Standard Test Method for Odor of Volatile Solvents and Diluents

SIGNIFICANCE AND USE
3.1 The comparative odor characteristics can be used, combined with other tests, for product identification and assessing compliance with a specification.  
3.2 The residual odor characteristics can be used to judge the presence of relatively nonvolatile materials that may be associated with manufacture or contamination during distribution. Since volatile solvents and diluents are used in a wide variety of chemical processes and residual materials may affect the efficiency of such processes, this test method provides a comparative test for manufacturing control and assessing compliance with a specification.
SCOPE
1.1 This test method covers a comparative procedure for observing the characteristic and residual odors of volatile organic solvents and diluents to determine their odor acceptability in a solvent system.  
1.2 It is not intended that this test method be employed to determine subtle odor differences between materials or to determine odor intensity.  
1.3 It is recommended that this test method not be employed to determine the residual odor of a liquid if its time for evaporation to dryness at room temperature exceeds 30 min or as agreed upon.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 4.  
1.6 For specific hazard information, see the supplier's Material Safety Data Sheet (MSDS).  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
28-Feb-2023
Current Stage
Ref Project

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ASTM D1296-23 - Standard Test Method for Odor of Volatile Solvents and Diluents
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D1296 − 23
Standard Test Method for
1
Odor of Volatile Solvents and Diluents
This standard is issued under the fixed designation D1296; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 3. Significance and Use
1.1 This test method covers a comparative procedure for 3.1 The comparative odor characteristics can be used, com-
observing the characteristic and residual odors of volatile bined with other tests, for product identification and assessing
organic solvents and diluents to determine their odor accept- compliance with a specification.
ability in a solvent system.
3.2 The residual odor characteristics can be used to judge
1.2 It is not intended that this test method be employed to the presence of relatively nonvolatile materials that may be
determine subtle odor differences between materials or to associated with manufacture or contamination during distribu-
determine odor intensity. tion. Since volatile solvents and diluents are used in a wide
variety of chemical processes and residual materials may affect
1.3 It is recommended that this test method not be employed
the efficiency of such processes, this test method provides a
to determine the residual odor of a liquid if its time for
comparative test for manufacturing control and assessing
evaporation to dryness at room temperature exceeds 30 min or
compliance with a specification.
as agreed upon.
1.4 The values stated in SI units are to be regarded as
4. Hazards
standard. No other units of measurement are included in this
4.1 Many solvents and diluents are hazardous or toxic. Take
standard.
special precautions while determining the odor of all products.
1.5 This standard does not purport to address all of the
Make the tests only as frequently as is necessary for control
safety concerns, if any, associated with its use. It is the
and base the evaluations on short sniffs, inhaling as little vapor
responsibility of the user of this standard to establish appro-
as possible.
priate safety, health, and environmental practices and deter-
4.2 Provide adequate ventilation to maintain solvent or
mine the applicability of regulatory limitations prior to use.
diluent concentration below the personnel exposure limit value
For specific hazard statements, see Section 4.
established for the general work area as given in the MSDS.
1.6 For specific hazard information, see the supplier’s
4.3 Other hazards may also be present. These may be, but
Material Safety Data Sheet (MSDS).
are not limited to, flammable, combustible, corrosive, or
1.7 This international standard was developed in accor-
explosive hazards.
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the
5. Procedures
Development of International Standards, Guides and Recom-
5.1 Characteristic Odor—Dip 25 mm by 75 mm strips of
mendations issued by the World Trade Organization Technical
rapid qualititive paper, free of foreign odor, to a depth of
Barriers to Trade (TBT) Committee.
50 mm into the specimen and the reference standard, each
2. Reference Standards contained in a beaker or other suitable container. Make an
immediate comparison between the odor of the two materials
2.1 Samples of the particular products being tested, having
on the filter papers.
odor characteristics satisfactory to purchaser and manufacturer,
are required.
5.2 Residual Odor—Dip 25 mm by 75 mm strips of a rapid
qualitative paper, free of foreign odor, to a depth of 50 mm into
the specimen under test and the reference sample, each
1
This test method is under the jurisdiction of ASTM Committee D01 on Paint
contained in a beaker or other suitable container. Permit the
and Related Coatings, Materials, and Applications and is the direct responsibility of
Subcommittee D01.35 on Solvents, Plasticizers, and Chemical Intermediates.
papers to dry in air at room temperature and examine them at
Current edition approved March 1, 2023. Published March 2023. Originally
suitable intervals for differences in odor (see 1.3). The evapo-
approved in 1953. Last previous edition approved in 2012 as D1296 – 01 (2012)
ration step may be omitted if only the“ characteristic” odor of
which was withdrawn in January 2021 and reinstated in March 2023. DOI:
10.1520/D1296-23. the material is to be determined.
Copyright © ASTM International, 100 B
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