ASTM D6610-00
(Practice)Standard Practice for Manual Sampling Coal from Surfaces of a Stockpile
Standard Practice for Manual Sampling Coal from Surfaces of a Stockpile
SCOPE
1.1 This practice covers procedures for obtaining a manual gross sample from the surface of coal stockpiles. These procedures are used to provide gross samples for general laboratory analysis and for estimating quality and total moisture. The gross sample is to be crushed and further prepared for analysis in accordance with Method D2013. Mechanical equipment such as auger samplers and core drill rigs are addressed by othe guides (D 4916) or working papers.
1.2 The user is cautioned that samples of this type do not satisfy the minimum requirements for probability sampling and as such cannot be used to draw statistical inferences about the precision, standard error, or bias.
1.3 This sampling method is intended for use only when sampling by more reliable methods that provide a probability sample is not possible.
1.4 The quantities stated in either acceptable SI units or in inch-pound units are regarded separately as standard. The quantities stated in each system may not be exact equivalents; therefore, each system must be used independently of the other, without combining quantities in any way.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation:D6610–00
Standard Practice for
1
Manual Sampling of Coal from Stockpiles
This standard is issued under the fixed designation D 6610; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (ϵ) indicates an editorial change since the last revision or reapproval.
1. Scope falling, or sliding down the sides of a pile or a result of the
peculiarities of a coal handling system used to build the pile.
1.1 This practice covers procedures for obtaining a manual
3.1.2 stockpile, n—material stored or reserved in a stacked
gross sample from the surface of coal stockpiles. These
pile or heap.
procedures are used to provide gross samples for general
laboratory analysis and for estimating quality and total mois-
4. Summary of Practice
ture.The gross sample is to be crushed and further prepared for
4.1 This practice is limited to manual collection of sample
analysis in accordance with Method D 2013.
increments of coal from the surface layer(s) of a coal stockpile
1.2 The user is cautioned that samples of this type do not
for the purpose of acquiring a gross sample.
satisfytheminimumrequirementsforprobabilitysamplingand
as such cannot be used to draw statistical inferences about the
5. Significance and Use
precision, standard error, or bias.
5.1 The guidelines, cautions, and suggested procedures
1.3 This sampling method is intended for use only when
presented here are intended to provide uniform methods for
sampling by more reliable methods that provide a probability
collection of manual samples from the surface layer(s) of coal
sample is not possible.
stored in a stockpile, taking into account the wide variety of
1.4 The quantities stated in either acceptable SI units or in
conditions that may be encountered.
inch-pound units are regarded separately as standard. The
5.2 Theseguidelinesprovideproceduresforcollectinggross
quantities stated in each system may not be exact equivalents;
samples from the exposed surface of coal in a stockpile; these
therefore,eachsystemmustbeusedindependentlyoftheother,
samples then being further processed to provide samples for
without combining quantities in any way.
required laboratory estimations. The use of this practice is
1.5 This standard does not purport to address all of the
conditional upon agreement among all interested parties con-
safety concerns, if any, associated with its use. It is the
cerning all relevant details of sample collection before sam-
responsibility of the user of this standard to establish appro-
pling begins. These include, but are not limited to: lot size;
priate safety and health practices and determine the applica-
number and mass of increments; the size, shape, and manipu-
bility of regulatory limitations prior to use.
lation of the increment collection devices; location of incre-
ment collection site or sites; circumstances under which
2. Referenced Documents
increments are not to be collected or suspended; and safety
2.1 ASTM Standards:
precautions. It is preferable that such agreements be in writing.
2
D 2013 Method of Preparing Coal Samples for Analysis
This practice provides instructions for sampling only the outer
2
D 2234 Practice for Collection of a Gross Sample of Coal
layers of coal contained in a stockpile. The user is cautioned
D 4749 Test Method for Performing SieveAnalysis of Coal
that samples so obtained do not represent material below the
2
and Designating Coal Size
point of penetration.
2
D 4916 Guide for Mechanical Auger Sampling
3
E 105 Practice for Probability Sampling of Materials 6. Procedure
6.1 Lot Size—All interested parties should agree to the size
3. Terminology
of the lot to be represented by one gross sample before
3.1 Definitions:
sampling begins. This practice provides instructions for sam-
3.1.1 particle size segregation, n—the segregation of sized
pling only the outer layers of coal contained in a stockpile.The
particles to specific areas as a result of the particles rolling,
user is cautioned that samples so obtained do not represent
material below the point of penetration.
1
This practice is under the jurisdiction of ASTM Committee D05 on Coal and
6.2 Increments—Before sampling a lot of coal using this
Coke and is the direct responsibility of Subcommittee D05.23 on Sampling .
method, a visual inspection for size distribution and possible
Current edition approved Nov. 10, 2000. Published January 2001.
2 size segregation within the stockpile should be performed.
Annual Book of ASTM Standards, Vol 05.06.
3
Annual Book of ASTM Standards, Vol 14.02. Notes should be made on the sampling log to reflect these
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