ASTM C781-96
(Practice)Standard Practice for Testing Graphite and Boronated Graphite Components for High-Temperature Gas-Cooled Nuclear Reactors
Standard Practice for Testing Graphite and Boronated Graphite Components for High-Temperature Gas-Cooled Nuclear Reactors
SCOPE
1.1 This practice covers the test methods for measuring those properties of graphite and boronated graphite materials that may be used for the design and evaluation of high-temperature gas-cooled reactors.
1.2 The test methods referenced herein are applicable to materials used for replaceable and permanent components as defined in Section 7 and include fuel and removable reflector elements; target elements and insulators; permanent side reflector elements; core support pedestals and elements; control rod, reserve shutdown, and burnable poison compacts, and neutron shield material.
1.3 This practice includes test methods that have been selected from existing ASTM standards, ASTM standards that have been modified, and new ASTM standards that are specific to the testing of materials listed in 1.2. Comments on individual test methods for graphite and for boronated graphite components are given in Sections 8 and 10, respectively. The test methods are summarized in Tables 1 and 2.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
General Information
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Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn. Contact ASTM
International (www.astm.org) for the latest information.
An American National Standard
Designation: C 781 – 96
Standard Practice for
Testing Graphite and Boronated Graphite Components for
High-Temperature Gas-Cooled Nuclear Reactors
This standard is issued under the fixed designation C 781; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope sorption Cross Section of Nuclear Graphite
C 651 Test Method for Flexural Strength of Manufactured
1.1 This practice covers the test methods for measuring
Carbon and GraphiteArticles Using Four-Point Loading at
those properties of graphite and boronated graphite materials
Room Temperature
that may be used for the design and evaluation of high-
C 695 Test Method for Compressive Strength of Carbon
temperature gas-cooled reactors.
and Graphite
1.2 The test methods referenced herein are applicable to
C 709 Terminology Relating to Manufactured Carbon and
materials used for replaceable and permanent components as
Graphite
defined in Section 7 and include fuel and removable reflector
C 747 Test Method for Moduli of Elasticity and Fundamen-
elements; target elements and insulators; permanent side re-
tal Frequencies of Carbon and Graphite Materials by Sonic
flector elements; core support pedestals and elements; control
Resonance
rod, reserve shutdown, and burnable poison compacts; and
C 749 Test Method for Tensile Stress-Strain of Carbon and
neutron shield material.
Graphite
1.3 This practice includes test methods that have been
C 816 Test Method for Sulfur in Graphite by Combustion-
selected from existing ASTM standards, ASTM standards that
Iodometric Titration Method
have been modified, and newASTM standards that are specific
C 838 Test Method for Bulk Density of As-Manufactured
tothetestingofmaterialslistedin1.2.Commentsonindividual
Carbon and Graphite Shapes
test methods for graphite and boronated graphite components
C 1179 Test Method for Oxidative Mass Loss of Manufac-
are given in Sections 8 and 10, respectively. The test methods
turered Carbon and Graphite Materials in Air
are summarized in Table 1 and Table 2.
C 1251 Test Method for Determination of Specific Surface
1.4 This standard does not purport to address all of the
Areas ofAdvanced Ceramic Materials by GasAdsorption
safety concerns, if any, associated with its use. It is the
D 2854 Test Method for Apparent Density of Activated
responsibility of the user of this standard to establish appro-
Carbon
priate safety and health practices and determine the applica-
D 2862 Test Method for Particle Size Distribution of
bility of regulatory limitations prior to use.
Granular Activated Carbon
2. Referenced Documents
D 4292 Test Method for Vibrated Bulk Density of Calcined
Petroleum Coke
2.1 ASTM Standards:
E 132 Test Method for Poisson’s Ratio at Room Tempera-
C 559 Test Method for Bulk Density by Physical Measure-
ture
ments of Manufactured Carbon and Graphite Articles
E 228 Test Method for Linear Thermal Expansion of Solid
C 560 Test Methods for Chemical Analysis of Graphite
Materials with a Vitreous Silica Dilatometer
C 561 Test Method for Ash in a Graphite Sample
E 261 Practice for Determining Neutron Fluence Rate, Flu-
C 577 Test Method for Permeability of Refractories
ence, and Spectra by Radioactivation Techniques
C 625 Practice for Reporting Irradiation Results on Graph-
E 1461 Test Method for Thermal Diffusivity of Solids by
ite
the Flash Method
C 626 Methods for Estimating the Thermal Neutron Ab-
3. Terminology
3.1 Definition:
This practice is under the jurisdiction of ASTM Committee D02 on Petroleum
Products and Lubricants and is the direct responsibility of Subcommittee D02.F on
Manufactured Carbon and Graphite Products . Discontinued; see 1985 Annual Book of ASTM Standards, Vol 15.01.
Current edition approved Nov. 10, 1996. Published December 1996. Originally Annual Book of ASTM Standards, Vol 05.02.
published as C 781 – 77. Last previous edition C 781 – 93. Annual Book of ASTM Standards, Vol 03.01.
2 7
Annual Book of ASTM Standards, Vol 05.05. Annual Book of ASTM Standards, Vol 14.02.
3 8
Annual Book of ASTM Standards, Vol 15.01. Annual Book of ASTM Standards, Vol 12.02.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn. Contact ASTM
International (www.astm.org) for the latest information.
C 781
TABLE 1 Summary of Test Methods for Graphite Components
NOTE 1—Designations under preparation will be added as editorial changes when approved.
Fuel, Removable Permanent Core
Reflector, and Core Side Support
Support Elements; Reflector Pedestals
Target Assemblies Elements and Dowel
and Insulators; and and Dowel Pins
Dowel Pins Pins
Bulk Density:
As-Manufactured Shapes C 838 C 838 C 838
Machined Specimens C 559 C 559 C 559
Thermal Properties:
A A A
Linear Thermal Expansion E 228 E 228 E 228
A A A
Thermal Conductivity E 1461 E 1461 E 1461
Mechanical Properties:
Compressive Strength C 695 C 695 C 695
A A A
Tensile Properties C 749 C 749 C 749
A A A
Poisson’s Ratio E 132 E 132 E 132
A A A
Flexural Strength C 651 C 651 C 651
BB B
Fracture Toughness
Modulus of Elasticity C 747 C 747 C 747
Oxidation Related Properties:
B B B
Relative Oxidation Rate C 1179 C 1179 C 1179
Surface Area C 1251 C 1251 C 1251
AB AB AB
Permeability C 577 C 577 C 577
B B B
Catalytic Impurities C 560 C 560 C 560
Sulfur Concentration C 816 C 816 C 816
BB B
Porosity
Neutronic Impurities:
A A A
Ash C 561 C 561 C 561
BB B
Spectroscopic Analysis
A AC
Thermal Absorption Cross C 626 C 626
Section
A
Modification of this test method is required. See Section 8 for details.
B
New test methods are required. See Section 8 for details.
C
There is no identified need for determining this property.
TABLE 2 Summary of Test Methods for Boronated Graphite
4. Significance and Use
Components
4.1 Properly data obtained with the recommended test
NOTE 1—Designations under preparation will be added as editorial
methods identified herein may be used for research and
changes when approved.
development, design, manufacturing control, specifications,
performance evaluation, and regulatory statutes pertaining to
Compacts
high temperature gas-cooled reactors.
Neutron Shield
Control Burnable Reserve
Material
4.2 The test methods are applicable primarily to specimens
Rod Poison Shutdown
in the unirradiated and unoxidized state. Many are also
Bulk Density C 838 C 838 C 838 D 4292
A A AB applicable to specimens in the irradiated or oxidized state, or
Linear Thermal Expansion E 228 E 228
CCC
Particle Size D 2862 both, provided the specimens meet all requirements of the test
Mechanical Strength:
method. The user is cautioned to consider the instructions
A A A B
Compressive Strength C 695 C 695 C 695
B B B C given in the test methods.
Impact Performance
Chemical Properties: 4.3 Additional test methods are in preparation and will be
CCC C
Catalytic Impurities
incorporated. The user is cautioned to employ the latest
CCC C
Sulfur Concentration
CCC C revision.
Hafnium Concentration
CCC C
Relative Oxidation Rate
Boron Analysis:
5. Sample Selection
CCC C
Total Boron
CCC C
Boron as Oxide 5.1 All test specimens should be selected from materials
D D D D
B C Particle Size D 2862 D 2862 D 2862 D 2862
that are representative of those to be used in the intended
A
Modification of this test method is required. See Section10 for details.
application.
B
There is no identified need for determining this property.
C
New test methods are required. See Section 10 for details.
D
6. Test Reports
Additional test methods are required. See Section10 for details.
6.1 Test results should be reported in accordance with the
3.1.1 Terminology C 709 shall be considered as applying to reporting requirements included in the applicable test method.
the terms used in this practice. Where relevant, information on grade designation, lot number,
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn. Contact ASTM
International (www.astm.org) for the latest information.
C 781
billet number, orientation, and location (position of sample in the target assembly insulators are to provide thermal insulation
the original billet) shall be provided. of the target assemblies from the fuel or removable reflector
6.2 Information on specimen irradiation conditions shall be elements and a physical constraint for the flow of coolant gas.
reported in accordance with Practices C 625 and E 261 or 7.3 Permanent Side Reflector Elements:
referenced to source information of equivalent content. 7.3.1 Apermanent side reflector element is a graphite block
that is designed to remain permanently in the core but may be
GRAPHITE COMPONENTS
removed for inspection and replacement, if necessary. A
permanent side reflector element contains channels for align-
7. Description and Function
ment dowel pins. It may also contain channels for neutron flux
7.1 Fuel and Removable Reflector Elements:
control materials (boronated steel pins) and nuclear instrumen-
7.1.1 A fuel element is a removable graphite element that
tation,andrecessedareasalongitslengthonitsouterperiphery
contains channels for the passage of coolant gas, the fuel
to provide channels for the passage of coolant gas between the
material, the alignment dowel pins, and the insertion of a
element and the metallic lateral restraint for the reactor core.
handling machine pickup head. A fuel element may also
7.3.2 The permanent side reflector elements encircle the
contain channels for reactivity control material (control rods),
active (fuel) elements and passive (removable reflector) ele-
reserve shutdown compacts, and burnable poison compacts,
ments of the reactor core and serve multiple functions, includ-
graphite target assemblies and insulators, and nuclear instru-
ing (a) vertical and lateral mechanical support for the perma-
mentation.
nent side reflector elements above and beside them, (b) lateral
7.1.2 The fuel elements serve multiple functions, including
mechanical support for the fuel, removable reflector, and core
(a)verticalandlateralmechanicalsupportforthefuelelements
support elements, (c) moderation of fast neutrons within the
and removable reflector elements above and adjacent to them,
reflector region, (d) reflection of thermal neutrons back into the
and for the fuel, reactivity control materials, target assemblies
core region, and (e) support, guide, and containment of nuclear
and insulators, and nuclear instrumentation within them, (b)
instrumentation and neutron flux control materials (boronated
moderation of fast neutrons within the core region, (c) a
steel pins) for reducing the neutron flux to metallic structures
thermal reservoir and conductor for nuclear heat generated in
outside the permanent side reflector boundary.
the fuel, (d) a physical constraint for the flow of coolant gases,
7.4 Core Support Pedestals and Elements:
and (e) a guide for and containment of fuel material, reactivity
7.4.1 A core support pedestal is a graphite column that is
control materials, target assemblies and insulators, and nuclear
designedtoremainpermanentlyinthecorebutcanberemoved
instrumentation.
for inspection and replacement, if necessary. A core support
7.1.3 Aremovable reflector element is a removable graphite
pedestal has a central reduced cross-section (dog bone shape)
element that contains channels for the alignment dowel pins
that at its upper end contains channels for the passage of
and the insertion of a handling machine pickup head. A
coolant gas, alignment dowel pins, and the insertion of a
removable reflector element may also contain channels for the
handling machine pickup head, and at its lower end contains a
passage of coolant gas, reactivity control materials (control
recessed region for locating it with respect to the metallic
rods), neutron flux control materials (neutron shield materials),
structure that supports the graphite core support assembly. A
target assemblies and insulators, and nuclear instrumentation.
core support element is a graphite element that contains
7.1.4 The primary function of the removable reflector ele-
channels for alignment dowel pins and the insertion of a
ments that are located at the boundaries of the active reactor
handling machine pickup head.The core support elements may
core (fuel elements) is to provide for moderation of fast
also contain channels for the passage of coolant gas, neutron
neutronsescapingfromandreflectionofthermalneutronsback
flux control materials, and nuclear instrumentation.
into the active core region.
7.4.2 The primary function of the core support pedestals is
7.1.5 Except for support, guide, and containment of fuel
to provide for vertical mechanical support for core support
material, removable reflector elements may also serve any of
elements and permanent side reflector elements above them. In
the functions listed in 7.1.2.
addition, core support pedestals provide for lateral mechanical
7.2 Target Assemblies and Insulators:
support for adjacent core support pedestals and permanent side
7.2.1 A target assembly is a removable graphite canister
reflector elements and physical constraint for the flow of
consisting of an inner and outer annular sleeve and bottom and
coolant gases. The primary function of the core support
top end caps, that contains an annular channel for target
elements is to provide for vertical mechanical support for core
materials and a central channel for the passage of cooling gas.
support, fuel, and removable reflector elements above them. In
A target assembly insulator is an annular sleeve containing a
addition, core support elements provide for lateral mechanical
recessed area around its outer circumference that provides a
support for adjacent core support and permanent side reflector
thermal insulating gap between the insulating sleeve and the
elementsandmayprovideforthephysicalconstraintofcoolant
adjoining element channel. The inner circumference of the
gases and for the support, guide, and containment of neutron
insulating sleeve provides a channel for the passage of coolant
flux control materials and nuclear instrumentation.
gas between the insulator and the target assembly.
8. Test Methods
7.2.2 The primary function of the target asemblies is to
provide support, guide, and containment of target materials 8.1 Bulk Density:
used for the production of special radioisotopes and a physical 8.1.1 Determine bulk density on as-manufactured
...
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