Determination of particle size distribution — Electrical sensing zone method — Part 2: Tunable resistive pulse sensing method

This document specifies the measurements of particle size distribution and concentration of suspended particles, ranging from 40 nm to 100 µm, using tunable resistive pulse sensing (TRPS). This document provides a comprehensive overview of the methodologies that are applied to achieve reproducible and accurate TRPS measurement results. This document also includes best practice considerations, possible pitfalls and information on how to alleviate or avoid these pitfalls.

Détermination de la distribution granulométrique — Méthode de détection de zones électrosensibles — Partie 2: Méthode par détection d'impulsions résistives accordable (TRPS)

General Information

Status
Published
Publication Date
18-Sep-2023
Current Stage
6060 - International Standard published
Start Date
19-Sep-2023
Due Date
11-May-2023
Completion Date
19-Sep-2023
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ISO 13319-2:2023 - Determination of particle size distribution — Electrical sensing zone method — Part 2: Tunable resistive pulse sensing method Released:19. 09. 2023
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REDLINE ISO 13319-2 - Determination of particle size distribution — Electrical sensing zone method — Part 2: Tunable resistive pulse sensing method Released:1. 03. 2023
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ISO 13319-2 - Determination of particle size distribution — Electrical sensing zone method — Part 2: Tunable resistive pulse sensing method Released:1. 03. 2023
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ISO/FDIS 13319-2 - Determination of particle size distribution — Electrical sensing zone method — Part 2: Tuneable resistive pulse sensing method Released:2/23/2022
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INTERNATIONAL ISO
STANDARD 13319-2
First edition
2023-09
Determination of particle size
distribution — Electrical sensing zone
method —
Part 2:
Tunable resistive pulse sensing
method
Détermination de la distribution granulométrique — Méthode de
détection de zones électrosensibles —
Partie 2: Méthode par détection d'impulsions résistives accordable
(TRPS)
Reference number
ISO 13319-2:2023(E)
© ISO 2023

---------------------- Page: 1 ----------------------
ISO 13319-2:2023(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2023
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
  © ISO 2023 – All rights reserved

---------------------- Page: 2 ----------------------
ISO 13319-2:2023(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols . 2
5 Principles . 3
6 General operation . 5
6.1 Determination of particle size . 5
6.2 Determination of particle concentration . 6
6.3 Calibration . 6
6.4 Dynamic range . 7
6.5 Coincidence events . 7
6.6 Off-axis particle transport . 8
6.7 Polarization . 8
6.8 Dielectrophoresis . 10
6.9 Drag . 11
7 Operational procedure .
...

ISO/FDIS 13319--2:20222023(E)
ISO/TC 24/SC 4/WG 5
Secretariat: BSI
Determination of particle size distribution — Electrical sensing zone method —
Part 2: TunableTuneable resistive pulse sensing method
Détermination de la distribution granulométrique — Méthode de détection de zones
électrosensibles — Partie 2: Méthode par détection d'impulsions résistives accordable
First edition
Date: 2022-11-252023-03-01

---------------------- Page: 1 ----------------------
ISO/FDIS 13319-2:2022(E)
© ISO 20222023
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of
this publication may be reproduced or utilized otherwise in any form or by any means, electronic or
mechanical, including photocopying, or posting on the internet or an intranet, without prior written
permission. Permission can be requested from either ISO at the address below or ISO's member body in the
country of the requester.
ISO Copyright Office
CP 401 • CH-1214 Vernier, Geneva
Phone: + 41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland.
ii © ISO 2022 – All rights reserved

---------------------- Page: 2 ----------------------
ISO/FDIS 13319-2:2022(E)
Contents Page
Foreword . v
Introduction . vi
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols . 2
5 Principles . 2
6 General operation . 4
6.1 Determination of particle size . 4
6.2 Determination of particle concentration . 5
6.3 Calibration . 6
6.4 Dynamic range . 6
6.5 Coincidence events . 7
6.6 Off-axis particle transport . 7
6.7 Polarisation . 7
6.8 Dielectrophoresis . 8
6.9 Drag . 9
7 Operational procedure . 10
7.1 Instrumental components . 10
7.2 System set-up and optimisation . 10
7.2.1 Preparing fluid cell and stretching the TPU aperture . 10
7.2.2 Wetting the TPU aperture. 11
7.2.3 Establishing stable baseline current and estimating the TPU aperture size . 11
7.2.4 Coating the TPU a
...

FINAL
INTERNATIONAL ISO/FDIS
DRAFT
STANDARD 13319-2
ISO/TC 24/SC 4
Determination of particle size
Secretariat: BSI
distribution — Electrical sensing zone
Voting begins on:
2023-03-15 method —
Voting terminates on:
Part 2:
2023-05-10
Tuneable resistive pulse sensing
method
Détermination de la distribution granulométrique — Méthode de
détection de zones électrosensibles —
Partie 2: Méthode par détection d'impulsions résistives accordable
(TRPS)
RECIPIENTS OF THIS DRAFT ARE INVITED TO
SUBMIT, WITH THEIR COMMENTS, NOTIFICATION
OF ANY RELEVANT PATENT RIGHTS OF WHICH
THEY ARE AWARE AND TO PROVIDE SUPPOR TING
DOCUMENTATION.
IN ADDITION TO THEIR EVALUATION AS
Reference number
BEING ACCEPTABLE FOR INDUSTRIAL, TECHNO-
ISO/FDIS 13319-2:2023(E)
LOGICAL, COMMERCIAL AND USER PURPOSES,
DRAFT INTERNATIONAL STANDARDS MAY ON
OCCASION HAVE TO BE CONSIDERED IN THE
LIGHT OF THEIR POTENTIAL TO BECOME STAN-
DARDS TO WHICH REFERENCE MAY BE MADE IN
NATIONAL REGULATIONS. © ISO 2023

---------------------- Page: 1 ----------------------
ISO/FDIS 13319-2:2023(E)
FINAL
INTERNATIONAL ISO/FDIS
DRAFT
STANDARD 13319-2
ISO/TC 24/SC 4
Determination of particle size
Secretariat: BSI
distribution — Electrical sensing zone
Voting begins on:
method —
Voting terminates on:
Part 2:
Tuneable resistive pulse sensing
method
Détermination de la distribution granulométrique — Méthode de
détection de zones électrosensibles —
Partie 2: Méthode par détection d'impulsions résistives accordable
(TRPS)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2023
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
RECIPIENTS OF THIS DRAFT ARE INVITED TO
ISO copyright office
SUBMIT, WITH THEIR COMMENTS, NOTIFICATION
OF ANY RELEVANT PATENT RIGHTS OF WHICH
CP 401 • Ch. de Blandonnet 8
THEY ARE AWARE AND TO PROVIDE SUPPOR TING
CH-1214 Vernier, Geneva
DOCUMENTATION.
Phone: +41 22 749 01 11
IN ADDITION TO THEIR EVALUATION AS
Reference number
Email: copyright@iso.org
BEING ACCEPTABLE FOR INDUSTRIAL, TECHNO-
ISO/FDIS 13319-2:2023(E)
Website: www.iso.org
LOGICAL, COMMERCIAL AND USER PURPOSES,
DRAFT INTERNATIONAL STANDARDS MAY ON
Published in Switzerland
OCCASION HAVE TO BE CONSIDERED IN THE
LIGHT OF THEIR POTENTIAL TO BECOME STAN-
DARDS TO WHICH REFERENCE MAY BE MADE IN
ii
  © ISO 2023 – All rights reserved
NATIONAL REGULATIONS. © ISO 2023

---------------------- Page: 2 ----------------------
ISO/FDIS 13319-2:2023(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols . 2
5 Principles . 3
6 General operation . 5
6.1 Determination of particle size . 5
6.2 Determination of particle concentration . 6
...

DRAFT INTERNATIONAL STANDARD
ISO/DIS 13319-2
ISO/TC 24/SC 4 Secretariat: BSI
Voting begins on: Voting terminates on:
2022-04-18 2022-07-11
Determination of particle size distribution — Electrical
sensing zone method —
Part 2:
Tuneable resistive pulse sensing method
Détermination de la distribution granulométrique — Méthode de détection de zones électrosensibles —
Partie 2: Méthode par détection d'impulsions résistives accordable (TRPS)
ICS: 19.120
THIS DOCUMENT IS A DRAFT CIRCULATED
FOR COMMENT AND APPROVAL. IT IS
THEREFORE SUBJECT TO CHANGE AND MAY
This document is circulated as received from the committee secretariat.
NOT BE REFERRED TO AS AN INTERNATIONAL
STANDARD UNTIL PUBLISHED AS SUCH.
IN ADDITION TO THEIR EVALUATION AS
BEING ACCEPTABLE FOR INDUSTRIAL,
TECHNOLOGICAL, COMMERCIAL AND
USER PURPOSES, DRAFT INTERNATIONAL
STANDARDS MAY ON OCCASION HAVE TO
BE CONSIDERED IN THE LIGHT OF THEIR
POTENTIAL TO BECOME STANDARDS TO
WHICH REFERENCE MAY BE MADE IN
Reference number
NATIONAL REGULATIONS.
ISO/DIS 13319-2:2022(E)
RECIPIENTS OF THIS DRAFT ARE INVITED
TO SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
PROVIDE SUPPORTING DOCUMENTATION. © ISO 2022

---------------------- Page: 1 ----------------------
ISO/DIS 13319-2:2022(E)
COPYRIGHT PROTECTED DOCUMENT
© ISO 2022
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on
the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below
or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii
  © ISO 2022 – All rights reserved

---------------------- Page: 2 ----------------------
ISO/DIS 13319-2:2022(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols . 2
5 Principles . 2
6 General operation . 4
6.1 Determination of particle size . 4
6.2 Determination of particle concentration . 4
6.3 Calibration . 5
6.4 Dynamic range . 6
6.5 Coincidence events . 6
6.6 Off‐axis particle transport .
...

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