ISO/TS 14411-1:2017

Preparation of particulate reference materials — Part 1: Polydisperse material based on picket fence of monodisperse spherical particles

ISO/TR 14411-1:2017 describes the preparation of polydisperse spherical particles based on a picket fence of quasi-monodisperse reference materials, the characterization of its monodisperse components with acceptable uncertainty and the estimation of the uncertainty of the mixture of these particles. This type of material is normally suitable for all particle characterization methods within the appropriate limits of the techniques. An example of using these reference materials in a reliability calculation for a mass-based cumulative size distribution is provided. ISO/TR 14411-1:2017 itself to the technical specificities of preparation beyond the general requirements for certified and non-certified reference materials as described in ISO Guide 30, ISO Guide 31, ISO Guide 35 and ISO 17034.

Préparation des matériaux de référence à l'état particulaire — Partie 1: Matériaux polydispersés composés d'un ensemble de particules sphériques monodispersées

General Information

• Status: Published
• Publication Date: 09-May-2017
• ICS: 19.120 - Particle size analysis. Sieving
• Technical Committee: ISO/TC 24/SC 4 - Particle characterization
• Drafting Committee: ISO/TC 24/SC 4/WG 11 - Sample preparation and reference materials
• Current Stage: 9060 - Close of review
• Start Date: 02-Sep-2027

Standards Content (Sample)

TECHNICAL ISO/TS
SPECIFICATION 14411-1
First edition
2017-05
Preparation of particulate reference
materials —
Part 1:
Polydisperse material based on picket
fence of monodisperse spherical
particles
Préparation des matériaux de référence à l’état particulaire —
Partie 1: Matériaux polydispersés composés d’un ensemble de
particules sphériques monodispersées
Reference number
ISO/TS 14411-1:2017(E)
©
ISO 2017

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ISO/TS 14411-1:2017(E)

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ii © ISO 2017 – All rights reserved

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ISO/TS 14411-1:2017(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms, definitions and symbols . 1
3.1 Terms and definitions . 1
3.2 Symbols . 2
4 Material requirements for preparing the individual monodisperse fractions .3
4.1 General description . 3
4.2 Requirements on the general properties of the material for individual pickets . 3
5 Characterization of the individual monodisperse fractions . 4
5.1 Particle size distribution . 4
5.2 Aspect ratio . 5
5.3 Density . 5
5.4 Refractive index . 5
6 Preparation of picket-fence distributions . 5
6.1 General . 5
6.2 Preparation of individual pickets . 6
6.2.1 General. 6
6.2.2 Preparation of suspensions fro
...