation conditions.
This practice uses exposure in a simulated collector with a single cover plate. Although collectors with additional cover plates will produce higher temperatures at stagnation, this procedure is considered to provide adequate thermal testing for most applications.
Note 1—Mathematical modelling has shown that a selective absorber, single glazed flat-plate solar collector can attain absorber plate stagnation temperatures as high as 226°C (437°F) with an ambient temperature of 37.8°C (100°F) and zero wind velocity; and a double glazed one as high as 245°C (482°F) under these conditions. The same configuration solar collector with a nonselective absorber can attain absorber stagnation temperatures as high as 146°C (284°F), if single glazed, and 185°C (360°F), if double glazed, with the same environmental conditions, (see “Performance Criteria for Solar Heating and Cooling Systems in Commercial Buildings,” NBS Technical Note 1187 ).
This practice evaluates the thermal stability of absorber materials. It does not evaluate the moisture stability of absorber materials used in actual solar collectors exposed outdoors. Moisture intrusion into solar collectors is a frequent occurrence in addition to condensation caused by diurnal breathing.
This practice differentiates between the testing of spectrally selective absorbers and nonselective absorbers.
Testing Spectrally Selective Absorber Coatings and Materials—Spec...
SCOPE
1.1 This practice covers a test procedure for evaluating absorptive solar receiver materials and coatings when exposed to sunlight under cover plate(s) for long durations. This practice is intended to evaluate the exposure resistance of absorber materials and coatings used in flat-plate collectors where maximum nonoperational stagnation temperatures will be approximately 200°C (392°F).
1.2 This practice shall not apply to receiver materials used in solar collectors without covers (unglazed) or in evacuated collectors, that is, those that use a vacuum to suppress convective and conductive thermal losses.
1.3 The values stated in SI units are to be regarded as the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Publication Date
31-Mar-2009
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ASTM E781-86(2009) - Standard Practice for Evaluating Absorptive Solar Receiver Materials When Exposed to Conditions Simulating Stagnation in Solar Collectors With Cover Plates
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E781 − 86(Reapproved 2009)
Standard Practice for
Evaluating Absorptive Solar Receiver Materials When
Exposed to Conditions Simulating Stagnation in Solar
Collectors With Cover Plates
This standard is issued under the fixed designation E781; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Hemispherical Emittance Using Solar Simulation
E772Terminology of Solar Energy Conversion
1.1 This practice covers a test procedure for evaluating
E903Test Method for Solar Absorptance, Reflectance, and
absorptive solar receiver materials and coatings when exposed
Transmittance of Materials Using Integrating Spheres
to sunlight under cover plate(s) for long durations. This
E962
practice is intended to evaluate the exposure resistance of
absorber materials and coatings used in flat-plate collectors
3. Terminology
where maximum nonoperational stagnation temperatures will
3.1 Definitions:
be approximately 200°C (392°F).
3.1.1 See Terminology E772 for definitions.
1.2 This practice shall not apply to receiver materials used
4. Significance and Use
in solar collectors without covers (unglazed) or in evacuated
collectors, that is, those that use a vacuum to suppress
4.1 Although this practice is intended for evaluating solar
convective and conductive thermal losses.
absorbermaterialsandcoatingsusedinflat-platecollectors,no
single procedure can duplicate the wide range of temperatures
1.3 The values stated in SI units are to be regarded as the
and environmental conditions to which these materials may be
standard.
exposed during in-service conditions.
1.4 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the 4.2 This practice is intended as a screening test for absorber
materials and coatings. All conditions are chosen to be repre-
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica- sentative of those encountered in solar collectors with single
bility of regulatory limitations prior to use. cover plates and with no added means of limiting the tempera-
ture during stagnation conditions.
2. Referenced Documents
4.3 Thispracticeusesexposureinasimulatedcollectorwith
2.1 ASTM Standards:
a single cover plate.Although collectors with additional cover
B537Practice for Rating of Electroplated Panels Subjected
plates will produce higher temperatures at stagnation, this
to Atmospheric Exposure
procedureisconsideredtoprovideadequatethermaltestingfor
D1898Practice for Sampling of Plastics (Withdrawn 1998)
most applications.
E408Test Methods for Total Normal Emittance of Surfaces
NOTE 1—Mathematical modelling has shown that a selective absorber,
Using Inspection-Meter Techniques
single glazed flat-plate solar collector can attain absorber plate stagnation
E434Test Method for Calorimetric Determination of Hemi-
temperatures as high as 226°C (437°F) with an ambient temperature of
spherical Emittance and the Ratio of SolarAbsorptance to
37.8°C (100°F) and zero wind velocity; and a double glazed one as high
as 245°C (482°F) under these conditions. The same configuration solar
collector with a nonselective absorber can attain absorber stagnation
This practice is under the jurisdiction of ASTM Committee E44 on Solar,
temperatures as high as 146°C (284°F), if single glazed, and 185°C
GeothermalandOtherAlternativeEnergySourcesandisthedirectresponsibilityof
(360°F), if double glazed, with the same environmental conditions, (see
Subcommittee E44.05 on Solar Heating and Cooling Systems and Materials.
“Performance Criteria for Solar Heating and Cooling Systems in Com-
Current edition approved April 1, 2009. Published June 2009. Originally 4
mercial Buildings,” NBS Technical Note 1187 ).
approved in 1981. Last previous edition approved in 2003 as E781–86(2003). DOI:
4.4 This practice evaluates the thermal stability of absorber
10.1520/E0781-86R09.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
materials.Itdoesnotevaluatethemoisturestabilityofabsorber
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. AvailablefromU.S.GovernmentPrintingOfficeSuperintendentofDocuments,
The last approved version of this historical standard is referenced on 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401, http://
www.astm.org. www.access.gpo.gov.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E781 − 86 (2009)
materials used in actual solar collectors exposed outdoors. 5.2.1.1 Type I—Tempered low-iron glass with spectral char-
Moistureintrusionintosolarcollectorsisafrequentoccurrence acteristics approximating those shown in Fig. 2.
in addition to condensation caused by diurnal breathing. 5.2.1.2 Type II—Alternativetypesofsolartransmittingglass
or plastic materials might be used for the cover plate if the
4.5 This practice differentiates between the testing of spec-
absorber is to be used under that material.
trally selective absorbers and nonselective absorbers.
5.2.2 The solar-weighted transmittance values of the cover
4.5.1 Testing Spectrally Selective Absorber Coatings and
plate test patches (5.2.3 and 5.2.4) shall remain above the
Materials—Spectrally selective solar absorptive coatings and
indicated percentage of their initial values in the following
materials require testing in a covered enclosure that contains a
wavelength regions:
selectively coated sample mounting plate, such that the enclo-
300 to 400 nm−90%
sureandmountingplatesimulatethetemperatureconditionsof
400 to 2100 nm−95%
a selective flat-plate collector exposed under stagnation condi-
5.2.3 An easily removable test patch of the cover material
tions.
measuring 50 by 50 mm (2 by 2 in.) shall be fastened onto the
4.5.2 Testing Nonselective Coatings and Materials—
innersurfaceofthetransparentcoverplateinornearonelower
Spectrally nonselective solar absorptive coatings and materials
corner.Byperiodicallymeasuringthetransmittanceofthistest
require testing in a covered enclosure that contains a nonse-
patch, an indication of the effect of any condensable effluents
lective coated sample mounting plate, such that the enclosure
on the cover material can be monitored.
and mounting plate simulate the temperature conditions of a
5.2.4 An easily removable specimen of the cover plate
covered, nonselective flat-plate collector exposed under stag-
material measuring 50 by 50 mm (2 by 2 in.) should also be
nation conditions.
mounteddirectlyonanexterioruppercornerofthecoverplate
to monitor the effects of atmospheric contamination and
5. Test Apparatus
ultravioletdegradation.Theseeffectsaregenerallymoresevere
5.1 Test Enclosure—(Fig. 1), consisting of a box that ap-
for plastic materials than for glass.
proximatesthedimensionsofatypicalflat-platesolarcollector
5.3 Seals—A seal that does not outgas at the stagnation
and shall have minimum dimensions of 0.75 by 1.5 by 0.1 m
temperature should be used to make the box weather-resistant.
(29 by 60 by 4 in.) deep. The box should be constructed of
materials that are impervious to moisture. Wood should not be
5.4 Insulation—The bottom and sides of the enclosure shall
usedforconstructionofthebox.Careshallbetakentoprevent
be insulated to have a thermal conductance of less than 0.515
2 2
water leakage at joints, seams, and seals.
W/(m ·K)(0.091 Btu/(h·ft ·°F)), that is, an R value of 11 or
5.1.1 Pre-Exposure of Test Box—Prior to use, the test
greater with materials that do not outgas at the stagnation
apparatus shall be placed in an operational environment where
temperature.
all components are allowed to equilibrate at the stagnation
5.5 Sample Mounting Plate—A metallic mounting plate
temperature for a sufficient length of time to allow for
with lateral dimensions approximately the same as the internal
outgassing of the components. This procedure may aid in
enclosure dimensions (less the thickness of the insulation on
eliminating contamination of the cover plate and the samples
the sides of the box) shall be mounted approximately 10 mm
during actual testing periods and is especially important where
(0.4 in.) above the bottom insulation by a thermally insulating
coatings employing organic components are used. If the cover
material.
plate is in place during this outgassing procedure, it shall be
5.5.1 The mounting plate used to support selective speci-
cleaned before the box is put into service in order to restore its
mens shall have a selective surface. The solar absorptance (α)
original transmittance.
oftheselectivecoatingshallbegreaterthan0.90,andtheroom
5.2 Cover Plate—The box shall have a single cover plate temperature emittance (ε) shall be less than 0.15 at all times.
that is glazed and hinged to provide access.
5.5.2 The mounting plate used to support nonselective
5.2.1 Two types of cover plate materials may be used: specimens shall be coated with any nonselective black coating
FIG. 1 Typical Cross Section of Exposure Test Apparatus
E781 − 86 (2009)
FIG. 2 Transmittance of Low-Iron Glass
that is the
...

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