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ASTM D6271-04

(Test Method)

Standard Test Method for Estimating Contribution of Environmental Tobacco Smoke to Respirable Suspended Particles Based on Solanesol

Standard Test Method for Estimating Contribution of Environmental Tobacco Smoke to Respirable Suspended Particles Based on Solanesol

SCOPE
1.1 This test method covers the sampling/analysis of respirable suspended particles (RSP) and the estimation of the RSP fraction attributable to environmental tobacco smoke (ETS). The test method is based on collection of total RSP on a membrane filter, extraction of the filter in methanol, and determination of solanesol, a C45 isoprenoid alcohol, by high performance liquid chromatography (HPLC) with ultraviolet (UV) detection.
1.2 This test method is compatible with the determinations of gravimetric RSP, ultraviolet particulate matter (UVPM), and fluorescent particulate matter (FPM) (see Test Methods D 5955), but does not require them. UVPM and FPM, which are based on the ultraviolet absorbance and fluorescence of the filter extract, are also used to estimate the contribution of ETS to RSP.
1.3 The sampling components consist of a 1.0-m pore size polytetrafluoroethylene (PTFE) membrane filter in a filter cassette connected on the inlet end to a particle size separating device and, on the outlet end, to a sampling pump. This test method is applicable to personal and area sampling.
1.4 This test method is limited in sample duration only by the capacity of the membrane filter. The test method has been evaluated up to 24-h sample duration; a minimum sample duration of 1 h is recommended.
1.5 Limits of detection (LOD) for this test method at a sampling rate of 2 L/min are 0.042 g/m3 for 1-h sample duration and 0.005 g/m3 for 8-h sample duration.
1.6 The values stated in SI units are to be regarded as standard.
This standard does not purport to address all the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary information is given in .

General Information

Status
Historical
Publication Date
31-Mar-2004
ICS
13.040.20 - Ambient atmospheres
Technical Committee
D22 - Air Quality
Drafting Committee
D22.05 - Indoor Air
Current Stage
Ref Project

Relations

Replaces
ASTM D6271-98 - Standard Test Method for Estimating Contribution of Environmental Tobacco Smoke to Respirable Suspended Particles Based on Solanesol
Effective Date
01-Apr-2004
Replaced By
ASTM D6271-10 - Standard Test Method for Estimating Contribution of Environmental Tobacco Smoke to Respirable Suspended Particles Based on Solanesol
Effective Date
01-Apr-2010
Referred By
ASTM D7297-21 - Standard Practice for Evaluating Residential Indoor Air Quality Concerns
Effective Date
01-Apr-2004

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ASTM D6271-04 - Standard Test Method for Estimating Contribution of Environmental Tobacco Smoke to Respirable Suspended Particles Based on SolanesolASTM D6271-04 - Standard Test Method for Estimating Contribution of Environmental Tobacco Smoke to Respirable Suspended Particles Based on Solanesol
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ASTM D6271-04 - Standard Test Method for Estimating Contribution of Environmental Tobacco Smoke to Respirable Suspended Particles Based on Solanesol
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information.
Designation:D6271–04
Standard Test Method for
Estimating Contribution of Environmental Tobacco Smoke
1
to Respirable Suspended Particles Based on Solanesol
This standard is issued under the fixed designation D6271; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 This test method covers the sampling/analysis of respi-
rable suspended particles (RSP) and the estimation of the RSP D1356 Terminology Relating to Sampling and Analysis of
fraction attributable to environmental tobacco smoke (ETS). Atmospheres
The test method is based on collection of total RSP on a D1357 Practice for Planning the Sampling of the Ambient
membrane filter, extraction of the filter in methanol, and Atmosphere
determination of solanesol, a C isoprenoid alcohol, by high D3631 Test Methods for Measuring Surface Atmospheric
45
performance liquid chromatography (HPLC) with ultraviolet Pressure
(UV) detection. D5337 Practice for Flow Rate Calibration of Personal
1.2 This test method is compatible with the determinations Sampling Pumps
of gravimetric RSP, ultraviolet particulate matter (UVPM), and D5955 Test Methods for Estimating Contribution of Envi-
fluorescent particulate matter (FPM) (see Test Methods ronmental Tobacco Smoke to Respirable Suspended Par-
D5955), but does not require them. UVPM and FPM, which ticles Based on UVPM and FPM
are based on the ultraviolet absorbance and fluorescence of the
3. Terminology
filter extract, are also used to estimate the contribution of ETS
to RSP. 3.1 Definitions: For definitions of terms used in this test
method, refer to Terminology D1356.
1.3 The sampling components consist of a 1.0-µm pore size
polytetrafluoroethylene (PTFE) membrane filter in a filter 3.2 Definitions of Terms Specific to This Standard:
3.2.1 environmental tobacco smoke (ETS)—an aged, dilute
cassette connected on the inlet end to a particle size separating
device and, on the outlet end, to a sampling pump. This test composite of exhaled tobacco smoke (exhaled mainstream
smoke) and smoke from tobacco products (sidestream smoke).
method is applicable to personal and area sampling.
3.2.2 respirable suspended particles (RSP)—particles
1.4 This test method is limited in sample duration only by
the capacity of the membrane filter. The test method has been which can be deposited in the gas-exchange region of the lung
and are defined as particles that pass through a sampler having
evaluated up to 24-h sample duration; a minimum sample
3
duration of1his recommended. a 4.0-µm median cutpoint (1) .
3.2.3 solanesol particulate matter (Sol-PM)—a tobacco-
1.5 Limits of detection (LOD) for this test method at a
3
sampling rate of 2 L/min are 0.042 µg/m for 1-h sample selective marker for the contribution of ETS particulate matter
3
to RSP.
duration and 0.005 µg/m for 8-h sample duration.
1.6 The values stated in SI units are to be regarded as
4. Summary of Test Method
standard.
4.1 A known volume of air is drawn through an inertial
1.7 This standard does not purport to address all the safety
impactor or cyclone assembly separating at 4.0 µm to separate
concerns, if any, associated with its use. It is the responsibility
respirable suspended particles (RSP) from total suspended
of the user of this standard to establish appropriate safety and
particulate matter and then through a filter assembly. Solanesol
health practices and determine the applicability of regulatory
is collected as a component of RSPon a PTFE membrane filter
limitations prior to use. Specific precautionary information is
contained within the filter assembly.
given in 13.6.
1 2
This test method is under the jurisdiction of ASTM Committee D22 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Sampling and Analysis of Atmospheres and is the direct responsibility of Subcom- contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
mittee D22.05 on Indoor Air. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved April 1, 2004. Published May 2004. Originally the ASTM website.
3
approved in 1998. Last previous edition approved in 1998 as D6271 - 98. DOI: The boldface numbers in parentheses refer to a list of references at the end of
10.1520/D6271-04. this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D6271–04
4.2 Solanesol is extracted from the filter with methanol in a solanesol is a better indicator of t
...

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5.3 It is anticipated that the main users of this practice will be manufacturers, developers, and distributors of outdoor air quality sensors, air quality agenc...
SCOPE
1.1 This practice establishes standardized tests for the performance evaluation of sensor-based continuous instruments for ambient outdoor air quality measurements. It describes both laboratory and field tests that provide information on candidate sensor repeatability, sensitivity, linearity, cross-interferences, drift, and comparability against reference instruments.  
1.2 This practice does not apply to sensors or instruments that remotely measure atmospheric pollutants using open path, lidar, or imaging technology.  
1.3 The evaluation procedures contained in this practice are for sensors that alone or in combination measure outdoor criteria pollutants in ambient air: particulate matter (PM2.5 and PM10), sulfur dioxide (SO2), ozone (O3), carbon monoxide (CO), or nitrogen dioxide (NO2) at concentrations that are relevant to public health.  
1.4 Testing is to be performed by a competent entity able to demonstrate that it operates in conformity with internationally accepted test laboratory quality standards such as ISO/IEC 17025.  
1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D2914-15(2022)(Test Method)
Standard Test Methods for Sulfur Dioxide Content of the Atmosphere (West-Gaeke Method)

SIGNIFICANCE AND USE
5.1 Sulfur dioxide is a major air pollutant, commonly formed by the combustion of sulfur-bearing fuels. The Environmental Protection Agency (EPA) has set primary and secondary air quality standards (7) that are designed to protect the public health and welfare.  
5.2 The Occupational Safety and Health Administration (OSHA) has promulgated exposure limits for sulfur dioxide in workplace atmospheres (8).  
5.3 These methods have been found satisfactory for measuring sulfur dioxide in ambient and workplace atmospheres over the ranges pertinent in 5.1 and 5.2.  
5.4 Method A has been designed to correspond to the EPA-Designated Reference Method (7) for the determination of sulfur dioxide.
SCOPE
1.1 These test methods cover the bubbler collection and colorimetric determination of sulfur dioxide (SO2) in the ambient or workplace atmosphere.  
1.2 These test methods are applicable for determining SO2 over the range from approximately 25 μg/m3 (0.01 ppm(v)) to 1000 μg/m3 (0.4 ppm(v)), corresponding to a solution concentration of 0.03 μg SO2/mL to 1.3 μg SO2/mL. Beer's law is followed through the working analytical range from 0.02 μg SO2/mL to 1.4 μg SO2/mL.  
1.3 The lower limit of detection is 0.075 μg SO2/mL (1),2 representing an air concentration of 25 μg SO2/m3 (0.01 ppm(v)) in a 30-min sample, or 13 μg SO2/m3 (0.005 ppm(v)) in a 24-h sample.  
1.4 These test methods incorporate sampling for periods between 30 min and 24 h.  
1.5 These test methods describe the determination of the collected (impinged) samples. A Method A and a Method B are described.  
1.6 Method A is preferred over Method B, as it gives the higher sensitivity, but it has a higher blank. Manual Method B is pH-dependent, but is more suitable with spectrometers having a spectral band width greater than 20 nm.
Note 1: These test methods are applicable at concentrations below 25 μg/m3 by sampling larger volumes of air if the absorption efficiency of the particular system is first determined, as described in Annex A4.
Note 2: Concentrations higher than 1000 μg/m3 can be determined by using smaller gas volumes, larger collection volumes, or by suitable dilution of the collected sample with absorbing solution prior to analysis.  
1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.8 Warning—Mercury has been designated by many regulatory agencies as a hazardous material that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Safety Data Sheet (SDS) for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.  
1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see 8.3.1, Section 9, and A3.1.3.  
1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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