iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
ASTM

ASTM D6349-13

(Test Method)

Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry

Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry

SIGNIFICANCE AND USE
5.1 A compositional analysis of coal and coke and their associated combustion residues are often useful in assessing their quality. Knowledge of the elemental composition of the associated residues is also useful in predicting the elemental enrichment/depletion compositional behavior of ashes and slags in comparison to the concentration levels in the parent coal. Utilization of the ash by-products and hazardous potential may also depend on the chemical composition and leachability of the inorganic constituents of the coal ash.  
5.2 The chemical composition of laboratory-prepared ash may not exactly represent the composition of mineral matter in coal or the composition of fly ash and slag resulting from commerical-scale burning of the coal.
SCOPE
1.1 This test method covers a procedure for the analysis of the commonly determined major and minor elements in coal, coke, and solid residues from combustion of coal and coke. These residues may be laboratory ash, bottom ash, fly ash, flue gas desulfurization sludge, and other combustion process residues.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
30-Sep-2013
ICS
75.160.10 - Solid fuels
Technical Committee
D05 - Coal and Coke
Drafting Committee
D05.29 - Major Elements in Ash and Trace Elements of Coal
Current Stage
Ref Project

Buy Standard

ASTM D6349-13 - Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission SpectrometryASTM D6349-13 - Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry
PreviousNext
Standard
ASTM D6349-13 - Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry
English language
10 pages
sale 15% off
Preview
sale 15% off
Preview
REDLINE ASTM D6349-13 - Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission SpectrometryREDLINE ASTM D6349-13 - Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry
PreviousNext
Standard
REDLINE ASTM D6349-13 - Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry
English language
10 pages
sale 15% off
Preview
sale 15% off
Preview

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D6349 − 13
Standard Test Method for
Determination of Major and Minor Elements in Coal, Coke,
and Solid Residues from Combustion of Coal and Coke by
Inductively Coupled Plasma—Atomic Emission
1
Spectrometry
This standard is issued under the fixed designation D6349; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D7348 Test Methods for Loss on Ignition (LOI) of Solid
Combustion Residues
1.1 This test method covers a procedure for the analysis of
D7582 Test Methods for Proximate Analysis of Coal and
the commonly determined major and minor elements in coal,
Coke by Macro Thermogravimetric Analysis
coke, and solid residues from combustion of coal and coke.
E691 Practice for Conducting an Interlaboratory Study to
These residues may be laboratory ash, bottom ash, fly ash, flue
Determine the Precision of a Test Method
gas desulfurization sludge, and other combustion process
3
2.2 ISO Standard:
residues.
ISO/IEC Guide 99:2007 International vocabulary of metrol-
1.2 The values stated in SI units are to be regarded as
ogy -- Basic and general concepts and associated terms
standard. No other units of measurement are included in this
(VIM)
standard.
1.3 This standard does not purport to address all of the 3. Terminology
safety concerns, if any, associated with its use. It is the
3.1 For definitions of terms used in this test method, refer to
responsibility of the user of this standard to establish appro-
Terminology D121.
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
4. Summary of Test Method
4.1 The sample to be analyzed is ashed under standard
2. Referenced Documents
conditionsandignitedtoconstantweight.Theashisfusedwith
2
2.1 ASTM Standards:
a fluxing agent followed by dissolution of the melt in dilute
D121 Terminology of Coal and Coke
acid solution.Alternatively, the ash is digested in a mixture of
D346 Practice for Collection and Preparation of Coke
hydrofluoric, nitric, and hydrochloric acids. The solution is
Samples for Laboratory Analysis
analyzedbyinductivelycoupledplasma-atomicemissionspec-
D1193 Specification for Reagent Water
trometry (ICP) for the elements. The basis of the method is the
D2013 Practice for Preparing Coal Samples for Analysis
measurement of atomic emissions. Aqueous solutions of the
D3173 Test Method for Moisture in the Analysis Sample of
samples are nebulized, and a portion of the aerosol that is
Coal and Coke
produced is transported to the plasma torch where excitation
D3174 Test Method forAsh in theAnalysis Sample of Coal
and emission occurs. Characteristic line emission spectra are
and Coke from Coal
produced by a radio-frequency inductively coupled plasma. A
D3180 Practice for Calculating Coal and Coke Analyses
gratingmonochromatorsystemisusedtoseparatetheemission
from As-Determined to Different Bases
lines, and the intensities of the lines are monitored by photo-
mutilplier tube or photodiode array detection. The photocur-
rents from the detector are processed and controlled by a
1
This test method is under the jurisdiction of ASTM Committee D05 on Coal
computer system. A background correction technique is re-
and Coke and is the direct responsibility of Subcommittee D05.29 on Major
quired to compensate for variable background contribution to
Elements in Ash and Trace Elements of Coal.
Current edition approved Oct. 1, 2013. Published October 2013. Originally
the determination of elements. Background must be measured
approved in 1998. Last previous edition approved in 2009 as D6349 - 09. DOI:
adjacent to analyte lines of samples during analysis. The
10.1520/D6349-13.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on Available from International Organization for Standardization (ISO), 1 rue de
the ASTM website. Varembé, Case postale 56, CH-1211, Geneva 20, Switzerland, http://www.iso.ch.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D6349 − 13
TABLE 1 Recommended Wavelengths for Elements Determined
and the recommended wavelengths using conventional nebu-
by ICP
lization. Sulfur may only be determined if the sample is
Element Wavelengths, nm
dissolved by the mixed acid dissolution described in 10.3.2.
4
6.1.3 Table 2 lists some interference effects for the recom-
Aluminum 396.152, 256.80, 308.215,
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D6349 − 09 D6349 − 13
Standard Test Method for
Determination of Major and Minor Elements in Coal, Coke,
and Solid Residues from Combustion of Coal and Coke by
Inductively Coupled Plasma—Atomic Emission
1
Spectrometry
This standard is issued under the fixed designation D6349; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers a procedure for the analysis of the commonly determined major and minor elements in coal, coke,
and solid residues from combustion of coal and coke. These residues may be laboratory ash, bottom ash, fly ash, flue gas
desulfurization sludge, and other combustion process residues.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D121 Terminology of Coal and Coke
D346 Practice for Collection and Preparation of Coke Samples for Laboratory Analysis
D1193 Specification for Reagent Water
D2013 Practice for Preparing Coal Samples for Analysis
D3173 Test Method for Moisture in the Analysis Sample of Coal and Coke
D3174 Test Method for Ash in the Analysis Sample of Coal and Coke from Coal
D3180 Practice for Calculating Coal and Coke Analyses from As-Determined to Different Bases
D7348 Test Methods for Loss on Ignition (LOI) of Solid Combustion Residues
D5142D7582 Test Methods for Proximate Analysis of the Analysis Sample of Coal and Coke by Instrumental ProceduresMacro
Thermogravimetric Analysis (Withdrawn 2010)
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
3
2.2 ISO Standard:
ISO/IEC Guide 99:2007 International vocabulary of metrology -- Basic and general concepts and associated terms (VIM)
3. Terminology
3.1 For definitions of terms used in this test method, refer to Terminology D121.
4. Summary of Test Method
4.1 The sample to be analyzed is ashed under standard conditions and ignited to constant weight. The ash is fused with a fluxing
agent followed by dissolution of the melt in dilute acid solution. Alternatively, the ash is digested in a mixture of hydrofluoric,
nitric, and hydrochloric acids. The solution is analyzed by inductively coupled plasma-atomic emission spectrometry (ICP) for the
elements. The basis of the method is the measurement of atomic emissions. Aqueous solutions of the samples are nebulized, and
1
This test method is under the jurisdiction of ASTM Committee D05 on Coal and Coke and is the direct responsibility of Subcommittee D05.29 on Major Elements in
Ash and Trace Elements of Coal.
Current edition approved Nov. 1, 2009Oct. 1, 2013. Published December 2009October 2013. Originally approved in 1998. Last previous edition approved in 20082009
ε1
as D6349 - 08D6349 - 09. . DOI: 10.1520/D6349-09.10.1520/D6349-13.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from International Organization for Standardization (ISO), 1 rue de Varembé, Case postale 56, CH-1211, Geneva 20, Switzerland, http://www.iso.ch.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D6349 − 13
TABLE 1 Recommended Wavelengths for Elements Determined
by ICP
Element Wavelengths, nm
Aluminum 396.152, 256.80, 308.215, 309.271
Barium 455.403, 493.41, 233.53
Calcium 317.93, 315.887, 364.44, 422.67
Iron 259.940, 271.44, 238.204
Magnesium 279.553, 279.08, 285.21, 277.983
Manganese 257.610, 294.92, 293.31, 293.93
Phosphorous 178.287, 214.900
Potassium 766.491, 769.896
Silicon 212.412, 288.16, 251. 611
Sodium 588.995, 589.592
Strontium 421.55
Sulfur 182.04
Titanium 337.280, 350.50, 334.941
a portion of the aerosol that is produced is transported to the plasma torch where excitation and emission occurs. Character
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

ASTM
ASTM D3402/D3402M-23(Test Method)
Standard Test Method for Tumbler Test for Coke

SIGNIFICANCE AND USE
4.1 Coke undergoes various degrees of degradation during removal from coke ovens, transportation, and its decent within a blast furnace to the combustion zone. These processes subject the coke to impact and abrasion. This test method is a relative measure of the resistance of coke to breakage when subjected to these degradation processes.
SCOPE
1.1 This test method describes a procedure for obtaining a relative measure of the resistance to degradation of coke by impact and abrasion.  
1.2 Standard Procedure—This procedure uses a coke sample that is sized to 75 mm by 50 mm [ 3.0 in. by 2 in.].  
1.3 Alternative Procedure—This procedure uses a composite coke sample that is comprised of coke sized 50 % of 63 mm by 50 mm [2.5 in. by 2 in.] and 50 % of 50 mm by 37.5 mm [2 in. by 1.50 in.].  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    5 pages
    English language
    sale 15% off
  • Standard
    5 pages
    English language
    sale 15% off
ASTM
ASTM D388-23(Classification)
Standard Classification of Coals by Rank

ABSTRACT
This specification covers the classification of coals by rank, that is, according to their degree of metamorphism, or progressive alteration, in the natural series from lignite to anthracite. These coals are mainly composed of vitrinite. The classification shall be based on gradational properties that depend on the degree of metamorphism. The classification shall also be according to fixed carbon and gross calorific value calculated to the mineral-matter-free basis.
SIGNIFICANCE AND USE
4.1 This classification establishes categories of coal based on gradational properties that depend principally on the degree of metamorphism to which the coal was subjected while buried. These categories indicate ranges of physical and chemical characteristics that are useful in making broad estimates of the behavior of coal in mining, preparation, and use.
SCOPE
1.1 This standard covers the classification of coals by rank, that is, according to their degree of metamorphism, or progressive alteration, in the natural series from lignite to anthracite.  
1.2 This classification is applicable to coals that are composed mainly of vitrinite.  
Note 1: Coals rich in inertinite or liptinite (exinite), or both, cannot be properly classified because, in those macerals, the properties that determine rank (calorific value, volatile matter, and agglomerating character) differ greatly from those of vitrinite in the same coal. Often, such coals can be recognized by megascopic examination. In North America, these coals are mostly nonbanded varieties that contain only a small proportion of vitrain and consist mainly of attrital materials. The degree of metamorphism of nonbanded and other vitrinite-poor coals can be estimated by determining the classification properties of isolated or concentrated vitrinite fractions, or by determining the reflectance of the vitrinite (see Test Method D2798 and Appendix X1 of this classification). However, in the use of these vitrinite-poor coals, some properties normally associated with rank, such as rheology, combustibility, hardness, and grindability (as well as the rank determining properties) may differ substantially from those of vitrinite-rich coals of the same degree of metamorphism.  
1.3 The accuracy of the classification of impure coal may be impaired by the effect of large amounts of mineral matter on the determination of volatile matter and calorific value, and on their calculation to the mineral-matter-free basis.  
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.  
1.4.1 Exception—The values stated in British thermal units per pound (Btu/lb) are to be regarded as the standard. The SI equivalents of Btu/lb are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    8 pages
    English language
    sale 15% off
  • Standard
    8 pages
    English language
    sale 15% off
ASTM
ASTM D2639/D2639M-23(Test Method)
Standard Test Method for Plastic Properties of Coal by the Constant-Torque Gieseler Plastometer

SIGNIFICANCE AND USE
5.1 Reliable values of the plastic properties of coals are used to predict or explain the behavior of a coal or blends during carbonization or in other processes such as gasification, liquefaction, and combustion.
SCOPE
1.1 This test method covers a relative measure of the plastic behavior of coal when heated under prescribed conditions. This test method may be used to obtain semiquantitative values of the plastic properties of coals and blends used in carbonization and in other situations where determination of plastic behavior of coals is of practical importance.  
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3 In this test method, the term “mass” applies to measurements expressed with both SI units (for example, kg) and inch-pound units (for example, lb).  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
    sale 15% off
  • Standard
    7 pages
    English language
    sale 15% off
ASTM
ASTM D3302/D3302M-22a(Test Method)
Standard Test Method for Total Moisture in Coal

SIGNIFICANCE AND USE
5.1 The collection and treatment of the sample as specified for the referee method is intended for the express purpose of determining the total moisture in coal. The standard is available to producers, sellers, and consumers as a method of determination when other techniques or modifications are not mutually agreed upon.  
5.2 The commercial method, which determines total moisture content of the crushed and divided sample, is designated as the method for total moisture for routine commercial practice.
SCOPE
1.1 This test method covers the measurement of the total moisture in coal as it exists at the site, at the time, and under the conditions it is sampled. It is applicable to coals as mined, processed, shipped, or used in normal commercial pursuits. It is not applicable to coal-water slurries, sludges, or pulverized products under 0.5 mm-diameter sieve size. It is applicable to coals of all ranks within the recognized limitations imposed by oxidation and decomposition characteristics of lower rank coals. Because of its empirical nature, strict adherence to basic principles and permissive procedures are required for valid results (see Appendix X1). This complete standard is available to producers, sellers, and consumers as a total moisture method when other procedures or modifications are not mutually agreed on.  
1.2 Since coal can vary from extremely wet (water-saturated) to completely dry, special emphasis must be placed on the sampling, sample preparation, and the moisture determination itself to ensure total reliability of measurement. Therefore, this standard entails collection of the gross sample, sample preparation, and the method of determination.  
1.3 While it is recognized that such a standard may be unwieldy for routine usage in commercial operations, it can provide a common base for agreement in cases of dispute or arbitration. The complete standard is referred to as the referee method. Embodied in the standard is the commercial method starting with the crushed and divided sample when the gross sample is not too wet to crush and divide. See Practice D2961/D2961M and Test Method D3173 for other moisture methods.  
1.4 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    10 pages
    English language
    sale 15% off
  • Standard
    10 pages
    English language
    sale 15% off
ASTM
ASTM D7430/D7430M-22(Practice)
Standard Practice for Mechanical Sampling of Coal

SIGNIFICANCE AND USE
6.1 It is intended that this practice be used to provide a sample representative of the coal from which it is collected. Because of the variability of coal and the wide variety of mechanical sampling equipment available, caution should be used in all stages of the sample collection process, the design of sampling system specifications, the equipment procurement, and the acceptance testing of installed equipment.  
6.2 After removal from the sampling system and further preparation (Practice D2013/D2013M), the sample may be analyzed for a number of different parameters. These parameters may define the lot's value, its ability to meet specifications, its environmental impact, as well as other properties.
SCOPE
1.1 This practice is divided into four parts: A, B, C, and D. These four parts represent the previous Practices D7256/D7256M, D4916, D4702, and D6518. These four standards are the four that govern the mechanical sampling of coal and have been combined into one document for the ease of reference of the users of these standards.  
1.2 The scope of Part A can be found in Section 4.  
1.3 The scope of Part B can be found in Section 13.  
1.4 The scope of Part C can be found in Section 19.  
1.5 The scope of Part D can be found in Section 32.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 7, 16, 21, 35, and 38.1.1.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    47 pages
    English language
    sale 15% off
  • Standard
    47 pages
    English language
    sale 15% off
ASTM
ASTM D6357-21b(Test Method)
Standard Test Methods for Determination of Trace Elements in Coal, Coke, and Combustion Residues from Coal Utilization Processes by Inductively Coupled Plasma Atomic Emission Spectrometry, Inductively Coupled Plasma Mass Spectrometry, and Graphite Furnace Atomic Absorption Spectrometry

SIGNIFICANCE AND USE
5.1 Coal contains several elements whose individual mass fractions are generally less than 0.01 %. These elements are commonly and collectively referred to as trace elements. These elements primarily occur as part of the mineral matter in coal. The potential release of certain trace elements from coal combustion sources has become an environmental concern.  
5.2 The ash prepared in accordance with these provisional test methods quantitatively retains the elements listed in 1.1 and is representative of their mass fractions in the coal or coke.
SCOPE
1.1 These test methods pertain to the determination of antimony, arsenic, beryllium, cadmium, chromium, cobalt, copper, lead, manganese, molybdenum, nickel, vanadium, and zinc in coal and coke. These test methods can also be used for the analysis of residues from coal combustion processes. Additionally, there are specific test methods outlined that pertain to the determination of rare earth elements in coal and coal combustion residues.
Note 1: These test methods may be applicable to the determination of other trace elements.
Note 2: Rare earth elements are understood to include: cerium, dysprosium, erbium, europium, gadolinium, holmium, lanthanum, lutetium, neodymium, praseodymium, samarium, scandium, terbium, thulium, ytterbium, and yttrium.  
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.2.1 All percentages are percent mass fractions unless otherwise noted.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    16 pages
    English language
    sale 15% off
  • Standard
    16 pages
    English language
    sale 15% off
ASTM
ASTM D4606-21(Test Method)
Standard Test Method for Determination of Arsenic and Selenium in Coal by the Hydride Generation/Atomic Absorption Method

SIGNIFICANCE AND USE
4.1 This test method permits measurement of the total mass fraction of arsenic and selenium in coal for the purpose of evaluating these elements where they can be of concern, for example, in coal combustion. When coal samples are prepared for analysis in accordance with this test method, the arsenic and selenium are quantitatively retained and are representative of the total mass fraction in the coal.
SCOPE
1.1 This test method2 covers the determination of total arsenic in the range of 0.7 ug/g to 12 ug/g and selenium in the range of 0.6 ug/g to 5 ug/g in coal.  
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    5 pages
    English language
    sale 15% off
  • Standard
    5 pages
    English language
    sale 15% off
ASTM
ASTM D4326-21(Test Method)
Standard Test Method for Major and Minor Elements in Coal Ash By X-Ray Fluorescence

SIGNIFICANCE AND USE
5.1 A compositional analysis of ash is used in describing the quality of coal for its complete characterization. Ash composition is useful in predicting slagging and fouling characteristics of combusted materials as well as the potential utilization of ash by-products.  
5.2 The chemical composition of laboratory prepared coal ash is rarely, if ever, representative of the composition of the mineral matter in the coal because the ashing process can alter some minerals. However, it can approximate the composition of the fly ash and slag resulting from commercial combustion of coal.
SCOPE
1.1 This test method covers the analysis of the commonly determined major and minor elements in ash from coal using X-ray fluorescence (XRF) techniques.
Note 1: Test Method D5016 is used for determination of sulfur.
Note 2: Although not included in the present method, the determination of barium, strontium, and manganese may be required to yield adequate totals.  
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    9 pages
    English language
    sale 15% off
  • Standard
    9 pages
    English language
    sale 15% off
ASTM
ASTM D6349-21(Test Method)
Standard Test Method for Determination of Major and Minor Elements in Coal, Coke, and Solid Residues from Combustion of Coal and Coke by Inductively Coupled Plasma—Atomic Emission Spectrometry

SIGNIFICANCE AND USE
5.1 A compositional analysis of coal and coke and their associated combustion residues are often useful in assessing their quality. Knowledge of the elemental composition of the associated residues is also useful in predicting the elemental enrichment/depletion compositional behavior of ashes and slags in comparison to the mass fraction in the parent coal. Utilization of the ash by-products and hazardous potential may also depend on the chemical composition and leachability of the inorganic constituents of the coal ash.  
5.2 The chemical composition of laboratory-prepared ash may not exactly represent the composition of mineral matter in coal or the composition of fly ash and slag resulting from commerical-scale burning of the coal.
SCOPE
1.1 This test method covers a procedure for the analysis of the commonly determined major and minor elements in coal, coke, and solid residues from combustion of coal and coke. These residues may be laboratory ash, bottom ash, fly ash, flue gas desulfurization sludge, and other combustion process residues.
Note 1: There are two interlaboratory studies associated with this test method. The first was conducted in 1997 ( RR:D05-1035)2 and the second was conducted in 2007 ( RR:D05-1032).3 Sulfur trioxide was only included in the 2007 study, and that study only included combustion residues derived from ash and no combustion residues derived from coke.  
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    12 pages
    English language
    sale 15% off
  • Standard
    12 pages
    English language
    sale 15% off
ASTM
ASTM D167/D167M-21a(Test Method)
Standard Test Method for Apparent and True Specific Gravity and Porosity of Lump Coke

SIGNIFICANCE AND USE
4.1 Apparent and true specific gravity, as determined by this test method, are influenced by the type of coals carbonized and the operating and preparational conditions of that carbonization, that is, charge bulk density, heating rate, and pulverization level. In turn, these properties directly influence the performance in processes using coke.
SCOPE
1.1 This test method covers the determination of apparent specific gravity (Sections 5 to 9) and true specific gravity (Sections 10 to 14) of lump coke larger than 25 mm [1 in.] size and calculating porosity (Section 15) from the specific gravity data.  
1.2 Units—The values stated in either SI units or non-SI units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    3 pages
    English language
    sale 15% off
  • Standard
    3 pages
    English language
    sale 15% off