ASTM D6627/D6627M-11
(Test Method)Standard Test Method for Determination of a Volatile Distillate Fraction of Cold Asphalt Mixtures
Standard Test Method for Determination of a Volatile Distillate Fraction of Cold Asphalt Mixtures
SIGNIFICANCE AND USE
This test method is used for determining the amount of a temperature specific volatile distillate fraction in cold mix asphalt mixtures.
SCOPE
1.1 This test method covers the determination, by direct measurement, of the ambient to 260°C [500°F] volatile distillate fraction of cold mix asphalt mixtures.
1.2 A precision and bias statement for this test method has not been developed since this test method is used for research purposes or information only. Therefore this test method should not be used for acceptance or rejection of a material for purchasing purposes.
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
General Information
Relations
Buy Standard
Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D6627/D6627M − 11
StandardTest Method for
Determination of a Volatile Distillate Fraction of Cold
1
Asphalt Mixtures
This standard is issued under the fixed designation D6627/D6627M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 3. Significance and Use
3.1 This test method is used for determining the amount of
1.1 This test method covers the determination, by direct
a temperature specific volatile distillate fraction in cold mix
measurement, of the ambient to 260°C [500°F] volatile distil-
asphalt mixtures.
late fraction of cold mix asphalt mixtures.
1.2 A precision and bias statement for this test method has
4. Apparatus
not been developed since this test method is used for research
4.1 AVertical Cylindrical Metal Still, similar to that used in
purposes or information only. Therefore this test method
Test Methods D244, having a faced flange at the top to which
should not be used for acceptance or rejection of a material for
theheadistightlyattachedbymeansofaclamp.Theheadshall
purchasing purposes.
be of a metal, preferably copper or brass, and shall be provided
1.3 The values stated in either SI units or inch-pound units with a tubular opening of 25 mm [1 in.] in inside diameter and
1
are to be regarded separately as standard. The values stated in an additional tubular opening of 13 mm [ ⁄2 in.] in inside
each system may not be exact equivalents; therefore, each diameter. Threaded into the 25 mm [1 in.] tubular opening is a
system shall be used independently of the other. Combining stainless steel or brass fitting connected firmly to a ground
values from the two systems may result in nonconformance glass joint by means of flexible stainless steel or glass tubing.
1
with the standard. Inserted into the 13 mm [ ⁄2 in.] tubular opening is a metal
thermometer with a range of 93 to 538°C (200 to 1000°F)
1.4 This standard does not purport to address all of the
extending 125 mm [5 in.] into the metal still and firmly
safety concerns, if any, associated with its use. It is the
connected by means of a graphite ferrule compression fitting.
responsibility of the user of this standard to establish appro-
4.2 Condenser, of the water-cooled reflux glass-tube type,
priate safety and health practices and determine the applica-
3
bility of regulatory limitations prior to use. having a condenser jacket not less than 400 mm [15 ⁄4 in.] long
3 1
with an inner tube 9.5 to 13 mm [ ⁄8 to ⁄2 in.] in the outside
diameter.The end of the condenser inserted in the ground glass
2. Referenced Documents
joint shall be ground off at an angle of 30° from the vertical
2
2.1 ASTM Standards:
axis of the condenser. For mixtures with very volatile solvents,
D244 Test Methods and Practices for Emulsified Asphalts
it may be necessary to supplement this water-cooled condenser
D979 Practice for Sampling Bituminous Paving Mixtures
with a second water-cooled condenser of approximately the
D1461 Test Method for Moisture or Volatile Distillates in
same dimensions.
Bituminous Paving Mixtures
4.3 CollectionFlask, cylinder of well-annealed glass having
D4753 Guide for Evaluating, Selecting, and Specifying Bal-
acapacityof100mL[3.4floz.]graduatedwithdivisionsof0.1
ances and Standard Masses for Use in Soil, Rock, and
mL[0.003 fl oz.] and attached to the condenser(s) by means of
Construction Materials Testing
a well-annealed glass bend. The glass bend attaching the
condenser to the graduated cylinder is secured by ground glass
1
joints on either end and vented witha3mm[ ⁄8 in.] vent on top
1
This test method is under the jurisdiction of ASTM Committee D04 on Road
of the bend directly above the graduated cylinder to prevent
and Paving Materials and is the direct responsibility of Subcommittee D04.27 on
pressure in the apparatus. The collection flask is submerged to
Cold Mix Asphalts.
Current edition approved June 1, 2011. Published July 2011. Originally approved the top of the gradations in an ice bath.
in 2001. Last previous edition approved in 2006 as D6627 – 01(2006). DOI:
4.4 Distillation Liquid, 40 mL [1.4 fl oz.] of distilled water.
10.1520/D6627_D6627M-11.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
4.5 Heating Device, of high temperature electrical heating
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
tape wrapped around the entire still and the connecting tubing
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. between the still and condenser.Avariable voltage transformer
Copyright © ASTM International, 100 Barr Harbor Drive, P
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D6627–01(Reapproved 2006) Designation: D6627/D6627M – 11
Standard Test Method for
Determination of a Volatile Distillate Fraction of Cold
1
Asphalt Mixtures
This standard is issued under the fixed designation D6627/D6627M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1This test method covers the determination, by direct measurement, of the ambient to 500°F (260°C) volatile distillate fraction
of cold mix asphalt mixtures.
1.2A precision and bias statement for the Standard has not been developed since this test method is used for research purposes
or information only. Therefore this Standard should not be used for acceptance or rejection of a material for purchasing purposes.
1.3The values stated in inch-pound units are to be regarded as the standard.The SI units given in parentheses are for information
only.
1.1 This test method covers the determination, by direct measurement, of the ambient to 260°C [500°F] volatile distillate
fraction of cold mix asphalt mixtures.
1.2 A precision and bias statement for this test method has not been developed since this test method is used for research
purposes or information only.Therefore this test method should not be used for acceptance or rejection of a material for purchasing
purposes.
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each
system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the
two systems may result in nonconformance with the standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D244 Test Methods and Practices for Emulsified Asphalts
D979 Practice for Sampling Bituminous Paving Mixtures
D1461 Test Method for Moisture or Volatile Distillates in Bituminous Paving Mixtures
D4753 Guide for Evaluating, Selecting, and Specifying Balances and Standard Masses for Use in Soil, Rock, and Construction
Materials Testing
3. Significance and Use
3.1 This test method is used for determining the amount of a temperature specific volatile distillate fraction in cold mix asphalt
mixtures.
4. Apparatus
4.1 A Vertical Cylindrical Metal Still, similar to that used in Test Methods D244, having a faced flange at the top to which the
head is tightly attached by means of a clamp. The head shall be of a metal, preferably copper or brass, and shall be provided with
1
a tubular opening of 25 mm (1 in.)[1 in.] in inside diameter and an additional tubular opening of 13 mm ([ ⁄2 in.) in.] in inside
diameter. Threaded into the 25 mm (1 in.)[1 in.] tubular opening is a stainless steel or brass fitting connected firmly to a ground
1
glass joint by means of flexible stainless steel or glass tubing. Inserted into the 13 mm ([ ⁄2 in.) in.] tubular opening is a metal
1
This test method is under the jurisdiction ofASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.27 on Cold Mix
Asphalts.
Current edition approved Dec. 15, 2006. Published December 2006. Originally approved in 2001. Last previous edition approved in 2001 as D6627–01. DOI:
10.1520/D6627-01R06.
Current edition approved June 1, 2011. Published July 2011. Originally approved in 2001. Last previous edition approved in 2006 as D6627 – 01(2006). DOI:
10.1520/D6627_D6627M-11.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. ForAnnualBookofASTMStandards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
---------------------- Page: 1 ----------------------
D6627/D6627M – 11
thermometer with a range of 93 to 538°C (200 to 1000°F) extending 125 mm (5 in.)[5 in.] into the metal still and firmly connected
by means of a graphite ferrule compression fitting.
3
4.2 Condenser, of the water-cooled reflux glass-tube type, having a condenser
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.