Standard Practice for Investigating the Effects of Neutron Radiation Damage Using Charged-Particle Irradiation

SIGNIFICANCE AND USE
4.1 A characteristic advantage of charged-particle irradiation experiments is the precise, individual control over most of the important irradiation conditions such as dose, dose rate, temperature, and quantity of gases present. Additional attributes are the lack of induced radioactivation of specimens and, in general, a substantial compression of irradiation time, from years to hours, to achieve comparable damage as measured in displacements per atom (dpa). An important application of such experiments is the investigation of radiation effects that may occur in materials exposed to environments which do not currently exist, such as in first wall materials used in fusion reactors.  
4.2 The primary shortcoming of ion bombardments stems from the damage rate, or temperature dependences of the microstructural evolutionary processes in complex alloys, or both. It cannot be assumed that the time scale for damage evolution can be comparably compressed for all processes by increasing the displacement rate, even with a corresponding shift in irradiation temperature. In addition, the confinement of damage production to a thin layer just (often ∼1 μm) below the irradiated surface can present substantial complications. It must be emphasized, therefore, that these experiments and this practice are intended for research purposes and not for the certification or the qualification of materials.  
4.3 This practice relates to the generation of irradiation-induced changes in the microstructure of metals and alloys using charged particles. The investigation of mechanical behavior using charged particles is covered in Practice E821.
SCOPE
1.1 This practice provides guidance on performing charged-particle irradiations of metals and alloys, although many of the methods may also be applied to ceramic materials. It is generally confined to studies of microstructural and microchemical changes induced by ions of low-penetrating power that come to rest in the specimen. Density changes can be measured directly and changes in other properties can be inferred. This information can be used to estimate similar changes that would result from neutron irradiation. More generally, this information is of value in deducing the fundamental mechanisms of radiation damage for a wide range of materials and irradiation conditions.  
1.2 Where it appears, the word “simulation” should be understood to imply an approximation of the relevant neutron irradiation environment for the purpose of elucidating damage mechanisms. The degree of conformity can range from poor to nearly exact. The intent is to produce a correspondence between one or more aspects of the neutron and charged-particle irradiations such that fundamental relationships are established between irradiation or material parameters and the material response.  
1.3 The practice appears as follows:    
Section  
Apparatus  
4  
Specimen Preparation  
5 – 10  
Irradiation Techniques (including Helium Injection)  
11 – 12  
Damage Calculations  
13  
Postirradiation Examination  
14 – 16  
Reporting of Results  
17  
Correlation and Interpretation  
18 – 22  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-May-2023
Current Stage
Ref Project

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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E521 − 23
Standard Practice for
Investigating the Effects of Neutron Radiation Damage
1
Using Charged-Particle Irradiation
This standard is issued under the fixed designation E521; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
This practice is intended to provide the nuclear research community with recommended procedures
for using charged-particle irradiation to investigate neutron radiation damage mechanisms as a
surrogate for neutron irradiation. It recognizes the diversity of energetic-ion producing devices, the
complexities in experimental procedures, and the difficulties in correlating the experimental results
with those produced by reactor neutron irradiation. Such results may be used to estimate density
changes and the changes in microstructure that would be caused by neutron irradiation. The
information can also be useful in elucidating fundamental mechanisms of radiation damage in reactor
materials.
1. Scope
Section
Apparatus 4
1.1 This practice provides guidance on performing charged-
Specimen Preparation 5 – 10
Irradiation Techniques (including Helium Injection) 11 – 12
particle irradiations of metals and alloys, although many of the
Damage Calculations 13
methods may also be applied to ceramic materials. It is
Postirradiation Examination 14 – 16
generally confined to studies of microstructural and micro- Reporting of Results 17
Correlation and Interpretation 18 – 22
chemical changes induced by ions of low-penetrating power
1.4 The values stated in SI units are to be regarded as
that come to rest in the specimen. Density changes can be
measured directly and changes in other properties can be standard. No other units of measurement are included in this
standard.
inferred. This information can be used to estimate similar
changes that would result from neutron irradiation. More
1.5 This standard does not purport to address all of the
generally, this information is of value in deducing the funda-
safety concerns, if any, associated with its use. It is the
mental mechanisms of radiation damage for a wide range of
responsibility of the user of this standard to establish appro-
materials and irradiation conditions.
priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use.
1.2 Where it appears, the word “simulation” should be
1.6 This international standard was developed in accor-
understood to imply an approximation of the relevant neutron
dance with internationally recognized principles on standard-
irradiation environment for the purpose of elucidating damage
ization established in the Decision on Principles for the
mechanisms. The degree of conformity can range from poor to
Development of International Standards, Guides and Recom-
nearly exact. The intent is to produce a correspondence
mendations issued by the World Trade Organization Technical
between one or more aspects of the neutron and charged-
Barriers to Trade (TBT) Committee.
particle irradiations such that fundamental relationships are
established between irradiation or material parameters and the
2. Referenced Documents
material response.
2
2.1 ASTM Standards:
1.3 The practice appears as follows:
C859 Terminology Relating to Nuclear Materials
E170 Terminology Relating to Radiation Measurements and
Dosimetry
1
This practice is under the jurisdiction of ASTM Committee E10 on Nuclear
Technology and Applications and is the direct responsibility of Subcommittee
2
E10.05 on Nuclear Radiation Metrology. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved June 1, 2023. Published July 2023. Originally approved contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
in 1976. Last previous edition approved in 2016 as E521 – 16. DOI: 10.1520/ Standards volume information, refer to the standard’s Document Summary page on
E0521-23. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E521 − 23
E821 Practice for Measurement of Mechanical Properties fluence.
During Charged-Particle Irradiation heavy ion—used here to denote an ion of mass >4.
E910 Test Method for Application and Analysis of Helium light ion—an arbitrary designation used here for conve-
Accumulation Fluence Monitors for Reactor Vessel S
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E521 − 16 E521 − 23
Standard Practice for
Investigating the Effects of Neutron Radiation Damage
1
Using Charged-Particle Irradiation
This standard is issued under the fixed designation E521; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
This practice is intended to provide the nuclear research community with recommended procedures
for using charged-particle irradiation to investigate neutron radiation damage mechanisms as a
surrogate for neutron irradiation. It recognizes the diversity of energetic-ion producing devices, the
complexities in experimental procedures, and the difficulties in correlating the experimental results
with those produced by reactor neutron irradiation. Such results may be used to estimate density
changes and the changes in microstructure that would be caused by neutron irradiation. The
information can also be useful in elucidating fundamental mechanisms of radiation damage in reactor
materials.
1. Scope
1.1 This practice provides guidance on performing charged-particle irradiations of metals and alloys, although many of the
methods may also be applied to ceramic materials. It is generally confined to studies of microstructural and microchemical changes
induced by ions of low-penetrating power that come to rest in the specimen. Density changes can be measured directly and changes
in other properties can be inferred. This information can be used to estimate similar changes that would result from neutron
irradiation. More generally, this information is of value in deducing the fundamental mechanisms of radiation damage for a wide
range of materials and irradiation conditions.
1.2 Where it appears, the word “simulation” should be understood to imply an approximation of the relevant neutron irradiation
environment for the purpose of elucidating damage mechanisms. The degree of conformity can range from poor to nearly exact.
The intent is to produce a correspondence between one or more aspects of the neutron and charged particle charged-particle
irradiations such that fundamental relationships are established between irradiation or material parameters and the material
response.
1.3 The practice appears as follows:
1
This practice is under the jurisdiction of ASTM Committee E10 on Nuclear Technology and Applications and is the direct responsibility of Subcommittee E10.05 on
Nuclear Radiation Metrology.
Current edition approved Oct. 1, 2016June 1, 2023. Published December 2016July 2023. Originally approved in 1976. Last previous edition approved in 20092016 as
ε2
E521 – 96 (2009)E521 – 16. . DOI: 10.1520/E0521-16.10.1520/E0521-23.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E521 − 23
Section
Apparatus 4
Specimen Preparation 5 – 10
Irradiation Techniques (including Helium Injection) 11–12
Irradiation Techniques (including Helium Injection) 11 – 12
Damage Calculations 13
Postirradiation Examination 14 – 16
Reporting of Results 17
Correlation and Interpretation 18 – 22
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
C859 Terminology Relating to Nuclear Materials
E170 Terminology Relating to Radiation Measurements and Dosimetry
E821 Practice for Measurement of Mechanical Properties During Charged-Particle Irradiation
E910 Test Method for Application and Analysis of Helium Accumulation Fluence Monitors for Reactor Vessel Surveillance
E942 Guide for Investigating the Effects of Helium in Irradiated Metals
3
2.2 ICRU Documen
...

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