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ASTM D4645-04e1

(Test Method)

Standard Test Method for Determination of the In-Situ Stress in Rock Using the Hydraulic Fracturing Method

Standard Test Method for Determination of the In-Situ Stress in Rock Using the Hydraulic Fracturing Method

SCOPE
1.1 This test method covers the determination of the in-situ state of stress in rock by hydraulic fracturing. Note 1Hydraulic fracturing for stress determination is also referred to as hydrofracturing, and sometimes as minifracing. Hydraulic fracturing and hydrofracturing may also refer to fracturing of the rock by fluid pressure for the purpose of altering rock properties, such as permeability and porosity.
1.2 Hydraulic fracturing is the widely accepted field method available for in situ stress measurements at depths greater than 50 m. It can be used in drill holes of any diameter.
1.3 Hydraulic fracturing can also be used in short holes for which other stress measuring methods, such as overcoring, are also available. The advantage of hydraulic fracturing is that it yields stresses averaged over a few square metres (the size of the induced hydraulic fracture) rather than over grain size areas, as in the case of overcoring techniques.
1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D 6026.
1.4.1 The method used to specifiy how data are collected, calculated, or recorded in this standard is not directly related to the accuracy to which the data can be applied in design or other uses, or both. How one applies the results obtained using this standard is beyond its scope.
1.5 The values stated in SI units are to be regarded as the standard.
1.6 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Dec-2003
ICS
93.020 - Earthworks. Excavations. Foundation construction. Underground works
Technical Committee
D18 - Soil and Rock
Drafting Committee
D18.12 - Rock Mechanics
Current Stage
Ref Project

Relations

Replaces
ASTM D4645-04 - Standard Test Method for Determination of the In-Situ Stress in Rock Using the Hydraulic Fracturing Method
Effective Date
01-Jan-2004
Replaced By
ASTM D4645-08 - Standard Test Method for Determination of In-Situ Stress in Rock Using Hydraulic Fracturing Method (Withdrawn 2017)
Effective Date
01-Jul-2008
Referred By
ASTM D420-18 - Standard Guide for Site Characterization for Engineering Design and Construction Purposes
Effective Date
01-Jan-2004
Referred By
ASTM D8359-21 - Standard Test Method for Determining the In Situ Rock Deformation Modulus and Other Associated Rock Properties Using a Flexible Volumetric Dilatometer
Effective Date
01-Jan-2004

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ASTM D4645-04e1 - Standard Test Method for Determination of the In-Situ Stress in Rock Using the Hydraulic Fracturing MethodASTM D4645-04e1 - Standard Test Method for Determination of the In-Situ Stress in Rock Using the Hydraulic Fracturing Method
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ASTM D4645-04e1 - Standard Test Method for Determination of the In-Situ Stress in Rock Using the Hydraulic Fracturing Method
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
e1
Designation: D 4645 – 04
Standard Test Method for
Determination of the In-Situ Stress in Rock Using the
1
Hydraulic Fracturing Method
This standard is issued under the fixed designation D4645; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1
e NOTE—Figure 2 was corrected editorially in September 2004.
1. Scope* 2. Referenced Documents
2
1.1 This test method covers the determination of the in-situ 2.1 ASTM Standards:
state of stress in rock by hydraulic fracturing. D653 Terminology Relating to Soil, Rock and Contained
Fluids
NOTE 1—Hydraulic fracturing for stress determination is also referred
D2113 Practice for Diamond Core Drilling for Site Inves-
to as hydrofracturing, and sometimes as minifracing. Hydraulic fracturing
tigation
and hydrofracturing may also refer to fracturing of the rock by fluid
pressure for the purpose of altering rock properties, such as permeability D3740 Practice for Minimum Requirements for Agencies
and porosity.
Engaged in theTesting and/or Inspection of Soil and Rock
as Used in Engineering Design and Construction
1.2 Hydraulicfracturingisthewidelyacceptedfieldmethod
D5079 Practices for Preserving and Transporting Rock
available for in situ stress measurements at depths greater than
Core Sample
50 m. It can be used in drill holes of any diameter.
D6026 Practice for Using Significant Digits in Geotechni-
1.3 Hydraulic fracturing can also be used in short holes for
cal Data
which other stress measuring methods, such as overcoring, are
also available. The advantage of hydraulic fracturing is that it
3. Terminology
yields stresses averaged over a few square metres (the size of
3.1 For terminology used in this test method, refer to
the induced hydraulic fracture) rather than over grain size
Terminology D653.
areas, as in the case of overcoring techniques.
3.2 Definitions of Terms Specific to This Standard:
1.4 All observed and calculated values shall conform to the
3.2.1 breakdown pressure—the pressure required to induce
guidelines for significant digits and rounding established in
a hydraulic fracture in a previously intact test interval.
Practice D6026.
3.2.2 in-situ stress—rock stress measured in situ (as op-
1.4.1 The method used to specifiy how data are collected,
posed to by remote sensing).
calculated,orrecordedinthisstandardisnotdirectlyrelatedto
3.2.3 secondary breakdown (or fracture reopening, or re-
theaccuracytowhichthedatacanbeappliedindesignorother
frac) pressure—the pressure required to reopen a closed,
uses, or both. How one applies the results obtained using this
previouslyinducedhydrofractureafterthetestintervalpressure
standard is beyond its scope.
has been allowed to return to its initial condition.
1.5 The values stated in SI units are to be regarded as the
3.2.4 shut-in pressure (or ISIP (instantaneous shut-in
standard.
pressure))—the pressure reached when the induced hydrofrac-
1.6 This standard does not purport to address all of the
ture closes back after pumping is stopped.
safety problems, if any, associated with its use. It is the
3.2.5 vertical and horizontal principal stresses—the three
responsibility of the user of this standard to establish appro-
principalstressesinsituaregenerallyassumedtoactoneinthe
priate safety and health practices and determine the applica-
vertical direction and the other two in the horizontal plane.
bility of regulatory limitations prior to use.
1 2
ThistestmethodisunderthejurisdictionofASTMCommitteeD18onSoiland For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Rock and is the direct responsibility of Subcommittee D18.12 on Rock Mechanics. contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Current edition approved Jan. 1, 2004. Published February 2004. Originally Standards volume information, refer to the standard’s Document Summary page on
approved in 1987. Last previous edition approved in 1997 as D4645–87(1997). the ASTM website.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
e1
D4645–04
4. Summary of Test Method 5.2.2 Vertical boreholes are assumed to be substantially
paralleltooneofthein-situprincipalstresses,sinceithasbeen
4.1 Asectionoftheboreholeisisolatedbypressurizingtwo
established from many geological observations and stress
inflatable rubber packers. The fluid pressure in the sealed-off
measurements by other methods that in most cases one of the
interval between the two packers i
...

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SCOPE
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ASTM D5102/D5102M-22(Test Method)
Standard Test Methods for Unconfined Compressive Strength of Compacted Soil-Lime Mixtures

SIGNIFICANCE AND USE
5.1 Compression testing of soil-lime specimens is performed to determine unconfined compressive strength of the cured soil-lime-water mixture to determine the suitability of the mixture for uses such as in pavement bases and subbases, stabilized subgrades, and structural fills.  
5.2 Compressive strength data are used in soil-lime mix design procedures: (a) to determine if a soil will achieve a significant strength increase with the addition of lime; (b) to group soil-lime mixtures into strength classes; (c) to study the effects of variables such as lime percentage, unit weight, water content, curing time, curing temperature, etc.; and (d) to estimate other engineering properties of soil-lime mixtures.  
5.3 Lime is generally classified as calcitic or dolomitic. Usually in soil stabilization, high-calcium lime [CaO] or dolomitic lime [CaO + MgO] are used. The lime is transformed from oxide to hydroxide form [[Ca(OH)2 or [Ca(OH)2 + Mg(OH)2]] by the addition of water in the soil, a slurry tank, or at a manufacturing facility. Lime may increase the strength of cohesive soil. The type of lime in combination with soil type influences the resulting compressive strength.
Note 2: The agency performing this test method can be evaluated in accordance with Practice D3740. Notwithstanding statements on precision and bias contained in this method: The precision of this test method is dependent on the competence of the personnel performing it and the suitability of the equipment and facility used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing. Users of this test method are cautioned that compliance with Practice D3740 does not, in itself, ensure reliable testing. Reliable testing depends on many factors; Practice D3740 provides a means of evaluating some of these factors.
SCOPE
1.1 This test method covers procedures for preparing, curing, and testing laboratory-compacted specimens of soil-lime and other lime-treated materials (Note 1) for determining unconfined compressive strength. Depending on the diameter to height ratio, two procedures for determining the unconfined compressive strength of compacted soil-lime mixtures have been developed for specimens prepared at the maximum unit weight and optimum water content, or for specimens prepared at other target unit weight and water content levels. Other applications are given in Section 5 on Significance and Use.
Note 1: Lime-based products other than commercial quicklime and hydrated lime are also used in the lime treatment of fine-grained cohesive soils. Lime kiln dust (LKD) is collected from the kiln exhaust gases by cyclone, electrostatic, or baghouse-type collection systems. Some lime producers hydrate various blends of LKD plus quicklime to produce a lime-based product.  
1.2 Cored specimens of soil-lime should be tested in accordance with Test Methods D2166/D2166M.  
1.3 Two alternative procedures are provided:  
1.3.1 Procedure A describes procedures for preparing and testing compacted soil-lime specimens having height-to-diameter ratios between 2.00 and 2.50. This test method provides the standard measure of compressive strength.  
1.3.2 Procedure B describes procedures for preparing and testing compacted soil-lime specimens using Test Methods D698 compaction equipment and molds commonly available in most soil testing laboratories. Procedure B is considered to provide relative measures of individual specimens in a suite of test specimens rather than standard compressive strength values. Because of the lesser height-to-diameter ratio (1.15) of the cylinders, compressive strength determined by Procedure B will normally be greater than that by Procedure A.  
1.3.3 Results of unconfined compressive strength tests using Procedure B should not be directly compared to those obtained using Procedure A.  
1.4 All observed and calculated values shall conform to the guideline...

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ASTM D4452/D4452M-22(Practice)
Standard Practice for X-Ray Radiography of Soil Samples

SIGNIFICANCE AND USE
5.1 Many geotechnical tests require the utilization of intact, representative samples of soil. The quality of these samples depends on many factors. Many of the samples obtained by intact sampling methods have inherent anomalies. Sampling procedures cause disturbances of varying types and intensities. These anomalies and disturbances, however, are not always readily detectable by visual inspection of the intact samples before or after testing. Often test results would be enhanced if the presence and the extent of these anomalies and disturbances are known before testing or before destruction of the sample by testing. Such determinations assist the user in detecting flaws in sampling methods, the presence of natural or induced shear planes, and the presence of natural intrusions, such as gravels or shells at critical regions in the samples, the presence of sand and silt seams, and the intensity of disturbances caused by sampling.  
5.2 X-ray radiography provides the user with a picture of the internal massive structure of the soil sample, regardless of whether the soil is X-rayed within or without the sampling tube. X-ray radiography assists the user in identifying the following:  
5.2.1 Appropriateness of sampling methods used.  
5.2.2 Effects of sampling in terms of the disturbances caused by the turning of the edges of various thin layers in varved soils, large disturbances caused in soft soils, shear planes induced by sampling, or extrusion, or both, effects of overdriving of samplers, the presence of cuttings in sampling tubes, or the effects of using bent, corroded, or nonstandard tubes for sampling.  
5.2.3 Naturally occurring fissures, shear planes, etc.  
5.2.4 The presence of intrusions within the sample, such as calcareous nodules, gravel, or shells.  
5.2.5 Sand and silt seams, organic matter, large voids, and channels developed by natural or artificial leaching of soil components.
Note 1: The quality of the results produced by this standard is de...
SCOPE
1.1 This practice covers the determination of the quality of soil samples in thin wall tubes or of extruded soil cores by X-ray radiography.  
1.2 This practice enables the user to determine the effects of sampling and natural variations within samples as identified by the extent of the relative penetration of X-rays through soil samples.  
1.3 This practice can be used to X-ray soil cores (or observe their features on a fluoroscope) in thin wall tubes or liners ranging from approximately 50 to 150 mm [2 to 6 in.] in diameter. X-rays of samples in the larger diameter tubes provide a radiograph of major features of soils and disturbances, such as large scale bending of edges of varved clays, shear planes, the presence of large concretions, silt and sand seams thicker than 6 mm [1/4 in.], large lumps of organic matter, and voids or other types of intrusions. X-rays of the smaller diameter cores provide higher resolution of soil features and disturbances, such as small concretions (3 mm [1/8 in.] diameter or larger), solution channels, slight bending of edges of varved clays, thin silt or sand seams, narrow solution channels, plant root structures, and organic matter. The X-raying of samples in thin wall tubes or liners requires minimal preparation.  
1.4 Greater detail and resolution of various features of the soil can be obtained by X-raying extruded soil cores, as compared to samples in metal tubes. The method used for X-raying soil cores is the same as that for tubes and liners, except that extruded cores have to be handled with extreme care and have to be placed in sample troughs (similar to Fig. 2) before X-raying. This practice should be used only when natural water content or other intact soil characteristics are irrelevant to the end use of the sample.  
1.4.1 Often it is necessary to obtain greater resolution of features to determine the propriety of sampling methods, the representative nature of soil samples,...

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ASTM D2434-22(Test Method)
Standard Test Methods for Measurement of Hydraulic Conductivity of Coarse-Grained Soils

ABSTRACT
This test method covers the determination of the coefficient of permeability by a constant-head method for the laminar flow of water through granular soils. The procedure is to establish representative values of the coefficient of permeability of granular soils that may occur in natural deposits as placed in embankments, or when used as base courses under pavements. The different apparatus used in determining the granular soil permeability are presented. The methods in preparing the test specimen are presented in details. The testing and calculation procedure for granular soil permeability determination are presented.
SIGNIFICANCE AND USE
5.1 These test methods are used to measure one-dimensional vertical flow of water through initially saturated coarse-grained, pervious (that is, free-draining) soils under an applied hydraulic gradient. Hydraulic conductivity of coarse-grained soils is used in various civil engineering applications. These test methods are suitable for determination of hydraulic conductivity for soils with k > 10–7 m/s.
Note 2: Clean coarse-grained soils that are classified using Practice D2487-17 as GP, GW, SP, and SW can be tested using these test methods. Depending on fraction and characteristics of fine-grained particles present in soils, these test methods may be suitable for testing other soil types with fines content greater than 5 % (for example, GP-GC, SP-SM).  
5.2 Coarse-grained soils are to be tested at a void ratio representative of field conditions. For engineered fills, compaction specification can be used to provide target test conditions, whereas for natural soils, field testing of in-situ density can be used to provide target test conditions.  
5.3 Use of a dual-ring permeameter is included in these test methods in addition to a single-ring permeameter for the rigid wall test apparatus. The dual-ring permeameter allows for reducing potential adverse effects of sidewall leakage on measured hydraulic conductivity of the test specimens. The use of a plate at the outflow end of the specimen that contains a ring with a diameter smaller than the diameter of the permeameter and the presence of two outflow ports (one from the inner ring, one from the annular space between the inner ring and the permeameter wall) allows for separating the flow from the central region of the test specimen from the flow near the sidewall of the permeameter.
Note 3: Sidewall leakage has been reported to have significant influence on flow conditions for coarse-grained soils due to presence of larger voids at the boundary and higher void ratio in this region of the specimen. Three modificat...
SCOPE
1.1 These test methods cover laboratory measurement of the hydraulic conductivity (also referred to as coefficient of permeability) of water-saturated coarse-grained soils (for example, sands and gravels) with k > 10–7 m/s. The test methods utilize low hydraulic gradient conditions.  
1.2 This standard describes two methods (A and B) for determining hydraulic conductivity of coarse-grained soils. Method A incorporates use of a rigid wall permeameter and Method B incorporates the use of a flexible wall permeameter. A single- or dual-ring rigid wall permeameter may be used in Method A. A dual-ring permeameter may be preferred over a single-ring permeameter when adverse effects from short-circuiting of permeant water along the sidewalls of the permeameter (that is, prevent sidewall leakage) are suspected by the user of this standard.  
1.3 The test methods are used under constant head conditions.  
1.4 The test methods are used under saturated soil conditions.  
1.5 Water is used to permeate the test specimen with these test methods.  
1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Note 1: Hydraulic conductivity has traditionally been reported in cm/s in the US, even though the official SI unit for hydraul...

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