ASTM D1108-96(2001)
(Test Method)Standard Test Method for Dichloromethane Solubles in Wood
Standard Test Method for Dichloromethane Solubles in Wood
SCOPE
1.1 This test method covers the determination of the dichloromethane soluble content of wood, which is a measure of the waxes, fats, resins, oils, and similar materials.
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 4.1.
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D1108–96 (Reapproved 2001) Technical Association of Pulp and Paper Industry
Standard Method T 204-os-76
Standard Test Method for
Dichloromethane Solubles in Wood
This standard is issued under the fixed designation D 1108; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 5. Test Specimen
1.1 This test method covers the determination of the dichlo- 5.1 The test specimen shall consist of2gofair-dried
romethane soluble content of wood, which is a measure of the sawdustthathasbeengroundtopassa425-µm(40meshsieve)
waxes, fats, resins, oils, and similar materials. and be retained on a 250-µm (60 mesh) sieve.
1.2 This standard does not purport to address all of the
6. Procedure
safety concerns, if any, associated with its use. It is the
6.1 Weigh two 2-g test specimens in tared Alundum or
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica- fritted-glass crucibles. Dry one specimen in an oven for2hat
100 to 105°C; then place in a loosely stoppered weighing
bility of regulatory limitations prior to use. Specific precau-
tionary statements are given in 4.1. bottle, cool in a desiccator, and weigh. Continue the drying for
1-h periods until the weight is constant. Calculate the propor-
2. Significance and Use
tion of moisture-free sawdust in the air-dry specimen.
2.1 Dichloromethane extractable content of wood is a mea- 6.2 Place the other specimen in a Soxhlet extraction appa-
sure of such substances as waxes, fats, resins, phytosterols, and ratushavingataredSoxhletextractionflask.Setasmalldiskof
nonvolatilehydrocarbons.Theamountisinfluencedbyseason- fine-mesh screen wire in the top of the crucible to prevent loss
ing or drying the wood. of sample. Extract with 150 mL of dichloromethane for 6 to 8
h, keeping the solvent boiling briskly. This should provide at
3. Apparatus
least six to eight siphonings per hour.
3.1 Filtering Crucibles—Alundum or fritted-glass filtering 6.3 After evaporating the solvent from the extraction flask,
crucibles of coarse porosity shall be used.
dry the flask and contents in an oven for 1 h at 100 to 105°C,
3.2 Extraction Apparatus—A compact form of Soxhlet cool in a desiccator, and weigh. Continue the drying until there
extraction apparatus, with ground-glass joints, is preferable.
is no further loss in weight.
The apparatus shall consist of the following items:
7. Calculation and Report
3.2.1 Soxhlet Extraction Flask, having a capacity of 250
mL. 7.1 Report the results as percentage by weight of dichlo-
3.2.2 Soxhlet Extraction Tube, 45 to 50 mm in inside romethanesolublematterinthemoisture-freewood,calculated
diameter
...
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ABSTRACT
This practice presents the two standard methods for determining the strength values of clear wood of different species in the unseasoned condition, unadjusted for end use, applicable to the establishment of working stresses for different solid wood products such as lumber, laminated wood, plywood, and round timbers. Method A provides for the use of the results of surveys of wood density involving extensive sampling of forest trees, in combination with the data obtained from standard strength tests. The average strength properties are obtained from wood density survey data through linear regression equations establishing the relation of specific gravity to the several strength properties. Method B, on the other hand, provides for the establishment of tables of strength values based on standard tests of small clear specimens in the unseasoned condition for use when data from density surveys are not available. Separate tables are employed to present the data on woods grown in the United States and on woods grown in Canada. Guidelines for the interpretation of the data in terms of assigned values, information basic to the translation of the clear wood values into working stresses, presently available data with appropriate provisions for their application and use, and methods for estimating some useful mechanical properties by relating them to other properties are presented herein as well.
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1.1 This practice covers the determination of strength values for clear wood of different species in the unseasoned condition, unadjusted for end use, applicable to the establishment of design values for different solid wood products such as lumber, laminated wood, plywood, and round timbers. Presented are:
1.1.1 Procedures by which test values obtained on small clear specimens may be combined with density data from extensive forest surveys to make them more representative,
1.1.2 Guidelines for the interpretation of the data in terms of assigned values for combinations of species or regional divisions within a species to meet special marketing needs, and
1.1.3 Information basic to the translation of the clear wood values into design values for different solid wood products for different end uses.
1.1.4 For species where density survey data are not as yet available for the re-evaluation of average strength properties, the presently available data from tests made under the sampling methods and procedures of Test Methods D143 or Practice E105 are provided with appropriate provision for their application and use. Because of the comprehensive manner in which the density survey is undertaken, it follows that the re-evaluated strength data are intended to be representative of the forest stand, or rather large forest subdivisions.
1.1.5 Some useful mechanical properties (tensile strengths parallel and perpendicular to grain, modulus of rigidity for a longitudinal-transverse plane, and transverse modulus of elasticity) have not been extensively evaluated. Methods are described for estimating these properties by their relation to other properties.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 These test methods cover tests on small clear specimens of wood that are made to provide the following:
4.1.1 Data for comparing the mechanical properties of various species,
4.1.2 Data for the establishment of correct strength functions, which in conjunction with results of tests of timbers in structural sizes (see Test Methods D198 and Test Methods D4761), afford a basis for establishing allowable stresses, and
4.1.3 Data to determine the influence on the mechanical properties of such factors as density, locality of growth, position in cross section, height of timber in the tree, change of properties with seasoning or treatment with chemicals, and change from sapwood to heartwood.
SCOPE
1.1 These test methods cover the determination of various strength and related properties of wood by testing small clear specimens.
1.1.1 These test methods represent procedures for evaluating the different mechanical and physical properties, controlling factors such as specimen size, moisture content, temperature, and rate of loading.
1.1.2 Sampling and collection of material is discussed in Practice D5536. Sample data, computation sheets, and cards have been incorporated, which were of assistance to the investigator in systematizing records.
1.1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard. When a weight is prescribed, the basic inch-pound unit of weight (lbf) and the basic SI unit of mass (Kg) are cited.
1.2 The procedures for the various tests appear in the following order:
Sections
Photographs of Specimens
5
Control of Moisture Content and Temperature
6
Record of Heartwood and Sapwood
7
Static Bending
8
Compression Parallel to Grain
9
Impact Bending
10
Toughness
11
Compression Perpendicular to Grain
12
Hardness
13
Shear Parallel to Grain
14
Cleavage
15
Tension Parallel to Grain
16
Tension Perpendicular to Grain
17
Nail Withdrawal
18
Specific Gravity and Shrinkage in Volume
19
Radial and Tangential Shrinkage
20
Moisture Determination
21
Permissible Variations
22
Calibration
23
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 This test method is useful as a screening procedure for selecting fungicides or formulations for more rigorous field evaluation.
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1.1 This (laboratory) test method is used for determining the minimum concentration of fungicide, or formulation of fungicides, that is effective in preventing biodeterioration by sapstain fungi and molds in selected species of wood under optimum laboratory conditions.
Note 1: From the results of this test, commercial treating solution concentrations cannot be estimated without further field tests.
1.2 The requirements for test materials and procedures are discussed in the following order:
Section
Summary of Test Method
4
Apparatus
6
Reagents
7
Wood
8
Test Fungi
9
Culture Media
10
Preparation of Inoculum
11
Preparation of Test Chambers
12
Treatment of Samples
13
Inoculation and Incubation
14
Evaluation of the Test
15
Report
16
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 This practice covers procedures of sampling for obtaining small, clear wood specimens which, when tested in accordance with Test Methods D143 and, in conjunction with full-size product tests, will provide mechanical properties for use in deriving design properties for lumber, panels, poles, house logs, and other products.
4.2 Data obtained by testing specimens sampled in accordance with these methods also provide information on the influence on mechanical properties of such factors as density, locality of growth, position in cross section, height in the tree, and moisture content.
4.3 Cruciform sampling is of principal value when information is desired on the influence on mechanical properties of height in the tree; of age or radial position in the tree; of rate of growth; the change from sapwood to heartwood; the relationships between mechanical properties and factors such as specific gravity; and making general comparisons between species for purposes of rating or selecting species for specific end-use products. Cruciform sampling does not provide unbiased estimates of mean values, percentile or other descriptive statistics, or a means of associating statistical confidence with estimates of descriptive statistics.
4.4 Double sampling is used when it is desired to improve or update existing estimates of mechanical property values that are the basis for establishing allowable design stresses for stress-graded lumber, plywood, poles and piling, and other wood products. The method involves predicting one property by carefully observing a well-correlated auxiliary property that is presumably easier or cheaper to measure. A sample estimate of the auxiliary property is obtained with a high degree of precision by representatively sampling the population. A smaller independent sample or a subsample of the large sample is used to establish a relationship between the auxiliary property and the property for which an estimate is desired. As applied to sampling a f...
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1.1 This practice offers two alternative physical sampling procedures: cruciform sampling and random sampling. The choice of procedure will depend upon the intended use for the test results, the resources available for sampling and testing, and the availability of existing data on the mechanical properties and specific gravity of the species of interest.
1.2 A third procedure, double sampling, is included primarily by reference. This procedure applies the results of cruciform or random samples through correlation to improve or update property values.
1.3 Units—The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
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1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 The purpose of this test method is to provide a relative measurement of the combustibility of fire-retardant-treated wood specimens based on their percentage loss in weight under controlled fire exposure conditions (1).3 In addition, other possible data include rate of weight loss, time of flaming and afterglowing, increase in temperature, and maximum vertical flame progress.
4.2 This test method is not sufficiently large scale to evaluate the suitability of a given treated product for building construction, but it is a convenient method to use for purposes of development or as a quality-control test during manufacture.
4.3 This test method gives a procedure for sampling and preparation of test specimens from a lot of treated material in which complete penetration is a requirement. A procedure is also given for the sampling of charges at a treating plant for purposes of quality control of the treatment process.
4.4 This test method has proven useful for evaluating comparative fire performance effectiveness of fire-retardant chemicals and treatment formulations for wood and wood products (2-5).
4.5 In this test method, the specimens are subjected to one or more specific sets of laboratory test conditions. If different test conditions are substituted or the anticipated end-use conditions are changed, it is possible that this test method will not predict changes in the fire-test-response characteristics measured. Therefore, the results are valid only for the fire test exposure conditions described in this procedure.
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1.1 This test method covers fire-tube test procedures for fire tests for combustible properties of wood treated to reduce flammability. This test method relates to properties of treated wood, as such, rather than to the performance of a fabrication used as an element of construction. Performance under this test method shall be as prescribed in requirements applicable to materials intended for specific uses.
1.2 This test method is a fire-test-response standard.
1.3 The SI values given in parentheses are provided for information purposes only.
1.4 This standard is used to measure and describe the response of materials, products, or assemblies to heat and flame under controlled conditions, but does not by itself incorporate all factors required for fire hazard or fire risk assessment of the materials, products, or assemblies under actual fire conditions.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 Fire testing is inherently hazardous. Adequate safeguards for personnel and property shall be employed in conducting these tests.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
6.1 The flexural properties established by this test method provide:
6.1.1 Data for use in development of grading rules and specifications;
6.1.2 Data for use in development of design values for structural members;
6.1.3 Data on the influence of imperfections on mechanical properties of structural members;
6.1.4 Data on strength properties of different species or grades in various structural sizes;
6.1.5 Data for use in checking existing equations or hypotheses relating to the structural behavior;
6.1.6 Data on the effects of chemical or environmental conditions on mechanical properties;
6.1.7 Data on effects of fabrication variables such as depth, taper, notches, or type of end joint in laminations; and
6.1.8 Data on relationships between mechanical and physical properties.
6.2 Procedures are described here in sufficient detail to permit duplication in different laboratories so that comparisons of results from different sources will be valid. Where special circumstances require deviation from some details of these procedures, these deviations shall be carefully described in the report (see Section 11).
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1.1 These test methods cover the evaluation of lumber and wood-based products in structural sizes by various testing procedures.
1.2 The test methods appear in the following order:
Sections
Flexure
4 – 11
Compression (Short Specimen)
13 – 20
Compression (Long Specimen)
21 – 28
Tension
29 – 36
Torsion
37 – 44
Shear Modulus
45 – 52
1.3 Notations and symbols relating to the various testing procedures are given in Appendix X1.
1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Density and specific gravity are cornerstone terms that help define many useful properties of wood and wood-based materials. These terms designate concepts that have distinct definitions though they relate to the same characteristic (mass in a unit volume). Generally, in the US and Canada, density of wood is measured in terms of specific gravity, or relative density. In the wood-based composites industry and internationally the term density is often preferred.
5.2 The basic density and basic specific gravity of wood are used in the forestry industry for calculating the oven-dry weight of wood fiber contained in a known wood volume of various wood species. Thus, it serves as an indicator of the amount of wood pulp that could be produced, the workability of the material or its shipping weight. This information is referenced in various resources, including Wood Handbook.5 Note that specific gravity varies within a tree, between trees, and between species. Since the specific gravity of wood cell wall substance is practically constant for all species (approximately 1.53), it is apparent that individual specific gravity value is indicative of the amount of wood cell wall substance present. It affords a rapid and valuable test method for selection of wood for specific uses. In US and Canadian building codes, the oven-dry specific gravity is correlated to various strength characteristics of wood products (for example, compression perpendicular to grain, shear strength and fastener holding capacity).
5.3 It is often desirable to know the density or specific gravity of a living tree, a structural member already in place, a log cross section, a segment of a research element, or the earlywood or latewood layer. Therefore, it is possible that specimens will be large or small, regular or irregular in shape, and at a variety of moisture contents. These test methods give procedures that include all of these variables and provides for calculation of density and specific gr...
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1.1 These test methods cover the determination of the density and specific gravity (relative density) of wood and wood-based materials to generally desired degrees of accuracy and for specimens of different sizes, shapes, and moisture content conditions. The test method title is indicative of the procedures used or the specific area of use.
Section
Test Method A—Volume by Measurement
8
Test Method B—Volume by Water Immersion
9
Test Method C—Flotation Tube
10
Test Method D—Forstner Bit
11
Test Method E—Increment Core
12
Test Method F—Chips
13
Test Method G—Full-Size Members
14
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SCOPE
1.1 This specification covers the physical characteristics of round timber construction poles to be used either treated or untreated.
1.2 This test method covers basic principles for establishing recommended design stress values for round timber construction poles that are applicable to the quality described.
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 Machining tests are made to determine the working qualities and characteristics of different species of wood and of different wood-based panel materials under a variety of machine operations such as are encountered in commercial manufacturing practice. The tests provide a systematic basis for comparing the behavior of different products with respect to woodworking machine operations and of evaluating their potential suitability for certain uses where these properties are of prime importance.
SCOPE
1.1 These test methods cover procedures for planing, routing/shaping, turning, mortising, boring, and sanding, all of which are common wood-working operations used in the manufacture of wood products. These tests apply, in different degrees, to two general classes of materials:
1.1.1 Wood in the form of lumber, and
1.1.2 Wood-base panel materials such as plywood and wood-base fiber and particle panels.
1.2 Because of the importance of planing, some of the variables that affect the results of this operation are explored with a view to determining optimum conditions. In most of the other tests, however, it is necessary to limit the work to one set of fairly typical commercial conditions in which all the different woods are treated alike.
1.3 Several factors enter into any complete appraisal of the machining properties of a given wood or wood-base panel. Quality of finished surface is recommended as the basis for evaluation of machining properties. Rate of dulling of cutting tools and power consumed in cutting are also important considerations but are beyond the scope of these test methods.
1.4 Although the methods presented include the results of progressive developments in the evaluation of machining properties, further improvements are anticipated. For example, by present procedures, quality of the finished surface is evaluated by visual inspection, but as new mechanical or physical techniques become available that will afford improved precision of evaluation, they should be employed.
1.5 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
4.1 Computer simulation is known to be a very powerful analytical tool for both practitioners and researchers in the area of wood products and their applications in structural engineering. Complex structural systems can be analyzed by computer with the computer generating the system components, given the probability distribution of each component. Frequently the components are single boards for which a compatible set of strength and stiffness properties are needed. However, the entire structural simulation process is dependent upon the adequacy of the standard uniform number generator required to generate random observations from prescribed probability distribution functions.
4.2 The technological capabilities and wide availability of microcomputers has encouraged their increased use for simulation studies. Tests of random number generators in commonly available microcomputers have disclosed serious deficiencies (1).3 Adequacy may be a function of intended end-use. This practice is concerned with generation of sets of random numbers, as may be required for simulations of large populations of material properties for simulation of complex structures. For more demanding applications, the use of packaged and pretested random number generators is encouraged.
SCOPE
1.1 This practice gives a minimum testing procedure of computer generation routines for the standard uniform distribution. Random observations from the standard uniform distribution, RU, range from zero to one with every value between zero and one having an equal chance of occurrence.
1.2 The tests described in this practice only support the basic use of random number generators, not their use in complex or extremely precise simulations.
1.3 Simulation details for the normal, lognormal, 2-parameter Weibull and 3-parameter Weibull probability distributions are presented.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.See specific warning statement in 5.5.3.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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