Standard Practice for Testing Graphite and Boronated Graphite Materials for High-Temperature Gas-Cooled Nuclear Reactor Components

SIGNIFICANCE AND USE
Property data obtained with the recommended test methods identified herein may be used for research and development, design, manufacturing control, specifications, performance evaluation, and regulatory statutes pertaining to high temperature gas-cooled reactors.
The test methods are applicable primarily to specimens in the non-irradiated and non-oxidized state. Many are also applicable to specimens in the irradiated or oxidized state, or both, provided the specimens meet all requirements of the test method. The user is cautioned to consider the instructions given in the test methods.
Additional test methods are in preparation and will be incorporated. The user is cautioned to employ the latest revision.
SCOPE
1.1 This practice covers the test methods for measuring the properties of graphite and boronated graphite materials. These properties may be used for the design and evaluation of high-temperature gas-cooled reactor components.
1.2 The test methods referenced herein are applicable to materials used for replaceable and permanent components as defined in Section 7 and Section 9, and includes fuel elements; removable reflector elements and blocks; permanent side reflector elements and blocks; core support pedestals and elements; control rod, reserve shutdown, and burnable poison compacts; and neutron shield material.
1.3 This practice includes test methods that have been selected from existing ASTM standards, ASTM standards that have been modified, and new ASTM standards that are specific to the testing of materials listed in 1.2. Comments on individual test methods for graphite and boronated graphite components are given in Sections 8 and 10, respectively. The test methods are summarized in Tables 1 and 2.
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
TABLE 1 Summary of Test Methods for Graphite Components
Note—Designations under preparation will be added when approved.  Fuel, Removable Reflector,
and Core Support Elements;
Pebble Bed Reflector,
Key and Sleeves;
and Dowel PinsPermanent Side
Reflector Elements
and Dowel PinsCore Support Pedestals
and Dowels Fabrication  As Manufactured Bulk DensityC838C838C838 Mechanical Properties  Compressive StrengthC695C695C695  Tensile PropertiesC749AC749AC749A  Poisson’s RatioE132BE132BE132B  Flexural StrengthC651AC651AC651A  Fracture ToughnessBBB  Modulus of ElasticityC747C747C747 Physical Properties  Bulk Density–Machined SpecimensC559C559C559  Surface Area (BET)C1274C1274C1274  PermeabilityC577A,BC577A,BC577A,B  Apparent PorosityC1039C1039C1039  Spectroscopic AnalysisBBB  Electrical ResistivityC611C611C611 Thermal Properties  Linear Thermal ExpansionE228A  Thermal ConductivityE1461AE1461AE1461A Chemical Properties  Oxidative Mass LossC1179BC1179BC1179B  Sulfur ConcentrationC816C816C816  Ash ContentC561AC561AC561A  Equivalent Boron ContentC1233AC1233AC
A Modification of this test method is required. See Section 8 for details.
B New test methods are required. See Section 8 for details.
C There is no identified need for determining this property.
TABLE 2 Summary of Test Methods for Boronated Graphite Components
Note—Designations under preparation will be added when approved.  CompactsNeutron
Shield
Material Control
RodBurnable
PoisonReserve
Shutdown Bulk DensityC838C838C838D4292 Linear Thermal ExpansionAE228AE228AB Particle SizeCCCD2862 Mechanical Strength:  Compressive StrengthC695AC695AC695AB  Impact PerformanceBBBC Chemical Properties:  Sulfur ConcentrationCCCC  Hafnium ConcentrationCCCC  Relative Oxidation RateCCCC Boron Analysis:  Total ...

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C781 − 08 AnAmerican National Standard
Standard Practice for
Testing Graphite and Boronated Graphite Materials for High-
1
Temperature Gas-Cooled Nuclear Reactor Components
This standard is issued under the fixed designation C781; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* ments of Manufactured Carbon and Graphite Articles
C561 Test Method for Ash in a Graphite Sample
1.1 This practice covers the test methods for measuring the
C577 Test Method for Permeability of Refractories
properties of graphite and boronated graphite materials. These
C611 TestMethodforElectricalResistivityofManufactured
properties may be used for the design and evaluation of
Carbon and Graphite Articles at Room Temperature
high-temperature gas-cooled reactor components.
C625 Practice for Reporting Irradiation Results on Graphite
1.2 The test methods referenced herein are applicable to
C651 Test Method for Flexural Strength of Manufactured
materials used for replaceable and permanent components as
CarbonandGraphiteArticlesUsingFour-PointLoadingat
defined in Section 7 and Section 9, and includes fuel elements;
Room Temperature
removable reflector elements and blocks; permanent side
C695 Test Method for Compressive Strength of Carbon and
reflector elements and blocks; core support pedestals and
Graphite
elements; control rod, reserve shutdown, and burnable poison
C709 Terminology Relating to Manufactured Carbon and
compacts; and neutron shield material.
Graphite
1.3 This practice includes test methods that have been
C747 Test Method for Moduli of Elasticity and Fundamental
selected from existing ASTM standards, ASTM standards that
Frequencies of Carbon and Graphite Materials by Sonic
have been modified, and newASTM standards that are specific
Resonance
tothetestingofmaterialslistedin1.2.Commentsonindividual
C749 Test Method for Tensile Stress-Strain of Carbon and
test methods for graphite and boronated graphite components
Graphite
are given in Sections 8 and 10, respectively. The test methods
C769 Test Method for Sonic Velocity in Manufactured
are summarized in Tables 1 and 2.
Carbon and Graphite Materials for Use in Obtaining
1.4 The values stated in SI units are to be regarded as
Young’s Modulus
standard. The values given in parentheses are for information
C816 Test Method for Sulfur in Graphite by Combustion-
only.
Iodometric Titration Method
1.5 This standard does not purport to address all of the C838 Test Method for Bulk Density of As-Manufactured
safety concerns, if any, associated with its use. It is the Carbon and Graphite Shapes
responsibility of the user of this standard to establish appro- C1039 Test Methods for Apparent Porosity, Apparent Spe-
priate safety and health practices and determine the applica- cific Gravity, and Bulk Density of Graphite Electrodes
bility of regulatory limitations prior to use.
C1179 Test Method for Oxidation Mass Loss of Manufac-
tured Carbon and Graphite Materials in Air
2. Referenced Documents
C1233 Practice for Determining Equivalent Boron Contents
2
of Nuclear Materials
2.1 ASTM Standards:
C1274 Test Method forAdvanced Ceramic Specific Surface
C559 Test Method for Bulk Density by Physical Measure-
Area by Physical Adsorption
D346 Practice for Collection and Preparation of Coke
1
Samples for Laboratory Analysis
This practice is under the jurisdiction of ASTM Committee D02 on Petroleum
Products and Lubricants and is the direct responsibility of Subcommittee D02.F0 on
D1193 Specification for Reagent Water
Manufactured Carbon and Graphite Products.
D2854 Test Method for Apparent Density of Activated
Current edition approved Sept. 1, 2008. Published October 2008. Originally
Carbon
approved in 1977. Last previous edition approved in 2002 as C781–02. DOI:
10.1520/C0781-08.
D2862 Test Method for Particle Size Distribution of Granu-
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
lar Activated Carbon
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
D3104 Test Method for Softening Point of Pitches (Mettler
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. Softening Point Method)
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C781 − 08
TABLE 1 Summary of Test Methods for Graphite Components
NOTE 1—Designations under preparation will be added when approved.
Fuel, Removable Reflector,
and Cor
...

This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
An American National Standard
Designation:C 781–02 Designation: C 781 – 08
Standard Practice for
Testing Graphite and Boronated Graphite
ComponentsMaterials for High-Temperature Gas-Cooled
1
Nuclear Reactor Components
This standard is issued under the fixed designation C 781; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1This practice covers the test methods for measuring those properties of graphite and boronated graphite materials that may
be used for the design and evaluation of high-temperature gas-cooled reactors. *
1.1 This practice covers the test methods for measuring the properties of graphite and boronated graphite materials. These
properties may be used for the design and evaluation of high-temperature gas-cooled reactor components.
1.2 The test methods referenced herein are applicable to materials used for replaceable and permanent components as defined
in Section 7 and Section 9, and includes fuel elements; removable reflector elements and blocks; permanent side reflector elements
and blocks; core support pedestals and elements; control rod, reserve shutdown, and burnable poison compacts; and neutron shield
material.
1.3 This practice includes test methods that have been selected from existingASTM standards,ASTM standards that have been
modified, and newASTM standards that are specific to the testing of materials listed in 1.2. Comments on individual test methods
for graphite and boronated graphite components are given in Sections 8 and 10, respectively. The test methods are summarized
in Table 1 and Table 2Tables 1 and 2.
1.4
1.4 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
C 559 Test Method for Bulk Density by Physical Measurements of Manufactured Carbon and Graphite Articles
2
C560Test Methods for Chemical Analysis of Graphite 561 Test Method for Ash in a Graphite Sample
2
C561Test Method for Ash in a Graphite Sample
C 577 Test Method for Permeability of Refractories
C 611 Test Method for Electrical Resistivity of Manufactured Carbon and Graphite Articles at Room Temperature
2
C 625Practice for Reporting Irradiation Results on Graphite
C626Methods for Estimating the Thermal Neutron Absorption Cross Section of Nuclear Graphite Practice for Reporting
Irradiation Results on Graphite
C 651 Test Method for Flexural Strength of Manufactured Carbon and Graphite Articles Using Four-Point Loading at Room
Temperature
C 695 Test Method for Compressive Strength of Carbon and Graphite
C 709 Terminology Relating to Manufactured Carbon and Graphite
C 747 Test Method for Moduli of Elasticity and Fundamental Frequencies of Carbon and Graphite Materials by Sonic
Resonance
C 749 Test Method for Tensile Stress-Strain of Carbon and Graphite
2
C816Test Method for Sulfur in Graphite by Combustion-Iodometric Titration Method 769 Test Method for Sonic Velocity in
1
This practice is under the jurisdiction of ASTM Committee D02 on Petroleum Products and Lubricants and is the direct responsibility of Subcommittee D02.F0 on
Manufactured Carbon and Graphite Products.
Current edition approved Dec. 10, 2002. Published April 2003. Originally approved in 1977. Last previous edition approved in 1996 as C781–96.
Current edition approved Sept. 1, 2008. Published October 2008. Originally approved in 1977. Last previous edition approved in 2002 as C 781–02.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
, Vol 05.05.volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
C781–08
TABLE 1 Summary of Test Methods for Graphite Components
NOTE—Designations under preparat
...

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