ASTM D113-07
(Test Method)Standard Test Method for Ductility of Bituminous Materials (Withdrawn 2016)
Standard Test Method for Ductility of Bituminous Materials (Withdrawn 2016)
SIGNIFICANCE AND USE
This test method provides one measure of tensile properties of bituminous materials and may be used to measure ductility for specification requirements.
SCOPE
1.1 This test method describes the procedure for determining the ductility of a bituminous material measured by the distance to which it will elongate before breaking when two ends of a briquet specimen of the material, of the form described in Section 4, are pulled apart at a specified speed and at a specified temperature. Unless otherwise specified, the test shall be made at a temperature of 25 ± 0.5°C and with a speed of 5 cm/min ± 5.0 %. At other temperatures the speed should be specified.
1.2 Because of the large number of methods for obtaining test samples, it is impractical to discuss specific products in this test method. Refer to individual product specifications for guidance in obtaining a test sample.
1.3 The values stated in SI units are to be regarded as the standard. Values in parenthesis in inch-pound units are provided for informational purposes only.
1.4 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet (MSDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury containing products, or both, in your state may be prohibited by state law.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
WITHDRAWN RATIONALE
This test method describes the procedure for determining the ductility of a bituminous material measured by the distance to which it will elongate before breaking when two ends of a briquet specimen of the material are pulled apart at a specified speed and at a specified temperature.
Formerly under the jurisdiction of Committee D04 on Road and Paving Materials, this test method was withdrawn in January 2016 in accordance with section 10.6.3 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
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Designation: D113 − 07 AmericanAssociation State
Highway and Transportation Officials Standard
AASHTO No.: T51
Standard Test Method for
1
Ductility of Bituminous Materials
This standard is issued under the fixed designation D113; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 2. Referenced Documents
2
1.1 This test method describes the procedure for determin-
2.1 ASTM Standards:
ing the ductility of a bituminous material measured by the
C670 Practice for Preparing Precision and Bias Statements
distance to which it will elongate before breaking when two
for Test Methods for Construction Materials
ends of a briquet specimen of the material, of the form
D5 Test Method for Penetration of Bituminous Materials
described in Section 4, are pulled apart at a specified speed and
D1754 Test Method for Effects of Heat andAir onAsphaltic
at a specified temperature. Unless otherwise specified, the test
Materials (Thin-Film Oven Test)
shall be made at a temperature of 25 6 0.5°C and with a speed
D2872 Test Method for Effect of Heat andAir on a Moving
of 5 cm/min 6 5.0 %. At other temperatures the speed should
Film of Asphalt (Rolling Thin-Film Oven Test)
be specified.
E1 Specification for ASTM Liquid-in-Glass Thermometers
E11 Specification for Woven Wire Test Sieve Cloth and Test
1.2 Because of the large number of methods for obtaining
Sieves
testsamples,itisimpracticaltodiscussspecificproductsinthis
E77 Test Method for Inspection and Verification of Ther-
test method. Refer to individual product specifications for
mometers
guidance in obtaining a test sample.
E220 Test Method for Calibration of Thermocouples By
1.3 The values stated in SI units are to be regarded as the
Comparison Techniques
standard. Values in parenthesis in inch-pound units are pro-
E644 Test Methods for Testing Industrial Resistance Ther-
vided for informational purposes only.
mometers
1.4 Warning—Mercury has been designated by EPA and
many state agencies as a hazardous material that can cause
3. Significance and Use
central nervous system, kidney and liver damage. Mercury, or
3.1 This test method provides one measure of tensile prop-
its vapor, may be hazardous to health and corrosive to
erties of bituminous materials and may be used to measure
materials. Caution should be taken when handling mercury and
ductility for specification requirements.
mercury containing products. See the applicable product Ma-
terial Safety Data Sheet (MSDS) for details and EPA’s website
4. Apparatus
(http://www.epa.gov/mercury/faq.htm) for additional informa-
tion. Users should be aware that selling mercury or mercury
4.1 Mold—Themoldshallbesimilarindesigntothatshown
containingproducts,orboth,inyourstatemaybeprohibitedby
in Fig. 1. The mold shall be made of brass, 10.0 6 0.1 mm
state law.
thick, the ends b and b' being known as clips, and the parts a
and a' as sides of the mold, with a brass base plate that is larger
1.5 This standard does not purport to address all of the
than the assembled mold. The dimensions of the assembled
safety concerns, if any, associated with its use. It is the
moldshallbeasshowninFig.1withthepermissiblevariations
responsibility of the user of this standard to establish appro-
indicated.
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
4.2 Water Bath for Conditioning Specimens—A water bath
capable of maintaining the specified test temperature, varying
1
This test method is under the jurisdiction of ASTM Committee D04 on Road
and Paving Materials and is the direct responsibility of Subcommittee D04.44 on
2
Rheological Tests. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Dec. 1, 2007. Published January 2008. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1921. Last previous edition approved in 1999 as D113 – 99. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/D0113-07. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D113 − 07
A—Distance between centers, 111.5 to 113.5 mm.
B—Total length of briquet, 74.5 to 75.5 mm.
C—Distance between clips, 29.7 to 30.3 mm.
D—Shoulder, 6.8 to 7.2 mm.
E—Radius, 15.75 to 16.25 mm.
F—Width at minimum cross section, 9.9 to 10.1 mm.
G—Width at mouth of clip, 19.8 to 20.2 mm.
H—Dist
...
This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
American Association State
Designation:D113–99 Designation: D 113 – 07 Highway and Transportation Officials Standard
AASHTO No.: T51
Standard Test Method for
1
Ductility of Bituminous Materials
This standard is issued under the fixed designation D 113; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope
1.1The ductility of a bituminous material is measured by the distance to which it will elongate before breaking when two ends
of a briquet specimen of the material, of the form described in Section 4, are pulled apart at a specified speed and at a specified
temperature. Unless otherwise specified, the test shall be made at a temperature of 25 6 0.5°C and with a speed of 5 cm/min 6
5.0%. At other temperatures the speed should be specified.
1.2
1.1 This test method describes the procedure for determining the ductility of a bituminous material measured by the distance
to which it will elongate before breaking when two ends of a briquet specimen of the material, of the form described in Section
4, are pulled apart at a specified speed and at a specified temperature. Unless otherwise specified, the test shall be made at a
temperature of 25 6 0.5°C and with a speed of 5 cm/min 6 5.0 %. At other temperatures the speed should be specified.
1.2 Because of the large number of methods for obtaining test samples, it is impractical to discuss specific products in this test
method. Refer to individual product specifications for guidance in obtaining a test sample.
1.3 The values stated in SI units are to be regarded as the standard. Values in parenthesis in inch-pound units are provided for
informational purposes only.
1.4 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central
nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution
should be taken when handling mercury and mercury containing products. See the applicable product Material Safety Data Sheet
(MSDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware
that selling mercury or mercury containing products, or both, in your state may be prohibited by state law.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
C 670 Practice for Preparing Precision and Bias Statements for Test Methods for Construction Materials
D 5 Test Method for Penetration of Bituminous Materials
D 1754 Test Method for Effects of Heat and Air on Asphaltic Materials (Thin-Film Oven Test)
D 2872 Test Method for Effect of Heat and Air on a Moving Film of Asphalt (Rolling Thin-Film Oven Test)
E 1 Specification for ASTM Liquid-in-Glass Thermometers
E 11Specification for Wire-Cloth Sieves for Testing Purposes Specification for Wire Cloth and Sieves for Testing Purposes
E 77 Test Method for Inspection and Verification of Thermometers
E 220 Test Method for Calibration of Thermocouples By Comparison Techniques
E 644 Test Methods for Testing Industrial Resistance Thermometers
3. Significance and Use
3.1 This test method provides one measure of tensile properties of bituminous materials and may be used to measure ductility
for specification requirements.
1
This test method is under the jurisdiction of ASTM Committee D-4D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.44 on
Rheological Tests.
Current edition approved Jan. 10, 1999.Dec. 1, 2007. Published May 1999.January 2008. Originally published as D113–21T.approved in 1921. Last previous edition
D113–86(1992).approved in 1999 as D 113 – 99.
2
Annual Book of ASTM Standards, Vol 04.02.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Consho
...
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