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ASTM D6209-98(2004)

(Test Method)

Standard Test Method for Determination of Gaseous and Particulate Polycyclic Aromatic Hydrocarbons in Ambient Air (Collection on Sorbent-Backed Filters with Gas Chromatographic/Mass Spectrometric Analysis)

Standard Test Method for Determination of Gaseous and Particulate Polycyclic Aromatic Hydrocarbons in Ambient Air (Collection on Sorbent-Backed Filters with Gas Chromatographic/Mass Spectrometric Analysis)

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1.1 This test method specifies sampling, cleanup, and analysis procedures for the determination of polycyclic aromatic hydrocarbons (PAH) in ambient air.
1.2 This test method is designed to collect both gas-phase and particulate-phase PAH and to determine them collectively.
1.3 This test method is a high-volume sampling (100 to 250 L/min) method capable of detecting PAH at sub-nanograms per cubic metre (ng/m3) concentrations with sampling volumes up to 350 m3 of air.
1.4 This test method has been validated for sampling periods up to 24 h.
1.5 Precision and bias under normal conditions can be expected to be 35 to 50 %.
1.6 This test method describes a sampling and analysis procedure for PAH that involves collection from air on a combination fine-particle filter and sorbent trap and subsequent analysis by gas chromatography/mass spectrometry (GC/MS).
1.7 The range of this test method is approximately 0.05 to 1000 ng/m3 of air sampled.
1.8 The values stated in SI units shall be regarded as standard.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See also Section for additional safety precautions.

General Information

Status
Historical
Publication Date
30-Sep-2004
ICS
13.040.20 - Ambient atmospheres
Technical Committee
D22 - Air Quality
Drafting Committee
D22.03 - Ambient Atmospheres and Source Emissions
Current Stage
Ref Project

Relations

Replaces
ASTM D6209-98e1 - Standard Test Method for Determination of Gaseous and Particulate Polycyclic Aromatic Hydrocarbons in Ambient Air (Collection on Sorbent-Backed Filters with Gas Chromatographic/Mass Spectrometric Analysis)
Effective Date
01-Oct-2004
Replaced By
ASTM D6209-98(2012) - Standard Test Method for Determination of Gaseous and Particulate Polycyclic Aromatic Hydrocarbons in Ambient Air (Collection on Sorbent-Backed Filters with Gas Chromatographic/Mass Spectrometric Analysis)
Effective Date
01-Nov-2012

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ASTM D6209-98(2004) - Standard Test Method for Determination of Gaseous and Particulate Polycyclic Aromatic Hydrocarbons in Ambient Air (Collection on Sorbent-Backed Filters with Gas Chromatographic/Mass Spectrometric Analysis)ASTM D6209-98(2004) - Standard Test Method for Determination of Gaseous and Particulate Polycyclic Aromatic Hydrocarbons in Ambient Air (Collection on Sorbent-Backed Filters with Gas Chromatographic/Mass Spectrometric Analysis)
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ASTM D6209-98(2004) - Standard Test Method for Determination of Gaseous and Particulate Polycyclic Aromatic Hydrocarbons in Ambient Air (Collection on Sorbent-Backed Filters with Gas Chromatographic/Mass Spectrometric Analysis)
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D6209 − 98(Reapproved 2004)
Standard Test Method for
Determination of Gaseous and Particulate Polycyclic
Aromatic Hydrocarbons in Ambient Air (Collection on
Sorbent-Backed Filters with Gas Chromatographic/Mass
1
Spectrometric Analysis)
This standard is issued under the fixed designation D6209; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope bility of regulatory limitations prior to use. See also Section 8
2 for additional safety precautions.
1.1 This test method specifies sampling, cleanup, and
analysis procedures for the determination of polycyclic aro-
2. Referenced Documents
matic hydrocarbons (PAH) in ambient air.
3
2.1 ASTM Standards:
1.2 This test method is designed to collect both gas-phase
D1356Terminology Relating to Sampling and Analysis of
and particulate-phase PAH and to determine them collectively.
Atmospheres
1.3 Thistestmethodisahigh-volumesampling(100to250
D1357Practice for Planning the Sampling of the Ambient
L/min)methodcapableofdetectingPAHatsub-nanogramsper
Atmosphere
3
cubic metre (ng/m ) concentrations with sampling volumes up
D3631Test Methods for Measuring Surface Atmospheric
3
to 350 m of air.
Pressure
E1Specification for ASTM Liquid-in-Glass Thermometers
1.4 This test method has been validated for sampling
periods up to 24 h.
3. Terminology
1.5 Precision and bias under normal conditions can be
3.1 Definitions—For definitions of terms used in this test
expected to be 635 to 50%.
method, refer to Terminology D1356.
1.6 This test method describes a sampling and analysis
3.2 Definitions of Terms Specific to This Standard:
procedure for PAH that involves collection from air on a
3.2.1 sampling effıciency (SE), n—ability of the sampler to
combinationfine-particlefilterandsorbenttrapandsubsequent
trap and retain PAH. The percent SE is the percentage of the
analysis by gas chromatography/mass spectrometry (GC/MS).
analyte of interest collected and retained by the sampling
1.7 The range of this test method is approximately 0.05 to
medium when it is introduced into the air sampler and the
3
1000 ng/m of air sampled.
sampler is operated under normal conditions for a period of
time equal to or greater than that required for the intended use.
1.8 The values stated in SI units shall be regarded as
standard.
3.2.2 dynamic retention effıciency, n—ability of the sam-
pling medium to retain a given PAH that has been added to the
1.9 This standard does not purport to address all of the
sorbenttrapinaspikingsolutionwhenairisdrawnthroughthe
safety concerns, if any, associated with its use. It is the
sampler under normal conditions for a period of time equal to
responsibility of the user of this standard to establish appro-
or greater than that required for the intended use.
priate safety and health practices and determine the applica-
4. Summary of Test Method
1 4.1 Sampling:
This test method is under the jurisdiction of ASTM Committee D22 on Air
Qualityand is the direct responsibility of Subcommittee D22.03 on Ambient 4.1.1 An air sample is collected directly from the ambient
Atmospheres and Source Emissions.
atmosphere by pulling air at approximately 225 L/min through
Current edition approved Oct. 1, 2004. Published December 2004. Originally
a fine particulate filter followed by a vapor trap containing
ε1
approved in 1997. Last previous edition approved in 1998 as D6209-98 . DOI:
10.1520/D6209-98R04.
2
This test method is based on U. S. Environmental ProtectionAgency Compen-
3
dum Method TO-13, Compendium of Methods for the Determination of Toxic For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Organic Compounds in Ambient Air, Report No. EPA/600-4-89/018, June 1988, contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
available from the National Technical Information Service, 5285 Port Royal Rd., Standards volume information, refer to the standard’s Document Summary page on
Springfield, VA 22161, Order No. PB90-11989/AS. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D6209 − 98 (2004)
TABLE 1 Formulae and Physical Properties of Selective PAH
Vapor
Melting
Boiling
Compound Molecular Pressure,
A
Formula Point, Point,
(Common Name) Weight kPa at
°C
°C
25°C
–2
Naphthalene C H 128.18 80.2 218 1.1 × 10
10 8
–3
Acenaphthylene C H 152.20 92-93 265-280 3.9 × 10
12 8
–2
Acenaphthene C H 154.20 90-96 278-279 2.1 × 10
12 10
–5
Fluorene C H 166.23 116-118 293-295 8.7 × 10
13 10
–5
9-Fluorenone C H O 180.21
...

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1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D1914-95(2022)(Practice)
Standard Practice for Conversion Units and Factors Relating to Sampling and Analysis of Atmospheres

SIGNIFICANCE AND USE
3.1 ASTM requires the use of SI units in all its publications and their use in reporting atmospheric measurement data. However, there are historic data and even data currently reported that are based on a variety of units of measurement. This practice tabulates factors that are necessary to convert such data to SI and other units of measurement.  
3.2 IEEE/ASTM SI-10 does not list all the conversion factors commonly used in air pollution and meteorological fields. This practice supplements IEEE/ASTM SI-10.  
3.3 The values reported here were obtained from a number of standard publications. They were adjusted to five figures and organized in a rational order. All values reflect the latest information from the 16th General Conference on Weights and Measurements held in 1979.  
3.4 The factors in Table 1 are provided to change units of measurement from one system to related units in other systems, as well as to smaller or larger units in the same system.  
3.5 Values of units in the left column may be converted to values of units in the right column merely by multiplying by the conversion factor provided in the center column.  (A) For specific applications and exceptions, see Terminology D1356.
SCOPE
1.1 This practice provides units and factors useful for members of the air pollution and meteorological communities.  
1.2 This practice is used together with IEEE/ASTM SI-10, which discusses SI units and contains selected conversion factors for inter-relation of SI units and some commonly used non-metric units.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D2914-15(2022)(Test Method)
Standard Test Methods for Sulfur Dioxide Content of the Atmosphere (West-Gaeke Method)

SIGNIFICANCE AND USE
5.1 Sulfur dioxide is a major air pollutant, commonly formed by the combustion of sulfur-bearing fuels. The Environmental Protection Agency (EPA) has set primary and secondary air quality standards (7) that are designed to protect the public health and welfare.  
5.2 The Occupational Safety and Health Administration (OSHA) has promulgated exposure limits for sulfur dioxide in workplace atmospheres (8).  
5.3 These methods have been found satisfactory for measuring sulfur dioxide in ambient and workplace atmospheres over the ranges pertinent in 5.1 and 5.2.  
5.4 Method A has been designed to correspond to the EPA-Designated Reference Method (7) for the determination of sulfur dioxide.
SCOPE
1.1 These test methods cover the bubbler collection and colorimetric determination of sulfur dioxide (SO2) in the ambient or workplace atmosphere.  
1.2 These test methods are applicable for determining SO2 over the range from approximately 25 μg/m3 (0.01 ppm(v)) to 1000 μg/m3 (0.4 ppm(v)), corresponding to a solution concentration of 0.03 μg SO2/mL to 1.3 μg SO2/mL. Beer's law is followed through the working analytical range from 0.02 μg SO2/mL to 1.4 μg SO2/mL.  
1.3 The lower limit of detection is 0.075 μg SO2/mL (1),2 representing an air concentration of 25 μg SO2/m3 (0.01 ppm(v)) in a 30-min sample, or 13 μg SO2/m3 (0.005 ppm(v)) in a 24-h sample.  
1.4 These test methods incorporate sampling for periods between 30 min and 24 h.  
1.5 These test methods describe the determination of the collected (impinged) samples. A Method A and a Method B are described.  
1.6 Method A is preferred over Method B, as it gives the higher sensitivity, but it has a higher blank. Manual Method B is pH-dependent, but is more suitable with spectrometers having a spectral band width greater than 20 nm.
Note 1: These test methods are applicable at concentrations below 25 μg/m3 by sampling larger volumes of air if the absorption efficiency of the particular system is first determined, as described in Annex A4.
Note 2: Concentrations higher than 1000 μg/m3 can be determined by using smaller gas volumes, larger collection volumes, or by suitable dilution of the collected sample with absorbing solution prior to analysis.  
1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.8 Warning—Mercury has been designated by many regulatory agencies as a hazardous material that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Safety Data Sheet (SDS) for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.  
1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see 8.3.1, Section 9, and A3.1.3.  
1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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