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ASTM D3728-99

(Specification)

Standard Specification for 2-Ethoxyethyl Acetate (99 % Grade)

Standard Specification for 2-Ethoxyethyl Acetate (99 % Grade)

SCOPE
1.1 This specification covers the properties of 99% grade 2-ethoxyethyl acetate.  
1.2 This material may be suitable for use in urethane coatings, providing that the water content is acceptable.
1.3 For specific hazard information and guidance, see the supplier's Material Safety Data Sheet for materials listed in this specification.

General Information

Status
Historical
Publication Date
09-Jun-1999
ICS
87.060.30 - Solvents
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.35 - Solvents, Plasticizers, and Chemical Intermediates
Current Stage
Ref Project

Relations

Replaced By
ASTM D3728-03 - Standard Specification for 2-Ethoxyethyl Acetate (99 % Grade)
Effective Date
01-Oct-2003

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ASTM D3728-99 - Standard Specification for 2-Ethoxyethyl Acetate (99 % Grade)ASTM D3728-99 - Standard Specification for 2-Ethoxyethyl Acetate (99 % Grade)
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ASTM D3728-99 - Standard Specification for 2-Ethoxyethyl Acetate (99 % Grade)
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NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: D 3728 – 99
AMERICAN SOCIETY FOR TESTING AND MATERIALS
100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
Standard Specification for
1,2
2-Ethoxyethyl Acetate (99 % Grade)
This standard is issued under the fixed designation D 3728; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Properties
1.1 This specification covers the properties of 99 % grade 3.1 2-Ethoxyethyl acetate (99 % grade) shall conform to the
2-ethoxyethyl acetate. following requirements:
1.2 For specific hazard information and guidance, see the
Purity weight %, min 99.0
Alcohol (as 2-ethoxy ethanol) 0.5
supplier’s Material Safety Data Sheet for materials listed in this
weight %, max
specification.
Apparent specific gravity,
1.3 The text of this standard references notes and footnotes
20/20°C 0.973 to 0.976
25/25°C 0.969 to 0.972
that provide explanatory material. These notes and footnotes
Distillation range, °C (see Note 1)
(excluding those in tables and figures) shall not be considered
Initial boiling point, min 150
as requirements of the standard.
Dry point, max 160
Acidity as acetic acid, 0.02, equivalent to 0.19 mg of KOH
weight %, max per gram of sample
2. Referenced Documents
Water, weight %, max 0.10
2.1 ASTM Standards:
Color Pt-Co scale, max 15
D 268 Guide for Sampling and Testing Volatile Solvents
NOTE 1—Optional as agreed upon between the buyer and the seller.
and Chemical Intermediates for Use in Paint and Related
Coatings and Material 4. Sampling
D 1078 Test Method for Distillation Range of Volatile
4.1 The material shall be sampled in accordance with
Organic Liquids
Practice E 300.
D 1209 Test Method for Color of Clear Liquids (Platinum-
5. Test Methods
Cobalt Scale)
D 1364 Test Method for Water in Volatile Solvents (Karl
5.1 The properties enumerated in this specification shall be
Fischer Reagent Titration Method)
determined in accordance with the following ASTM test
D 1613 Test Method for Acidity in Volatile Solvents and
methods:
Chemical Intermediates Used in Paint, Varnish, Lacquer
5.1.1 Purity and Alcohol Content—Test Method D 3545.
and Related Products
5.1.2 Apparent Specific Gravity—Determine the apparent
D 3545 Test Method for Alcohol Content and Purity of
specific gravity by any convenient method that is accurate to
Acetate Esters by Gas Chromatography
the third decimal place, the te
...

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1.1 This test method is for the determination of acetone, methyl acetate, or parachlorobenzotrifluoride (PCBTF), or combination of any of the three, in paints and coatings, by solid phase microextraction (SPME) headspace sampling, and subsequent injection into a gas chromatograph. It has been evaluated for cellulose nitrate, acrylic, and urethane solvent-borne systems. The established working range of this test method is: acetone, 28 to 90 %; methyl acetate, 12 to 22 %; parachlorobenzotrifluoride, 10 to 17 %. There is no reason to believe that it will not work outside these ranges. A minor modification of this test method would make it suitable for the analysis of the same analytes in water-borne coatings (see Note 1).
Note 1: Water-borne paints are internally standardized and diluted with water followed by addition of solid sodium chloride.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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