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ASTM D6565-00(2005)

(Test Method)

Standard Test Method for Determination of Water (Moisture) Content of Soil by the Time-Domain Reflectometry (TDR) Method (Withdrawn 2014)

Standard Test Method for Determination of Water (Moisture) Content of Soil by the Time-Domain Reflectometry (TDR) Method (Withdrawn 2014)

SIGNIFICANCE AND USE
The determination of the water-content, or moisture content, of soil is one of the fundamental needs in the soil physics and hydrology disciplines. The need arises from requirements for defining the optimal time for irrigation, the infiltration rate, the soil-moisture flux, contaminant transport rates, and evaluating the potential for leakage from a waste site or a surface or subsurface barrier.
The TDR application covered in this test method is that used for point measurements of moisture content in soil. The application is either through manual insertion into the soil or by burying a probe in the subsurface to acquire moisture content data at a specific location. In addition, core samples may be tested with TDR at a drill site to acquire real-time soil moisture data.
SCOPE
1.1 This test method covers the determination of water content (or moisture content) in soil by the use of the electromagnetic technique called Time-Domain Reflectometry (TDR).
1.2 This test method was written to detail the procedure for conventional TDR measurements of soil. Other TDR applications exist for the purpose of quantifying water content in soil and are not covered here, such as flat probe technologies and wetting front advance methods.
1.3 Commercial TDR applications exist which automate the TDR methodology and are not detailed in this test method. It is likely that overlap exists in the automated commercial systems versus this applied method, and the user is encouraged to adhere to this test method when applicable.
1.4 This test method is one of a series on vadose zone characterization methods. Other standards have been prepared on vadose zone characterization techniques.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
WITHDRAWN RATIONALE
This test method covered the determination of water content (or moisture content) in soil by the use of the electromagnetic technique called Time-Domain Reflectometry (TDR).
Formerly under the jurisdiction of Committee D18 on Soil and Rock, this test method was withdrawn in July 2014 in accordance with section 10.6.3 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

General Information

Status
Withdrawn
Publication Date
31-Oct-2005
Withdrawal Date
14-Jul-2014
ICS
13.080.40 - Hydrological properties of soils
Technical Committee
D18 - Soil and Rock
Drafting Committee
D18.21 - Groundwater and Vadose Zone Investigations
Current Stage
Ref Project

Relations

Replaces
ASTM D6565-00 - Standard Test Method for Determination of Water (Moisture) Content of Soil by the Time-Domain Reflectometry (TDR) Method
Effective Date
01-Nov-2005

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ASTM D6565-00(2005) - Standard Test Method for Determination of Water (Moisture) Content of Soil by the Time-Domain Reflectometry (TDR) Method (Withdrawn 2014)ASTM D6565-00(2005) - Standard Test Method for Determination of Water (Moisture) Content of Soil by the Time-Domain Reflectometry (TDR) Method (Withdrawn 2014)
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ASTM D6565-00(2005) - Standard Test Method for Determination of Water (Moisture) Content of Soil by the Time-Domain Reflectometry (TDR) Method (Withdrawn 2014)
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D6565 −00(Reapproved 2005)
Standard Test Method for
Determination of Water (Moisture) Content of Soil by the
1
Time-Domain Reflectometry (TDR) Method
This standard is issued under the fixed designation D6565; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope (Moisture) Content of Soil and Rock by Mass
D4643 Test Method for Determination of Water (Moisture)
1.1 This test method covers the determination of water
Content of Soil by Microwave Oven Heating
content (or moisture content) in soil by the use of the
D4700 Guide for Soil Sampling from the Vadose Zone
electromagnetic technique called Time-Domain Reflectometry
D4944 TestMethodforFieldDeterminationofWater(Mois-
(TDR).
ture)ContentofSoilbytheCalciumCarbideGasPressure
1.2 This test method was written to detail the procedure for
Tester
conventional TDR measurements of soil. Other TDR applica-
D5220 Test Method for Water Mass per Unit Volume of Soil
tions exist for the purpose of quantifying water content in soil
and Rock In-Place by the Neutron Depth Probe Method
and are not covered here, such as flat probe technologies and
wetting front advance methods.
3. Terminology
1.3 Commercial TDR applications exist which automate the 3.1 Definitions:
TDR methodology and are not detailed in this test method. It is
3.1.1 time domain reflectometry (TDR)—an electromagnetic
likely that overlap exists in the automated commercial systems method used in the determination of water content of soil.
versus this applied method, and the user is encouraged to
3.1.2 Definitions of other terminology used in this guide
adhere to this test method when applicable.
may be found in Terminology D653.
1.4 This test method is one of a series on vadose zone
4. Summary of Test Method
characterization methods. Other standards have been prepared
on vadose zone characterization techniques.
4.1 Aspeciallyconstructed,multi-wave-guideTDRprobeis
inserted into the soil. The electronic cable tester (or automated
1.5 This standard does not purport to address all of the
commercial TDR electronics) is used to send a pulsed wave-
safety concerns, if any, associated with its use. It is the
form to the probe.The cable tester then receives a return signal
responsibility of the user of this standard to establish appro-
which was influenced by the dielectric constant of the soil,
priate safety and health practices and determine the applica-
which in turn is a function of water content.An analysis of the
bility of regulatory limitations prior to use.
waveform trace supplies the necessary information to calculate
2. Referenced Documents the water content of the soil.
2
2.1 ASTM Standards:
5. Significance and Use
D653 Terminology Relating to Soil, Rock, and Contained
5.1 The determination of the water-content, or moisture
Fluids
content, of soil is one of the fundamental needs in the soil
D1452 Practice for Soil Exploration and Sampling byAuger
physics and hydrology disciplines. The need arises from
Borings
requirements for defining the optimal time for irrigation, the
D2216 Test Methods for Laboratory Determination of Water
infiltration rate, the soil-moisture flux, contaminant transport
rates, and evaluating the potential for leakage from a waste site
or a surface or subsurface barrier.
1
This test method is under the jurisdiction ofASTM Committee D18 on Soil and
Rock and is the direct responsibility of Subcommittee D18.21.02 on Vadose Zone
5.2 The TDR application covered in this test method is that
Monitoring.
used for point measurements of moisture content in soil. The
Current edition approved Nov. 1, 2005. Published December 2005. Originally
applicationiseitherthroughmanualinsertionintothesoilorby
approved in 2000. Last previous edition approved in 2000 as D6565 – 00. DOI:
10.1520/D6565-00R05.
burying a probe in the subsurface to acquire moisture content
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
data at a specific location. In addition, core samples may be
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
tested withTDR at a drill site to acquire real-time soil moisture
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. data.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D6565−00 (2005)
Fig. 1(a ) Properly installed probe Fig. 1(b) Improperly installed probe
FIG. 1Properly and Improperly Installed TDR Probes
6. Interferences 6.5 A static charge on the coaxial cab
...

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1.1 This test method outlines procedures for determining the water (moisture) content of soil by chemical reaction using calcium carbide as a reagent to react with the available water in the soil producing a gas. A measurement is made of the gas pressure produced when a specified mass of wet or moist soil is placed in a testing device with an appropriate volume of reagent and mixed.  
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1.1 This test method outlines procedures for determining the water content of soils by incrementally drying soil in a microwave oven.  
1.2 This test method can be used as a substitute for Test Method D2216 when more rapid results are desired to expedite other phases of testing and slightly less accurate results are acceptable.  
1.3 When questions of accuracy between this test method and Test Method D2216 arise, Test Method D2216 shall be the referee method.  
1.4 This test method is applicable for most soil types. For some soils, such as those containing significant amounts of halloysite, mica, montmorillonite, gypsum or other hydrated materials, highly organic soils, or soils in which the pore water contains significant amounts of dissolved solids (such as salt in the case of marine deposits), this test method may not yield reliable water content values due to the potential for heating above 110°C or lack of means to account for the presence of precipitated solids that were previously dissolved.  
1.5 The values stated in SI units are to be regarded as the standard. Performance of the test method utilizing another system of units shall not be considered non-conformance. The sieve designations are identified using the “standard” system in accordance with Specification E11, such as 2.0-mm and 19-mm, followed by the “alternative” system of No. 10 and 3/4-in., respectively, in parentheses.  
1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless otherwise superseded by this standard.  
1.6.1 The procedures used to specify how data are collected/recorded or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies...

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ASTM
ASTM D6836-16(Test Method)
Standard Test Methods for Determination of the Soil Water Characteristic Curve for Desorption Using Hanging Column, Pressure Extractor, Chilled Mirror Hygrometer, or Centrifuge

SIGNIFICANCE AND USE
5.1 The soil water characteristic curve (SWCC) is fundamental to hydrological characterization of unsaturated soils and is required for most analyses of water movement in unsaturated soils. The SWCC is also used in characterizing the shear strength and compressibility of unsaturated soils. The unsaturated hydraulic conductivity of soil is often estimated using properties of the SWCC and the saturated hydraulic conductivity.  
5.2 This method applies only to soils containing two pore fluids: a gas and a liquid. The liquid is usually water and the gas is usually air. Other liquids may also be used, but caution must be exercised if the liquid being used causes excessive shrinkage or swelling of the soil matrix.  
5.3 A full investigation has not been conducted regarding the correlation between soil water characteristic curves obtained using this method and soil water characteristics curves of in-place materials. Thus, results obtained from this method should be applied to field situations with caution and by qualified personnel.
Note 1: The quality of the result produced by this standard depends on the competence of the personnel performing the test and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors. Practice D3740 provides a means of evaluating some of these factors.
SCOPE
1.1 These test methods cover the determination of soil water characteristic curves (SWCCs) for desorption (drying). SWCCs describe the relationship between suction and volumetric water content, gravimetric water content, or degree of water saturation. SWCCs are also referred to as soil water retention curves, soil water release curves, or capillary pressure curves.  
1.2 This standard describes five methods (A-E) for determining the soil water characteristic curve. Method A (hanging column) is suitable for making determinations for suctions in the range of 0 to 80 kPa. Method B (pressure chamber with volumetric measurement) and Method C (pressure chamber with gravimetric measurement) are suitable for suctions in the range of 0 to 1500 kPa. Method D (chilled mirror hygrometer) is suitable for making determinations for suctions in the range of 500 kPa to 100 MPa. Method E (centrifuge method) is suitable for making determinations in the range 0 to 120 kPa. Method A typically is used for coarse soils with little fines that drain readily. Methods B and C typically are used for finer soils, which retain water more tightly. Method D is used when suctions near saturation are not required and commonly is employed to define the dry end of the soil water characteristic curve (that is, water contents corresponding to suctions >1000 kPa). Method E is typically used for coarser soils where an appreciable amount of water can be extracted with suctions up to 120 kPa. The methods may be combined to provide a detailed description of the soil water characteristic curve. In this application, Method A or E is used to define the soil water characteristic curve at lower suctions (0 to 80 kPa for A, 0 to 120 kPa for E) near saturation and to accurately identify the air entry suction, Method B or C is used to define the soil water characteristic curve for intermediate water contents and suctions (100 to 1000 kPa), and Method D is used to define the soil water characteristic curves at low water contents and higher suctions (>1000 kPa).  
1.3 All observed and calculated values shall conform to the guide for significant digits and rounding established in Practice D6026. The procedures in Practice D6026 that are used to specify how data are collected, recorded, and calculated are regarded as the industry standard. In addition, they are represe...

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ASTM
ASTM D8037/D8037M-16(Practice)
Standard Practice for Direct Push Hydraulic Logging for Profiling Variations of Permeability in Soils

SIGNIFICANCE AND USE
5.1 The injection logging system provides a rapid and efficient way to ascertain the pressure required to inject water into unconsolidated formations at the given flow rate in real time (Fig. 1) (1-4, 7).5 The measured injection pressure and flow rate are then used to assess variations in formation permeability versus depth and infer changes in formation lithology and understand the local hydrostratigraphy (1-4, 8-16). Log interpretation should be confirmed with targeted soil coring adjacent to selected log locations or running logs adjacent to one or more previously logged borings. Practice D3740 was developed for agencies engaged in the testing and/or inspection of soils and rock. As such, it is not totally applicable to agencies performing this practice. However, users of this practice should recognize that the framework of Practice D3740 is appropriate for evaluating the quality of an agency performing this practice. Currently there is no known qualifying national authority that inspects agencies that perform this practice.
SCOPE
1.1 This practice describes a method for rapid delineation of variations in formation permeability in the subsurface using an injection logging tool. Clean water is injected from a port on the side of the probe as it is advanced at approximately 2cm/s into virgin soils. Logging with the injection tool is typically performed with direct push equipment, however other drilling machines may be modified to run the logs by direct push methods (for example, addition of a suitable hammer and/or hydraulic ram systems). Injection logs exceeding 100 ft [30m] depth have been obtained. Direct push methods are not intended to penetrate consolidated rock and may encounter refusal in very dense formations or when cobbles or boulders are encountered in the subsurface. However, injection logging has been performed in some semi-consolidated or soft formations.  
1.2 This standard practice describes how to obtain a real time vertical log of injection pressure and flow rate with depth. The data obtained is indicative of the variations of permeability in the subsurface and is typically used to infer formation lithology. The person(s) responsible for review, interpretation and application of the injection logging data should be familiar with the logging technique as well as the soils, geology and hydrogeology of the area under investigation.  
1.3 The injection logging system may be operated with a built in electrical conductivity sensor to provide additional real time information on stratigraphy and is essential for targeting test zones. Other sensors, such as fluorescence detectors (Practice D6187), a membrane interface probe (Practice D7352) or a cone penetration tool (Test Method D5778) may be used in conjunction with injection logging to provide additional information. The use of the injection logging tool in concert with an electrical conductivity array or cone penetration tool is highly recommended (although not mandatory) to further define hydrostratigraphic conditions, such as migration pathways, low permeability zones (for example, aquitards) and to guide confirmation sampling. The EC log and injection pressure log may be compared in some settings to identify the presence of ionic contaminants or ionic injectates used for remediation.  
1.4 The injection logging system does not provide quantitative permeability or hydraulic conductivity information. However, injection pressure and flow data may be used to provide a qualitative indication of formation permeability. Semi-quantitative values of permeability may be obtained by correlation of injection logging data with other methods (1-4).2 Also, a log of estimated hydraulic conductivity (5) may be calculated for the saturated zone using an empirical model included in some versions of the log viewing software. The data allows for estimates of hydraulic conductivity (K) at the inch-scale using the corrected injection pressure ...

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ASTM
ASTM D4959-16(Test Method)
Standard Test Method for Determination of Water Content of Soil By Direct Heating

SIGNIFICANCE AND USE
5.1 The water content of a soil is used throughout geotechnical engineering practice both in the laboratory and in the field. The use of Test Methods D2216 for water content determination can be time consuming and there are occasions when a more expedient method is desirable. Drying by direct heating is one such method. Results of this test method have been demonstrated to be of satisfactory accuracy for use in field control work, such as in the determination of water content, and in the determination of in-place dry unit weight of soils.  
5.2 The principal objection to the use of the direct heating for water content determination is the possibility of overheating the soil, thereby yielding a water content higher than would be determined by Test Methods D2216. While not eliminating this possibility, the incremental drying procedure in this test method will minimize its effects. Some heat sources have settings or controls that can also be used to reduce overheating. Loose fitting covers or enclosures can also be used to reduce overheating while assisting in uniform heat distribution.  
5.3 The behavior of a soil when subjected to direct heating is dependent on its mineralogical composition, and as a result, no one procedure is applicable for all types of soils or heat sources. The general procedure of this test method applies to all soils, but test details may need to be tailored to the soil being tested.  
5.4 When this test method is to be used repeatedly on the same or similar soil from a given site, a correction factor can usually be determined by making several comparisons between the results of this test method and Test Methods D2216. A correction factor is valid when the difference is consistent for several comparisons, and is reconfirmed on a regular specified basis.  
5.5 This test method may not be appropriate when precise results are required, or when minor variations in water content will affect the results of other test methods, such as borderline s...
SCOPE
1.1 This test method covers procedures for determining the water content of soils by drying with direct heat, such as using a hotplate, stove, blowtorch, and the like.  
1.2 This test method can be used as a substitute for Test Methods D2216 when more rapid results are desired to expedite other phases of testing and slightly less accurate results are acceptable.  
1.3 When questions of accuracy between this test method and Test Methods D2216 arise, Test Methods D2216 shall be the referee method.  
1.4 This test method is applicable for most soil types. For some soils, such as those containing significant amounts of halloysite, mica, montmorillonite, gypsum, or other hydrated materials, highly organic soils or soils that contain dissolved solids, (such as salt in the case of marine deposits), this test method may not yield reliable water content values due to the potential for heating above 110°C or lack of means to account for the presence of precipitated solids that were previously dissolved.  
1.5 The values stated in SI units are to be regarded as standard. Performance of the test method utilizing another system of units shall not be considered non-conformance. The sieve designations are identified using the “standard” system in accordance with Specification E11, such as 2.0-mm and 19-mm, followed by the “alternative” system of No. 10 and 3/4-in., respectively, in parentheses.  
1.6 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in D6026, unless otherwise superseded by this standard.  
1.6.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any consider...

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