ASTM D4525-08
(Test Method)Standard Test Method for Permeability of Rocks by Flowing Air
Standard Test Method for Permeability of Rocks by Flowing Air
SIGNIFICANCE AND USE
This test method is designed to measure the permeability to air of a small sample of rock. By extrapolation, this test method also determines an equivalent of the liquid permeability. This parameter is used to calculate the flow through rock of fluids subjected to a pressure differential.
Note 1—Notwithstanding the statements on precision and bias contained in this test method, the measures of precision of this test method is dependent on the competence of the personnel performing them, and on the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D 3740 are generally considered capable of competent and objective testing. Users of this test method are cautioned that compliance with Practice D 3740 does not in itself assure reliable testing. Reliable testing depends on many factors; Practice D 3740 provides a means for evaluating some of those factors.
SCOPE
1.1 This test method covers the determination of the coefficient of specific permeability for the flow of air through rocks. The procedure establishes representative values of the coefficient of permeability of rocks or well-indurated soils.
1.2 This test method is limited to permeability values greater than 0.9869 pm2 (1.0 picodarcy), and is limited to rocks free of oil or unctuous matter.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D4525 − 08
StandardTest Method for
1
Permeability of Rocks by Flowing Air
This standard is issued under the fixed designation D4525; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* 4. Summary of Test Method
1.1 This test method covers the determination of the coef- 4.1 The permeability of a rock sample is measured by
ficient of specific permeability for the flow of air through flowing dry air through the specimen and measuring the
rocks. The procedure establishes representative values of the absolute pressure, the flow rate, and absolute pressure differ-
coefficient of permeability of rocks or well-indurated soils. ential of the air. Three or more tests are performed on a sample
at different mean air pressure values. The permeability values
1.2 This test method is limited to permeability values
2 are plotted as a function of the reciprocal mean absolute
greater than 0.9869 pm (1.0 picodarcy), and is limited to rocks
pressure; those points lying on a straight line are extrapolated
free of oil or unctuous matter.
to a value corresponding to an infinite mean air pressure to
1.3 The values stated in SI units are to be regarded as the
obtain an equivalent permeability value for liquids.
standard. The values given in parentheses are mathematical
5. Significance and Use
conversions to inch-pound units that are provided for informa-
tion only and are not considered standard.
5.1 This test method is designed to measure the permeabil-
1.4 This standard does not purport to address all of the ity to air of a small sample of rock. By extrapolation, this test
safety concerns, if any, associated with its use. It is the
method also determines an equivalent of the liquid permeabil-
responsibility of the user of this standard to establish appro- ity.This parameter is used to calculate the flow through rock of
priate safety and health practices and determine the applica-
fluids subjected to a pressure differential.
bility of regulatory limitations prior to use.
NOTE 1—Notwithstanding the statements on precision and bias con-
tained in this test method, the measures of precision of this test method is
2. Referenced Documents
dependent on the competence of the personnel performing them, and on
2 the suitability of the equipment and facilities used.Agencies that meet the
2.1 ASTM Standards:
criteria of Practice D3740 are generally considered capable of competent
D653 Terminology Relating to Soil, Rock, and Contained
and objective testing. Users of this test method are cautioned that
Fluids
compliance with Practice D3740 does not in itself assure reliable testing.
D3740 Practice for Minimum Requirements for Agencies Reliable testing depends on many factors; Practice D3740 provides a
means for evaluating some of those factors.
Engaged in Testing and/or Inspection of Soil and Rock as
Used in Engineering Design and Construction
6. Apparatus
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2.2 American Petroleum Institute Standard:
6.1 Permeameter—The permeameter shall have a specimen
RP-40 Recommended Practice for Core Analysis Procedure
holder; a pressure transducer or gauge, or manometers, for
measuring the air pressure differential across the ends of the
3. Terminology
specimen; a means for measuring the flow rate of the air; and
3.1 For terminology used in this test method, refer to
a means for providing dry air to the flow stream (see Fig. 1).
Terminology D653.
6.1.1 Specimen Holder—The specimen holder shall have a
diameterofatleasttentimesthediameterofthelargestparticle
of the specimen. Where suitable, the preferred diameter is 2.54
1 cm. The entrance and exit flow ports shall be sufficiently large
This test method is under the jurisdiction ofASTM Committee D18 on Soil and
Rock and is the direct responsibility of Subcommittee D18.12 on Rock Mechanics.
to prevent pressure loss at maximum flow rate.The length shall
Current edition approved July 1, 2008. Published July 2008. Originally approved
be 1.3 to 1.7 times the diameter.
in 1985. Last previous edition approved in 2004 as D4525 – 04. DOI: 10.1520/
6.1.2 PreferredApparatus—Inthepreferredform,thespeci-
D4525-08.
2
men holder shall be an elastomer sleeve and have means for
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
confining the sleeve and compressing it against the specimen
Standards volume information, refer to the standard’s Document Summary page on
so as to prevent bypassing of air under pressure between the
the ASTM website.
3
sleeve and the specimen. The holder shall also have a means
Available fr
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This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
ϵ1
Designation:D 4525–90(Reapproved 1995) Designation: D4525 – 08
Standard Test Method for
1
Permeability of Rocks by Flowing Air
This standard is issued under the fixed designation D4525; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
1
superscript epsilon (ϵ) indicates an editorial change since the last revision or reapproval. ϵ NOTE—Section 12 was changed editorially
in December 1991.
1. Scope*
1.1 This test method covers the determination of the coefficient of specific permeability for the flow of air through rocks. The
procedure is to establish establishes representative values of the coefficient of permeability of rocks or well-indurated soils.
2
1.2 This test method is limited to permeability values greater than 0.9869 nmpm (1.0 microdarcy), and is limited to rocks free
of oil or unctuous matter.
1.3The values stated in SI units are to be regarded as the standard. (1.0 picodarcy), and is limited to rocks free of oil or unctuous
matter.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are mathematical
conversions to inch-pound units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
D2434Test Method for Permeability of Granular Soils (Constant Head)
2 2
D3877Test Methods for One-Dimensional Expansion, Shrinkage, and Uplift Pressure of Soil-Lime Mixtures
D653 Terminology Relating to Soil, Rock, and Contained Fluids
D3740 Practice for Minimum Requirements for Agencies Engaged in Testing and/or Inspection of Soil and Rock as Used in
Engineering Design and Construction
2.2 American Petroleum Institute Standards:
3
RP-27Recommended Practice for Determining Permeability of Porous MediaAmerican Petroleum Institute Standard:
RP-40 Recommended Practice for Core Analysis Procedure
3. Summary of Test Method
3.1The permeability of a rock sample is measured by flowing dry air through the specimen and measuring the pressure, the flow
rate, and pressure differential of the air. Three or more tests are performed on a sample at different mean air pressure values. The
permeability values are plotted as a function of the reciprocal mean pressure; those points lying on a straight line are extrapolated
to a value corresponding to an infinite mean air pressure to obtain an equivalent permeability value for liquids. Terminology
3.1 For terminology used in this test method, refer to Terminology D653.
4. Significance and Use
4.1This test method is designed to measure the permeability to air of a small sample of rock. By extrapolation, this test method
also determines an equivalent of the liquid permeability. This parameter is used to calculate the flow through rock of fluids
subjected to a pressure differential. Summary of Test Method
4.1 Thepermeabilityofarocksampleismeasuredbyflowingdryairthroughthespecimenandmeasuringtheabsolutepressure,
the flow rate, and absolute pressure differential of the air. Three or more tests are performed on a sample at different mean air
1
This test method is under the jurisdiction ofASTM Committee D-18D18 on Soil and Rock and is the direct responsibility of Subcommittee D18.12 on Rock Mechanics.
Current edition approved May 25, 1990. Published July 1990. Originally published as D 4525–85. Last previous edition D 4525–85.
Current edition approved July 1, 2008. Published July 2008. Originally approved in 1985. Last previous edition approved in 2004 as D4525 – 04. DOI: 10.1520/D4525-08.
2
Annual Book of ASTM Standards, Vol 04.08.
2
ForreferencedASTMstandards,visittheASTMwebsite,www.astm.org,orcontactASTMCustomerServiceatservice@astm.org.ForAnnualBookofASTMStandards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from American Petroleum Institute, 2101 L St., NW, Washington, DC 20037.
3
Available from American Petroleum Institute (API), 1220 L. St., NW, Washington, DC 20005-4070, http://www.api.org.
*A Summary of Changes section appears at the end of this standard.
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