Determination of platinum in platinum jewellery alloys - Gravimetric method after reduction with mercury(I) chloride (ISO 11489:1995)

Specifies a gravimetric method for the determination of platinum in platinum jewellery alloys, preferably within the range of fineness stated in ISO 9202. The procedure applies specifically to platinum alloys incorporating palladium, iridium, rhodium, copper, cobalt, gold, ruthenium, gallium, chromium, indium and less than 5 % tungsten. Some modifications are indicated where palladium, iridium, rhodium, gold or ruthenium are present.

Bestimmung von Platin in Platin-Schmucklegierungen - Gravimetrische Bestimmung durch Reduktion mit Quecksilber(I)-chlorid (ISO 11489:1995)

Dosage du platine dans les alliages de platine pour la bijouterie-joaillerie - Méthode gravimétrique après réduction au chlorure de mercure(I) (ISO 11489:1995)

La présente Norme internationale prescrit une méthode gravimétrique de dosage du platine dans les alliages de platine utilisés en bijouterie-joaillerie, de titres compris, de préférence, dans les limites indiquées dans l'ISO 9202. Le mode opératoire s'applique de manière spécifique aux alliages de platine contenant du palladium, de l'iridium, de l'or, du rhodium, du cuivre, du cobalt, du ruthénium, du gallium, du chrome, de l'indium et moins de 5 % de tungstène. Des modifications sont indiquées en cas de présence de palladium, d'or, de ruthénium, d'iridium ou de rhodium.

Določevanje platine v zlitinah za nakit iz platine - Gravimetrična metoda po redukciji z živosrebrovim(I) kloridom (ISO 11489:1995)

General Information

Status
Withdrawn
Publication Date
30-Apr-1995
Withdrawal Date
07-Nov-2017
Current Stage
9960 - Withdrawal effective - Withdrawal
Completion Date
08-Nov-2017

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 11489:1998
01-april-1998
'RORþHYDQMHSODWLQHY]OLWLQDK]DQDNLWL]SODWLQH*UDYLPHWULþQDPHWRGDSR
UHGXNFLML]åLYRVUHEURYLP , NORULGRP ,62
Determination of platinum in platinum jewellery alloys - Gravimetric method after
reduction with mercury(I) chloride (ISO 11489:1995)
Bestimmung von Platin in Platin-Schmucklegierungen - Gravimetrische Bestimmung
durch Reduktion mit Quecksilber(I)-chlorid (ISO 11489:1995)
Dosage du platine dans les alliages de platine pour la bijouterie-joaillerie - Méthode
gravimétrique apres réduction au chlorure de mercure(I) (ISO 11489:1995)
Ta slovenski standard je istoveten z: EN ISO 11489:1995
ICS:
39.060 Nakit Jewellery
SIST EN ISO 11489:1998 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 11489:1998

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SIST EN ISO 11489:1998

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SIST EN ISO 11489:1998

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SIST EN ISO 11489:1998

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SIST EN ISO 11489:1998

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SIST EN ISO 11489:1998
INTERNATIONAL
ISO
STANDARD 11489
First edition
1995-05-01
Determination of platinum in platinum
jewellery alloys - Gravimetric
determination by reduction with mercury( 1)
chloride
Dosage du Platine dans /es alliages de Platine pour Ia
bijouterie-joaillerie - Dosage gravimetrique par reduction au chlorure de
mercurefl)

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SIST EN ISO 11489:1998
ISO 11489:1995(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide
federation of national Standards bodies (ISO member bodies). The work
of preparing International Standards is normally carried out through ISO
technical committees. Esch member body interested in a subject for
which a technical committee has been established has the right to be
represented on that committee. International organizations, governmental
and non-governmental, in liaison with ISO, also take part in the work. ISO
collaborates closely with the International Electrotechnical Commission
(IEC) on all matters of electrotechnical standardization.
Draft International Standards adopted by the technical committees are
circulated to the member bodies for voting. Publication as an International
Standard requires approval by at least 75 % of the member bodies casting
a vote.
International Standard ISO 11489 was prepared by Technical Committee
lSO/TC 174, Jewellery.
Annex A of this International Standard is for information only.
0 ISO 1995
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced
or utilized in any form or by any means, electronrc or mechanical, inciuding photocopying and
microfilm, without Permission in writing from the publisher.
International Organization for Standardization
Case Postale 56 l CH-l 211 Geneve 20 l Switzerland
Printed in Switzerland
ii

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SIST EN ISO 11489:1998
ISO 11489:1995(E)
INTERNATIONAL STANDARD 0 ISO
Determination of platinum in platinum jewellery
alloys - Gravimetric determination by reduction with
mercury(l) chloride
and Palladium will also be precipitated by this re-
1 Scope
duction procedure. Their content shall be determined
separately by, for example, atomic absorption or in-
This International Standard specifies a gravimetric
ductively coupled Plasma (ICP) emission spectro-
method for the determination of platinum in platinum
metry, and a correction applied.
jewellery alloys, preferably within the range of
fineness stated in ISO 9202.
4 Reagents
The procedure applies specifically to platinum alloys
incorporating Palladium, iridium, rhodium, topper,
During the analysis, unless otherwise stated, use only
Cobalt, gold, ruthenium, gallium, chromium, indium
reagents of recognized analytical grade and only dis-
and less than 5 % tungsten. Some modifications are
tilled water or water of equivalent purity.
indicated where Palladium, iridium, rhodium, gold or
ruthenium are present.
4.1 Hydrochlorit acid, 36 % (m/m) to 38 % (m/m),
m
p20 = IJ 9 g/cm ”.
2 Normative reference
4.2 Dilute hydrochloric acid, 18 % (m/m),
The following Standard contains provisions which,
cm3.
p2() = ID g
through reference in this text, constitute provisions
of this International Standard. At the time of publi-
4.3 Dilute hydrochloric acid, 8,5 % (dm),
cation, the edition indicated was valid. All Standards
3
cm .
p20 = 1104 g
are subject to revision, and Parties to agreements
based on this International Standard are encouraged
r)
to investigate the possibility of applying the most re- 4.4 Nitrit acid, 69 % bwbz), p20 = 1
...

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