Standard Practice for Freezing of Emulsified Asphalts

SIGNIFICANCE AND USE
Certain agencies, who desire to use, store, or transport emulsified asphalt under less than ideal weather conditions, may require that the product remain homogeneous (unbroken) after being subjected to temperatures of −18°C.
SCOPE
1.1 Emulsified asphalt is normally damaged by freezing temperatures, but specially formulated materials are expected to pass this practice.
1.2 This practice does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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Historical
Publication Date
31-Jul-2004
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ASTM D6929-04 - Standard Practice for Freezing of Emulsified Asphalts
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D6929 – 04
Standard Practice for
Freezing of Emulsified Asphalts
This standard is issued under the fixed designation D6929; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
NOTE 1—Emulsified asphalts with viscosity testing requirements of
1. Scope
25°C may be heated and stirred as specified in 3.2, if necessary. In the
1.1 Emulsified asphalt is normally damaged by freezing
event the 3.2 method is used, the sample should be cooled to 25 6 3°C.
temperatures, but specially formulated materials are expected
to pass this practice.
4. Apparatus
1.2 This practice does not purport to address all of the
4.1 Freezer—Capable of maintaining a test temperature of
safety concerns, if any, associated with its use. It is the
-1865°C.
responsibility of the user of this standard to establish appro-
4.2 Metal Container—such as a 500-mL press-top can.
priate safety and health practices and determine the applica-
4.3 Glass Stirring Rod—of optional size.
bility of regulatory limitations prior to use.
5. Procedure
2. Significance and Use
5.1 Place approximately 400 g of the emulsified asphalt in a
2.1 Certain agencies, who desire to use, store, or transport
clean metal container.
emulsified asphalt under less than ideal weather conditions,
5.2 Expose the emulsified asphalt in the closed container to
may require that the product remain homogeneous (unbroken)
an air temperature of −18 6 5°C for 12 to 18 consecutive
after being subjected to temperatures of −18°C.
hours.
5.3 At the expiration of the freezing period, permit the
3. Sample Conditioning
emulsified asphalt to thaw by exposure of the container to
3.1 All emulsified asphalts shall be properly stirred to
ambient temperature.
achieve homogeneity.
5.4 Repeat the freezing and thawing periods until the
3.2 All emulsified asphalts with viscosity testing require-
emulsified asphalt has been subjected to three cycles of
ments of 50°C shall be heated to 50 6 3°C in the original
freezing and thawing.
sample container in a water bath
...

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