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ASTM D801-02

(Test Method)

Standard Test Methods for Sampling and Testing Dipentene

Standard Test Methods for Sampling and Testing Dipentene

SIGNIFICANCE AND USE
The testing procedures described in these test methods have been in use for many years and emphasize the physical properties rather than the chemical composition of dipentene. These procedures were sufficient when dipentene was used primarily as a solvent. Currently, however, dipentene finds application as a chemical raw material and a knowledge of its chemical composition is therefore important. Test Methods D 6387 describe a capillary gas chromatography method which is suitable for determining both the major and minor components found in dipentene.
SCOPE
1.1 These test methods cover procedures for sampling and testing dipentene and related terpene solvents, consisting chiefly of monocyclic terpene hydrocarbons distilling above the range for turpentine.
1.2 The procedures given in these test methods appear in the following order:SectionSampling4Detection and Removal of Separated Water5Appearance6Color7Odor8Specific Gravity9Refractive Index10Composition11Flash Point12Moisture13
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-May-2002
ICS
87.060.30 - Solvents
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.34 - Pine Chemicals and Hydrocarbon Resins
Current Stage
Ref Project

Relations

Replaces
ASTM D801-97 - Standard Test Methods for Sampling and Testing Dipentene
Effective Date
10-May-2002
Replaced By
ASTM D801-02(2009) - Standard Test Methods for Sampling and Testing Dipentene
Effective Date
01-Jun-2009
Referred By
ASTM D6387-19 - Standard Test Methods for Composition of Turpentine and Related Terpene Products by Capillary Gas Chromatography
Effective Date
10-May-2002
Referred By
ASTM E1405-98(2022) - Standard Specification for Laboratory Glass Distillation Flasks
Effective Date
10-May-2002

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ASTM D801-02 - Standard Test Methods for Sampling and Testing DipenteneASTM D801-02 - Standard Test Methods for Sampling and Testing Dipentene
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ASTM D801-02 - Standard Test Methods for Sampling and Testing Dipentene
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D801–02
Standard Test Methods for
1
Sampling and Testing Dipentene
This standard is issued under the fixed designation D 801; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
4
1. Scope E 300 Practice for Sampling Industrial Chemicals
1.1 These test methods cover procedures for sampling and
3. Significance and Use
testing dipentene and related terpene solvents, consisting
3.1 The testing procedures described in these test methods
chiefly of monocyclic terpene hydrocarbons distilling above
have been in use for many years and emphasize the physical
the range for turpentine.
properties rather than the chemical composition of dipentene.
1.2 The procedures given in these test methods appear in the
These procedures were sufficient when dipentene was used
following order:
primarily as a solvent. Currently, however, dipentene finds
Section
application as a chemical raw material and a knowledge of its
Sampling 4
Detection and Removal of Separated Water 5
chemical composition is therefore important. Test Methods
Appearance 6
D 6387 describe a capillary gas chromatography method which
Color 7
is suitable for determining both the major and minor compo-
Odor 8
Specific Gravity 9
nents found in dipentene.
Refractive Index 10
Composition 11
4. Sampling
Flash Point 12
Moisture 13
4.1 Sample the material in accordance with the procedure
described in Guide D 268 and Practice E 300. If a sample from
1.3 This standard does not purport to address all of the
close to the bottom of a tank shows a decided difference in
safety concerns, if any, associated with its use. It is the
colororappearancefromsamplestakenatotherdepths,takean
responsibility of the user of this standard to establish appro-
extra bottom sample and examine it separately from the
priate safety and health practices and determine the applica-
composite sample. In such case the composite sample shall not
bility of regulatory limitations prior to use.
include any portion of such bottom sample.
2. Referenced Documents
5. Detection and Removal of Separated Water
2.1 ASTM Standards:
5.1 Draw a portion of the dipentene by means of a glass or
D 268 Guide for Sampling and Testing Volatile Solvents
5
metal container with a removable stopper or top, or with a
and Chemical Intermediates for Use in Paint and Related
2
thief, from the lowest part of the container, or by opening the
Coatings and Materials
3 bottom valve of the level tank car. If water is found to be
D 890 Test Method for Water in Liquid Naval Stores
present, draw it all out, record the quantity, and deduct it from
D 1209 Test Method for Color of Clear Liquids (Platinum-
2 the total volume of liquid delivered.
Cobalt Scale)
D 6166 Test Method for Color of Naval Stores and Related
6. Appearance
3
Products (Instrumental Determination of Gardner Color)
6.1 Examine a portion of the sample after agitation to
D 6387 Test Methods for Composition of Turpentine and
determine its clarity and freedom from foreign matter and
Related Terpene Products by Capillary Gas Chromatogra-
3 separated water.
phy
7. Color
1
7.1 Compare the color of the sample in any suitable or
These test methods are under the jurisdiction of ASTM Committee D01 on
Paint and Related Coatings, Materials, and Applications and are the direct
designated apparatus with the accepted or specific color
responsibility of Subcommittee D01.34 on Naval Stores.
Current edition approved May 10, 2002. Published July 2002. Originally
4
published as D 801 – 44. Last previous edition D 801 – 97. Annual Book of ASTM Standards, Vol 15.05.
2 5
Annual Book of ASTM Standards, Vol 06.04. Detailed description of equipment suitable for such sampling is given in
3
Annual Book of ASTM Standards, Vol 06.03. Practice E 300.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D801
standard.Accepted color standards are the Gardner color scale 12. Flash Point
found in Test Method D 6166 and the platinum-cobalt scale
12.1 Determine the flash point by any acceptable means
found in Test Method D 1209.
agreed upon between the producer and the customer.
8. Odor
13. Moisture
8.1 Compare the odor of the sample with an agreed upon
water-free reference sample kept in the dark in a completely
13.1 The recommended method for the determination of
filled well-stoppered bottle. In the absence of such a reference
dissolved water uses the Karl Fischer reagent and is described
sample, compare with samples of known purity similarly
in Test Method D 890. This method is
...

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1.1 This test method is for the determination of acetone, methyl acetate, or parachlorobenzotrifluoride (PCBTF), or combination of any of the three, in paints and coatings, by solid phase microextraction (SPME) headspace sampling, and subsequent injection into a gas chromatograph. It has been evaluated for cellulose nitrate, acrylic, and urethane solvent-borne systems. The established working range of this test method is: acetone, 28 to 90 %; methyl acetate, 12 to 22 %; parachlorobenzotrifluoride, 10 to 17 %. There is no reason to believe that it will not work outside these ranges. A minor modification of this test method would make it suitable for the analysis of the same analytes in water-borne coatings (see Note 1).
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1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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