ASTM D1045-19
(Test Method)Standard Test Methods for Sampling and Testing Plasticizers Used in Plastics
Standard Test Methods for Sampling and Testing Plasticizers Used in Plastics
SIGNIFICANCE AND USE
4.1 These test methods shall be used in establishing and confirming quality control standards for liquid plasticizers used in the compounding of plastics.
SCOPE
1.1 These test methods cover sampling and testing of liquid plasticizers used in compounding of plastics. Acid number, ester content, specific gravity, color, refractive index, and water content are determined.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards information is given in Section 5.
Note 1: There is no known ISO equivalent to this standard.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
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Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D1045 − 19
Standard Test Methods for
1
Sampling and Testing Plasticizers Used in Plastics
This standard is issued under the fixed designation D1045; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* D1209 Test Method for Color of Clear Liquids (Platinum-
Cobalt Scale)
1.1 These test methods cover sampling and testing of liquid
D1218 Test Method for Refractive Index and Refractive
plasticizers used in compounding of plastics. Acid number,
Dispersion of Hydrocarbon Liquids
estercontent,specificgravity,color,refractiveindex,andwater
D1544 Test Method for Color of Transparent Liquids (Gard-
content are determined.
ner Color Scale)
1.2 The values stated in SI units are to be regarded as the
D1600 Terminology forAbbreviatedTerms Relating to Plas-
standard. The values given in parentheses are for information
tics
only.
D3465 Test Method for Purity of Monomeric Plasticizers by
1.3 This standard does not purport to address all of the Gas Chromatography
safety concerns, if any, associated with its use. It is the
D4052 Test Method for Density, Relative Density, and API
responsibility of the user of this standard to establish appro- Gravity of Liquids by Digital Density Meter
priate safety, health, and environmental practices and deter-
D5386 Test Method for Color of Liquids Using Tristimulus
mine the applicability of regulatory limitations prior to use. Colorimetry
Specific hazards information is given in Section 5.
E1 Specification for ASTM Liquid-in-Glass Thermometers
E203 Test Method for Water Using Volumetric Karl Fischer
NOTE 1—There is no known ISO equivalent to this standard.
Titration
1.4 This international standard was developed in accor-
E2251 Specification for Liquid-in-Glass ASTM Thermom-
dance with internationally recognized principles on standard-
eters with Low-Hazard Precision Liquids
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom-
3. Terminology
mendations issued by the World Trade Organization Technical
3.1 Definitions—Definitions are in accordance with Termi-
Barriers to Trade (TBT) Committee.
nology D883 and Terminology D1600, unless otherwise indi-
cated.
2. Referenced Documents
2
2.1 ASTM Standards:
4. Significance and Use
D70 Test Method for Density of Semi-Solid Asphalt Binder
4.1 These test methods shall be used in establishing and
(Pycnometer Method)
confirmingqualitycontrolstandardsforliquidplasticizersused
D287 Test Method for API Gravity of Crude Petroleum and
in the compounding of plastics.
Petroleum Products (Hydrometer Method)
D792 Test Methods for Density and Specific Gravity (Rela-
5. Hazards
tive Density) of Plastics by Displacement
5.1 Chemical Hazard of Reagents—It is possible that some
D883 Terminology Relating to Plastics
of the chemicals used in this test method are hazardous.
D1193 Specification for Reagent Water
Accepted laboratory safety procedures must be followed. See
suppliers’ material safety data sheets for further information.
5.2 Hazards with Mercury Thermometers—Hazards associ-
1
These methods are under the jurisdiction ofASTM Committee D20 on Plastics
ated with mercury thermometers are discussed in 8.2.
and are the direct responsibility of Subcommittee D20.15 on Thermoplastic
Materials (Section D20.15.07 on Vinyl Chloride Polymers).
Current edition approved Aug. 1, 2019. Published August 2019. Originally 6. Sampling
approved in 1949. Last previous edition approved in 2014 as D1045 - 14. DOI:
6.1 The method of sampling specified in 6.2 or 6.3 shall be
10.1520/D1045-19.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or used, according to the special conditions that exist.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
6.2 From Loaded Tank Car or Other Large Vessel—The
Standards volume information, refer to the standard’s Document Summary page on
1
the ASTM website. composite sample taken shall be not less than 2 L( ⁄2 gal). It is
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D1045 − 19
important that the composite sample consists of small samples should be aware that selling mercury and/or mercury-
of not more than 1 L (1 qt) each, taken from near the top and containing products in your
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D1045 − 14 D1045 − 19
Standard Test Methods for
1
Sampling and Testing Plasticizers Used in Plastics
This standard is issued under the fixed designation D1045; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
1.1 These test methods cover sampling and testing of liquid plasticizers used in compounding of plastics. Acid number, ester
content, specific gravity, color, refractive index, and water content are determined.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use. Specific hazards information is given in Section 5.
NOTE 1—There is no known ISO equivalent to this standard.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D70 Test Method for Density of Semi-Solid Asphalt Binder (Pycnometer Method)
D287 Test Method for API Gravity of Crude Petroleum and Petroleum Products (Hydrometer Method)
D792 Test Methods for Density and Specific Gravity (Relative Density) of Plastics by Displacement
D883 Terminology Relating to Plastics
D1193 Specification for Reagent Water
D1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D1218 Test Method for Refractive Index and Refractive Dispersion of Hydrocarbon Liquids
D1544 Test Method for Color of Transparent Liquids (Gardner Color Scale)
D1600 Terminology for Abbreviated Terms Relating to Plastics
D3465 Test Method for Purity of Monomeric Plasticizers by Gas Chromatography
D4052 Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
D5386 Test Method for Color of Liquids Using Tristimulus Colorimetry
E1 Specification for ASTM Liquid-in-Glass Thermometers
E203 Test Method for Water Using Volumetric Karl Fischer Titration
E2251 Specification for Liquid-in-Glass ASTM Thermometers with Low-Hazard Precision Liquids
3. Terminology
3.1 Definitions—Definitions are in accordance with Terminology D883 and Terminology D1600, unless otherwise indicated.
4. Significance and Use
4.1 These test methods shall be used in establishing and confirming quality control standards for liquid plasticizers used in the
compounding of plastics.
1
These methods are under the jurisdiction of ASTM Committee D20 on Plastics and are the direct responsibility of Subcommittee D20.15 on Thermoplastic Materials
(Section D20.15.07 on Vinyl Chloride Polymers).
Current edition approved March 1, 2014Aug. 1, 2019. Published March 2014August 2019. Originally approved in 1949. Last previous edition approved in 20082014 as
D1045 - 08.D1045 - 14. DOI: 10.1520/D1045-14.10.1520/D1045-19.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D1045 − 19
5. Hazards
5.1 Chemical Hazard of Reagents—It is possible that some of the chemicals used in this test method are hazardous. Accepted
laboratory safety procedures must be followed. See suppliers’ material safety data sheets for further information.
5.2 Hazards with Mercury Thermometers—Hazards associated with mercury thermometers are discussed in 8.2.
6. Sampling
6.1 The method of sampling specified in 6.2 or 6.3 shall be used, according to the special conditions that exist.
1
6.2 From Loaded Tank Car or Other Large Vessel—The composite sample taken shall be not less than 2 L ( ⁄2 gal). It is
important
...
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