Standard Practice for Determining the Effect of Overbaking on Organic Coatings

SIGNIFICANCE AND USE
Most coatings are designed for a specific baking time and temperature. For a variety of reasons (line stoppages, rerouting back through ovens, oven overheating, etc.) the prescribed time or temperature, or both, of the bake is often exceeded. This practice has been found to be useful in evaluating the effects of overbakes on coatings.
SCOPE
1.1 This practice covers the determination of the time-temperature effect of overbaking on the physical and chemical properties of organic coatings.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of whoever uses this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in Section 7.

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Publication Date
09-Nov-1995
Current Stage
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ASTM D2454-95(2002) - Standard Practice for Determining the Effect of Overbaking on Organic Coatings
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D2454–95(Reapproved 2002)
Standard Practice for
Determining the Effect of Overbaking on Organic Coatings
This standard is issued under the fixed designation D 2454; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope D 1730 Practices for Preparation of Aluminum and
Aluminum-Alloy Surfaces for Painting
1.1 This practice covers the determination of the time-
D 1731 Practices for Preparation of Hot-Dip Aluminum
temperature effect of overbaking on the physical and chemical
Surfaces for Painting
properties of organic coatings.
D 2092 Guide for Preparation of Zinc-Coated (Galvanized)
1.2 This standard does not purport to address all of the
Steel Surfaces for Painting
safety concerns, if any, associated with its use. It is the
D 2197 Test Method for Adhesion of Organic Coatings by
responsibility of whoever uses this standard to consult and
Scrape Adhesion
establish appropriate safety and health practices and deter-
D 2201 Practice for Preparation of Zinc-Coated and Zinc-
mine the applicability of regulatory limitations prior to use.
Alloy-Coated Steel Panels for Testing Paint and Related
Specific hazard statements are given in Section 7.
Coating Products
2. Referenced Documents D 2244 Test Method for Calculation of Color Differences
From Instrumentally Measured Color Coordinates
2.1 ASTM Standards:
D 2794 Test Method for Resistance of Organic Coatings to
D 522 Test Methods for Mandrel Bend Test of Attached
the Effects of Rapid Deformation (Impact)
Organic Coatings
D 3359 Test Methods for Measuring Adhesion by Tape
D 523 Test Method for Specular Gloss
Test
D 609 Practice for Preparation of Cold-Rolled Steel Panels
D 3363 Test Method for Film Hardness by Pencil Test
for Testing Paint, Varnish, Conversion Coatings, and
E 805 Practice for Identification of Instrumental Methods of
Related Coating Products
Color or Color-Difference Measurement of Materials
D 823 Practices for Producing Films of Uniform Thickness
of Paint, Varnish, and Related Products on Test Panels
3. Terminology
D 1005 Test Method for Measurement of Dry-Film Thick-
3.1 Definition:
ness of Organic Coatings Using Micrometers
3.1.1 overbaking—an exposure of the coating to a moder-
D 1186 Test Methods for Nondestructive Measurement of
ately higher temperature or to a longer period of baking, or
Dry Film Thickness of Nonmagnetic Coatings Applied to
2 both,thanrecommendedbythemanufacturerofthecoatingfor
a Ferrous Base
normal curing.This condition is in contrast to “heat resistance”
D 1308 Test Method for Effect of Household Chemicals on
3 which is a parameter relating to the service life of a coating.
Clear and Pigmented Organic Finishes
D 1400 Test Method for Nondestructive Measurement of
4. Summary of Practice
DryFilmThicknessofNonconductiveCoatingsAppliedto
2 4.1 Four panels are prepared and baked at the schedule
a Nonferrous Metal Base
normally recommended for the coating. Two of the panels are
D 1640 Test Methods for Drying, Curing, or Film Forma-
2 then removed and the remaining two are subjected to an
tion of Organic Coatings at Room Temperature
additional overbake in which the time and temperature are
D 1729 Practice for Visual Appraisal of Colors and Color
2 mutually agreed upon between the purchaser and the seller.
Differences of Diffusely-Illuminated Opaque Materials
The sets of panels, after a suitable conditioning interval, are
then evaluated for the properties that are compatible with the
This practice is under the jurisdiction of ASTM Committee D01 on Paint and
substrate. Among these are gloss, color, flexibility, adhesion,
Related Coatings, Materials, and Applications and is the direct responsibility of
impact resistance, and resistance to reagents. Note that glass
Subcommittee D01.27 on Accelerated Testing.
Current edition approved Nov. 10, 1995. Published January 1996. Originally
published as D 2454 – 66 T. Last previous edition D 2454 – 91.
Annual Book of ASTM Standards, Vol 06.01.
3 4
Annual Book of ASTM Standards, Vol 06.02. Annual Book of ASTM Standards, Vol 02.05.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D2454
Test Methods D 1005, D 1186, or D 1400, whichever is applicable. The
substrates should not be tested for impact, and zinc-coated
adhesion, flexibility, and color can vary considerably with thickness.
substrates can influence both flexibility and impact.
8.2 Baking:
5. Significance and Use
8.2.1 The baking schedule for each coating including
5.1 Most coatings are designed for a specific baking time primer, topcoat, and primer/topcoat systems shall be mutually
and temperature. For a variety of reasons (line stoppages, agreed upon between the purchaser and the seller and shall
rerouting back through ovens, oven overheating, etc.) the include the following:
prescribed time or temperature, or both, of the bake is often 8.2.1.1 Normal Baking Schedule (Time and Temperature)
exceeded. This practice has been found to be useful in recommended for the development of optimum film properties,
evaluating the effects of overbakes on coatings. and
8.2.1.2 Overbaking Cycle—This cycle shall be within prac-
6. Materials
tical limits in order to simulate conditions that might be
encountered in actual production where baking oven or con-
6.1 Standard Baking-Type Coating mutually agreed upon
veyor lines, or both might malfunction temporarily due to
between the purchaser and the seller.
mechanical or electrical failure.
7. Hazards 8.3 Prepare four panels of each coating or coating system
and bake them at the schedule normally recommended to
7.1 The flash points of most solvents used in many organic
obtain optimum properties. Conduct the baking of these panels
coatings and related products are low enough that adequate
in a me
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