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ASTM

ASTM D5678-95(2002)

(Test Method)

Standard Test Method for Freeze/Thaw Resistance of Wax Emulsion Floor Polish

Standard Test Method for Freeze/Thaw Resistance of Wax Emulsion Floor Polish

SIGNIFICANCE AND USE
This test method is used to determine the effect of freezing on wax emulsion floor polishes. It may be used to predict the stability of a floor polish in transit or when exposed to freezing, and whether or not the polish is damaged by freezing.
SCOPE
1.1 This test method covers the determination of the stability of wax emulsion floor polishes when these are exposed to repeated cycles of freezing and thawing. Possible degradation of the emulsion is observed and possible reduction of initial gloss is measured.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
14-Mar-1995
ICS
71.100.99 - Other products of the chemical industry
Technical Committee
D21 - Polishes
Drafting Committee
D21.03 - Chemical and Physical Testing
Current Stage
Ref Project

Relations

Replaces
ASTM D5678-95 - Standard Test Method for Freeze/Thaw Resistance of Wax Emulsion Floor Polish
Effective Date
15-Mar-1995
Replaced By
ASTM D5678-95(2008) - Standard Test Method for Freeze/Thaw Resistance of Wax Emulsion Floor Polish
Effective Date
01-Mar-2008

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ASTM D5678-95(2002) - Standard Test Method for Freeze/Thaw Resistance of Wax Emulsion Floor PolishASTM D5678-95(2002) - Standard Test Method for Freeze/Thaw Resistance of Wax Emulsion Floor Polish
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ASTM D5678-95(2002) - Standard Test Method for Freeze/Thaw Resistance of Wax Emulsion Floor Polish
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D5678–95 (Reapproved 2002)
Standard Test Method for
Freeze/Thaw Resistance of Wax Emulsion Floor Polish
This standard is issued under the fixed designation D5678; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 4.4 60-Deg Gloss Meter.
4.5 Polishes, to be tested.
1.1 This test method covers the determination of the stabil-
ity of wax emulsion floor polishes when these are exposed to
5. Procedure
repeated cycles of freezing and thawing. Possible degradation
5.1 Determine the turbidity of each polish, visually or by
of the emulsion is observed and possible reduction of initial
any other suitable method.
gloss is measured.
5.2 Apply one coat of each test polish on a black vinyl
1.2 The values stated in SI units are to be regarded as the
composition tile using pour method (E) (see Test Method
standard. The values given in parentheses are for information
D1436). Allow polish to dry in a vertical position at room
only.
temperature.After polish is dry, wait 1 h, then buff with a soft
1.3 This standard does not purport to address all of the
cotton cloth. Determine the initial gloss in accordance with
safety concerns, if any, associated with its use. It is the
Test Method D1455.
responsibility of the user of this standard to establish appro-
5.3 Place 100 mL of polish in each of three 125 mL (4 oz)
priate safety and health practices and determine the applica-
clear bottles. Place the filled bottles side by side, horizontally,
bility of regulatory limitations prior to use.
in the freezer on a rack. Provide a minimum of 25 mm (1 in.)
2. Referenced Documents between the bottles and the freezer walls and keep the contact
area between the bottles and the rack to a minimum.
2.1 ASTM Standards:
5.4 Allow the samples to remain in the freezer for 16 h, or
D1436 Test Method for Application of Emulsion Floor
a minimum of 8 h after becoming solid.
Polishes to Substrates for Testing Purposes
5.5 Remove all the samples of frozen polish and allow to
D1455 Test Method for 60-Deg Specular Gloss of Emul-
thaw,undisturbed,at18to24°C(65to76°F)foraperiodof24
sion Floor Polish
h.
3. Significance and Use
5.6 Inspect all thawed samples visually. Observe and record
any separation or stratification without disturbing the sample.
3.1 This test method is used to determine the effect of
5.7 Mix one bottle of the thawed polish by inverting it ten
freezing on wax emulsion floor polishes. It may be used to
times. Then apply one coat of polish on a black vinyl
predictthestabilityofafloorpolishintransitorwhenexposed
composition tile using the same procedure as in 5.2. Allow
to freezing, and whether or not the polish is damaged by
polish to dry in a vertical position at room temperature. After
freezing.
polish is dry, wait 1 h, then buff with a soft cotton cloth.
4. Apparatus
Determine the gloss in accordance with Test Method D1455.
Also determine and record while applying the polish if this
4.1 Freezer, adjusted to−7.8 to−6.7°C (18 to 20°F).
agitatedsampleisafreeflowingliquid,orhasseparated,orha
...

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