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ASTM

ASTM D6627-01

(Test Method)

Standard Test Method for Determination of a Volatile Distillate Fraction of Cold Asphalt Mixtures

Standard Test Method for Determination of a Volatile Distillate Fraction of Cold Asphalt Mixtures

SCOPE
1.1 This test method covers the determination, by direct measurement, of the ambient to 500oF (260oC) volatile distillate fraction of cold mix asphalt mixtures.
1.2 A precision and bias statement for the Standard has not been developed since this test method is used for research purposes or information only. Therefore this Standard should not be used for acceptance or rejection of a material for purchasing purposes.
1.3 The values stated in inch-pound units are to be regarded as the standard. The SI units given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Feb-2001
ICS
75.140 - Waxes, bituminous materials and other petroleum products
Technical Committee
D04 - Road and Paving Materials
Drafting Committee
D04.27 - Cold Mix Asphalts
Current Stage
Ref Project

Relations

Replaced By
ASTM D6627-01(2006) - Standard Test Method for Determination of a Volatile Distillate Fraction of Cold Asphalt Mixtures
Effective Date
15-Dec-2006

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ASTM D6627-01 - Standard Test Method for Determination of a Volatile Distillate Fraction of Cold Asphalt MixturesASTM D6627-01 - Standard Test Method for Determination of a Volatile Distillate Fraction of Cold Asphalt Mixtures
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ASTM D6627-01 - Standard Test Method for Determination of a Volatile Distillate Fraction of Cold Asphalt Mixtures
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D6627–01
Standard Test Method for
Determination of a Volatile Distillate Fraction of Cold
Asphalt Mixtures
This standard is issued under the fixed designation D 6627; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope theheadistightlyattachedbymeansofaclamp.Theheadshall
be of a metal, preferably copper or brass, and shall be provided
1.1 This test method covers the determination, by direct
with a tubular opening of 25 mm (1 in.) in inside diameter and
measurement, of the ambient to 500°F (260°C) volatile distil-
an additional tubular opening of 13 mm ( ⁄2 in.) in inside
late fraction of cold mix asphalt mixtures.
diameter. Threaded into the 25 mm (1 in.) tubular opening is a
1.2 A precision and bias statement for the Standard has not
stainless steel or brass fitting connected firmly to a ground
been developed since this test method is used for research
glass joint by means of flexible stainless steel or glass tubing.
purposes or information only. Therefore this Standard should
Inserted into the 13 mm ( ⁄2 in.) tubular opening is a metal
not be used for acceptance or rejection of a material for
thermometer with a range of 93 to 538°C (200 to 1000°F)
purchasing purposes.
extending 125 mm (5 in.) into the metal still and firmly
1.3 The values stated in inch-pound units are to be regarded
connected by means of a graphite ferrule compression fitting.
as the standard. The SI units given in parentheses are for
4.2 Condenser, of the water-cooled reflux glass-tube type,
information only.
having a condenser jacket not less than 400 mm (15 ⁄4 in.) long
1.4 This standard does not purport to address all of the
3 1
with an inner tube 9.5 to 13 mm ( ⁄8 to ⁄2 in.) in the outside
safety concerns, if any, associated with its use. It is the
diameter.The end of the condenser inserted in the ground glass
responsibility of the user of this standard to establish appro-
joint shall be ground off at an angle of 30° from the vertical
priate safety and health practices and determine the applica-
axis of the condenser. For mixtures with very volatile solvents,
bility of regulatory limitations prior to use.
it may be necessary to supplement this water-cooled condenser
2. Referenced Documents
with a second water-cooled condenser of approximately the
same dimensions.
2.1 ASTM Standards:
4.3 CollectionFlask, cylinder of well-annealed glass having
D 244 Test Methods and Practices for EmulsifiedAsphalts
a capacity of 100 mL graduated with divisions of 0.1 mL and
D 979 Practice for Sampling Bituminous Paving Mixtures
attached to the condenser(s) by means of a well-annealed glass
D 1461 Test Method for Moisture or Volatile Distillates in
bend. The glass bend attaching the condenser to the graduated
Bituminous Paving Mixtures
cylinder is secured by ground glass joints on either end and
D 4753 Specification or Evaluating, Selecting and Specify-
vented witha3mm( ⁄8 in.) vent on top of the bend directly
ing Balances and Scales for Use in Soil, Rock and
above the graduated cylinder to prevent pressure in the
Construction Materials Testing
apparatus. The collection flask is submerged to the top of the
3. Significance and Use
gradations in an ice bath.
4.4 Distillation Liquid, 40 mL of distilled water.
3.1 This test method is used for determining the amount of
4.5 Heating Device, of high temperature electrical heating
a temperature specific volatile distillate fraction in cold mix
tape wrapped around the entire still and the connecting tubing
asphalt mixtures.
between the still and condenser.Avariable voltage transformer
4. Apparatus
connected to the heating tape is used to control the rate of
temperature rise to approximately 5°C (10°F) per minute.
4.1 AVertical Cylindrical Metal Still, similar to that used in
Insulate the entire still, including the connecting tubing from
Test Methods D 244, having a faced flange at the top to which
the still to the condenser, with 25 mm (1 in.) of fiberglass
insulation to prevent heat loss.
This test method is under the jurisdiction of AS
...

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1.1 This test method covers the determination of bulk specific gravity of compacted asphalt mixtures by the vacuum sealing method.  
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SIGNIFICANCE AND USE
3.1 This test method is used for determining the amount of a temperature-specific volatile distillate fraction in cold mix asphalt mixtures.
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SCOPE
1.1 This practice covers the conditioning of asphalt binders to simulate accelerated aging (oxidation) by means of pressurized air and elevated temperature. This is intended to simulate the changes in rheology which occur in asphalt binders during in-service oxidative aging, but may not accurately simulate the relative rates of aging. It is normally intended for use with residue from Test Method D2872 (RTFOT), which is designed to simulate plant aging.
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1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard
Note 2: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.  
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Standard Test Method for Resistance to Plastic Flow of Bituminous Mixtures Using Marshall Apparatus (6 in. Diameter Specimen)

SIGNIFICANCE AND USE
3.1 This test method is used in the laboratory mix design of bituminous mixtures. Specimens are prepared in accordance with the method and tested for maximum load and flow. Density and voids properties may also be determined on specimens prepared in accordance with the method. The testing section of this method can also be used to obtain maximum load and flow for bituminous paving specimens cored from pavements or prepared by other methods. These results may differ from values obtained on specimens prepared by this test method.
SCOPE
1.1 This test method covers the measurement of the resistance to plastic flow of cylindrical specimens of bituminous paving mixture loaded on the lateral surface by means of the Marshall apparatus. This test method is for use with mixtures containing asphalt cement and aggregate up to 11/2 in. (37.5 mm) nominal maximum size.  
1.2 The values stated in inch-pound units are to be regarded as standard except for reference to sieve sizes and size of aggregate as measured by testing sieves in which SI units are standard according to Specification E11. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
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3.1 This test method is useful in confirming that a material has been added to the asphalt to provide a significant elastomeric characteristic. It does not necessarily identify the type or amount of material added.
Note 1: The quality of results produced by this standard is dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guidance provides a means of evaluating and controlling some of those factors.
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1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This method indicates approximate change in properties of asphalt during conventional hot-mixing at about 150 °C [302 °F] as indicated by viscosity, penetration, or ductility measurements. It yields a residue which approximates the asphalt condition as incorporated in the pavement. If the mixing temperature differs appreciably from the 150 °C [302 °F] level, more or less effect on properties will occur.
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SCOPE
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SIGNIFICANCE AND USE
5.1 The penetration test is used as a measure of consistency. Higher values of penetration indicate softer consistency.
Note 2: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This test method covers determination of the penetration of semi-solid and solid bituminous materials.  
1.2 The needles, containers, and other conditions described in this test method provide for the determinations of penetrations up to 500.
Note 1: See the section on Penetration of Test Methods D244 for information and precision and bias on testing emulsion residue.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.4 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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