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ASTM D1045-14

(Test Method)

Standard Test Methods for Sampling and Testing Plasticizers Used in Plastics

Standard Test Methods for Sampling and Testing Plasticizers Used in Plastics

SIGNIFICANCE AND USE
4.1 These test methods shall be used in establishing and confirming quality control standards for liquid plasticizers used in the compounding of plastics.
SCOPE
1.1 These test methods cover sampling and testing of liquid plasticizers used in compounding of plastics. Acid number, ester content, specific gravity, color, refractive index, and water content are determined.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific hazards information is given in Section 5. Note 1—There is no known ISO equivalent to this standard.

General Information

Status
Historical
Publication Date
28-Feb-2014
ICS
83.040.30 - Auxiliary materials and additives for plastics
Technical Committee
D20 - Plastics
Drafting Committee
D20.15 - Thermoplastic Materials
Current Stage
Ref Project

Relations

Replaces
ASTM D1045-08 - Standard Test Methods for Sampling and Testing Plasticizers Used in Plastics
Effective Date
01-Mar-2014
Replaced By
ASTM D1045-19 - Standard Test Methods for Sampling and Testing Plasticizers Used in Plastics
Effective Date
01-Aug-2019
Referred By
ASTM F942-18(2023)e1 - Standard Guide for Selection of Test Methods for Interlayer Materials for Aerospace Transparent Enclosures
Effective Date
01-Mar-2014

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REDLINE ASTM D1045-14 - Standard Test Methods for Sampling and Testing Plasticizers Used in PlasticsREDLINE ASTM D1045-14 - Standard Test Methods for Sampling and Testing Plasticizers Used in Plastics
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D1045 − 14
Standard Test Methods for
1
Sampling and Testing Plasticizers Used in Plastics
This standard is issued under the fixed designation D1045; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* D3465 Test Method for Purity of Monomeric Plasticizers by
Gas Chromatography
1.1 These test methods cover sampling and testing of liquid
D4052 Test Method for Density, Relative Density, and API
plasticizers used in compounding of plastics. Acid number,
Gravity of Liquids by Digital Density Meter
estercontent,specificgravity,color,refractiveindex,andwater
D5386 Test Method for Color of Liquids Using Tristimulus
content are determined.
Colorimetry
1.2 The values stated in SI units are to be regarded as the
E1 Specification for ASTM Liquid-in-Glass Thermometers
standard. The values given in parentheses are for information
E203 Test Method for Water Using Volumetric Karl Fischer
only.
Titration
1.3 This standard does not purport to address all of the E2251 Specification for Liquid-in-Glass ASTM Thermom-
safety concerns, if any, associated with its use. It is the
eters with Low-Hazard Precision Liquids
responsibility of the user of this standard to establish appro-
3. Terminology
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. Specific hazards
3.1 Definitions—Definitions are in accordance with Termi-
information is given in Section 5.
nology D883 and Terminology D1600, unless otherwise indi-
cated.
NOTE 1—There is no known ISO equivalent to this standard.
2. Referenced Documents
4. Significance and Use
2
2.1 ASTM Standards:
4.1 These test methods shall be used in establishing and
D70 Test Method for Density of Semi-Solid Bituminous
confirmingqualitycontrolstandardsforliquidplasticizersused
Materials (Pycnometer Method)
in the compounding of plastics.
D287 Test Method for API Gravity of Crude Petroleum and
5. Hazards
Petroleum Products (Hydrometer Method)
D792 Test Methods for Density and Specific Gravity (Rela-
5.1 Chemical Hazard of Reagents—It is possible that some
tive Density) of Plastics by Displacement
of the chemicals used in this test method are hazardous.
D883 Terminology Relating to Plastics
Accepted laboratory safety procedures must be followed. See
D1193 Specification for Reagent Water
suppliers’ material safety data sheets for further information.
D1209 Test Method for Color of Clear Liquids (Platinum-
Cobalt Scale)
6. Sampling
D1218 Test Method for Refractive Index and Refractive
6.1 The method of sampling specified in 6.2 or 6.3 shall be
Dispersion of Hydrocarbon Liquids
used, according to the special conditions that exist.
D1544 Test Method for Color of Transparent Liquids (Gard-
6.2 From Loaded Tank Car or Other Large Vessel—The
ner Color Scale)
1
composite sample taken shall be not less than 2 L( ⁄2 gal). It is
D1600 Terminology forAbbreviatedTerms Relating to Plas-
important that the composite sample consists of small samples
tics
of not more than 1 L (1 qt) each, taken from near the top and
bottom by means of a metal or glass container with removable
1
These methods are under the jurisdiction ofASTM Committee D20 on Plastics
stopper or top. This device, attached to a suitable pole, shall be
and are the direct responsibility of Subcommittee D20.15 on Thermoplastic
Materials (Section D20.15.07 on Vinyl Chloride Polymers).
lowered to the desired depth, when the stopper or top shall be
Current edition approved March 1, 2014. Published March 2014. Originally
removed and the container allowed to fill. A bomb sampler
approved in 1949. Last previous edition approved in 2008 as D1045 - 08. DOI:
attached to a chain is convenient to use; adjust the opening so
10.1520/D1045-14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or that the bomb will fill on the way down.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
6.3 From Barrels and Drums—At least 5 % of the packages
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. in any shipment shall be represented in the sample. It is
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D1045 − 14
permissible for the purchaser to increase the percentage of 10.2 Addafewdropsofbromthymolblueindicatorsolution
packages to be sampled at his discretion; in the case of and titrate with 0.01 N NaOH or KOH solution. If
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D1045 − 08 D1045 − 14
Standard Test Methods for
1
Sampling and Testing Plasticizers Used in Plastics
This standard is issued under the fixed designation D1045; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
1.1 These test methods cover sampling and testing of liquid plasticizers used in compounding of plastics. Acid number, ester
content, specific gravity, color, refractive index, and water content are determined.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. Specific hazards information is given in Section 5.
NOTE 1—There is no similar or equivalent ISO known ISO equivalent to this standard.
2. Referenced Documents
2
2.1 ASTM Standards:
D70 Test Method for Density of Semi-Solid Bituminous Materials (Pycnometer Method)
D287 Test Method for API Gravity of Crude Petroleum and Petroleum Products (Hydrometer Method)
D792 Test Methods for Density and Specific Gravity (Relative Density) of Plastics by Displacement
D883 Terminology Relating to Plastics
D1193 Specification for Reagent Water
D1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D1218 Test Method for Refractive Index and Refractive Dispersion of Hydrocarbon Liquids
D1544 Test Method for Color of Transparent Liquids (Gardner Color Scale)
D1600 Terminology for Abbreviated Terms Relating to Plastics
D3465 Test Method for Purity of Monomeric Plasticizers by Gas Chromatography
D4052 Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
D5386 Test Method for Color of Liquids Using Tristimulus Colorimetry
E1 Specification for ASTM Liquid-in-Glass Thermometers
E203 Test Method for Water Using Volumetric Karl Fischer Titration
E2251 Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
3. Terminology
3.1 Definitions—Definitions are in accordance with Terminology D883 and Terminology D1600, unless otherwise indicated.
4. Significance and Use
4.1 These test methods shall be used in establishing and confirming quality control standards for liquid plasticizers used in the
compounding of plastics.
5. Hazards
5.1 Chemical Hazard of Reagents—It is possible that some of the chemicals used in this test method are hazardous. Accepted
laboratory safety procedures must be followed. See suppliers’ material safety data sheets for further information.
1
These methods are under the jurisdiction of ASTM Committee D20 on Plastics and are the direct responsibility of Subcommittee D20.15 on Thermoplastic Materials
(Section D20.15.11 on Plasticizers).D20.15.07 on Vinyl Chloride Polymers).
Current edition approved Aug. 1, 2008March 1, 2014. Published September 2008March 2014. Originally approved in 1949. Last previous edition approved in 20012008
as D1045 - 95D1045 - 08.(2001). DOI: 10.1520/D1045-08.10.1520/D1045-14.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D1045 − 14
6. Sampling
6.1 The method of sampling specified in 6.2 or 6.3 shall be used, according to the special conditions that exist.
1
6.2 From Loaded Tank Car or Other Large Vessel—The composite sample taken shall be not less than 2 L ( ⁄2 gal). It is
important that the composite sample consists of small samples of not more than 1 L (1 qt) each, taken from near the top and bottom
by means of a metal or glass container with removable stopper or top. This device, attached to a suitable pole, shall be lowered
to the desired depth, when the stopper or top shall be removed and the container allowed to fill. A bomb sampler attached to a chain
is con
...

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