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ASTM D7928-21e1

(Test Method)

Standard Test Method for Particle-Size Distribution (Gradation) of Fine-Grained Soils Using the Sedimentation (Hydrometer) Analysis

Standard Test Method for Particle-Size Distribution (Gradation) of Fine-Grained Soils Using the Sedimentation (Hydrometer) Analysis

SIGNIFICANCE AND USE
5.1 Particle-size distribution (gradation) is a descriptive term referring to the proportions by dry mass of a soil distributed over specified particle-size ranges. The gradation curve generated using this method yields the distribution of silt and clay size fractions present in the soil based on size definitions, not mineralogy or Atterberg limit classification.  
5.2 Unless the sedimentation sample is representative of the entire sample, the sedimentation results must be combined with a sieve analysis to obtain the complete particle size distribution.  
5.3 The clay size fraction is material finer than 2 µm. The clay size fraction is used in combination with the Plasticity Index (Test Methods D4318) to compute the activity, which provides an indication of the mineralogy of the clay fraction.  
5.4 The gradation of the silt and clay size fractions is an important factor in determining the susceptibility of fine-grained soils to frost action.  
5.5 The gradation of a soil is an indicator of engineering properties such as hydraulic conductivity, compressibility, and shear strength. However, soil behavior for engineering and other purposes is dependent upon many factors, such as effective stress, mineral type, structure, plasticity, and geological origin, and cannot be based solely upon gradation.  
5.6 Some types of soil require special treatment in order to correctly determine the particle sizes. For example, chemical cementing agents can bond clay particles together and should be treated in an effort to remove the cementing agents when possible. Hydrogen peroxide and moderate heat can digest organics. Hydrochloric acid can remove carbonates by washing and Dithionite-Citrate-Bicarbonate extraction can be used to remove iron oxides. Leaching with test water can be used to reduce salt concentration. All of these treatments, however, add significant time and effort when performing the sedimentation test and are allowable but outside the scope of this test method. ...
SCOPE
1.1 This test method covers the quantitative determination of the distribution of particle sizes of the fine-grained portion of soils. The sedimentation by hydrometer method is used to determine the particle-size distribution (gradation) of the material that is finer than the No. 200 (75-µm) sieve and larger than about 0.2-µm. The test is performed on material passing the No. 10 (2.0-mm) or finer sieve and the results are presented as the mass percent finer of this fraction versus the log of the particle diameter.  
1.2 This method can be used to evaluate the fine-grained fraction of a soil with a wide range of particle sizes by combining the sedimentation results with results from a sieve analysis using D6913 to obtain the complete gradation curve. The method can also be used when there are no coarse-grained particles or when the gradation of the coarse-grained material is not required or not needed.
Note 1: The significant digits recorded in this test method preclude obtaining the grain size distribution of materials that do not contain a significant amount of fines. For example, clean sands will not yield detectable amounts of silt and clay sized particles, and therefore should not be tested with this method. The minimum amount of fines in the sedimentation specimen is 15 g.  
1.3 When combining the results of the sedimentation and sieve tests, the procedure for obtaining the material for the sedimentation analysis and calculations for combining the results will be provided by the more general test method, such as Test Methods D6913 (Note 2).
Note 2: Subcommittee D18.03 is currently developing a new test method “Test Method for Particle-Size Analysis of Soils Combining the Sieve and Sedimentation Techniques.”  
1.4 The terms “soil” and “material” are used interchangeably throughout the standard.  
1.5 The sedimentation analysis is based on the concept that larger particles will fall through a fluid faster than...

General Information

Status
Published
Publication Date
30-Apr-2021
ICS
13.080.20 - Physical properties of soils
Technical Committee
D18 - Soil and Rock
Drafting Committee
D18.03 - Texture, Plasticity and Density Characteristics of Soils
Current Stage
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ASTM D7928-21e1 - Standard Test Method for Particle-Size Distribution (Gradation) of Fine-Grained Soils Using the Sedimentation (Hydrometer) AnalysisASTM D7928-21e1 - Standard Test Method for Particle-Size Distribution (Gradation) of Fine-Grained Soils Using the Sedimentation (Hydrometer) Analysis
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ASTM D7928-21e1 - Standard Test Method for Particle-Size Distribution (Gradation) of Fine-Grained Soils Using the Sedimentation (Hydrometer) Analysis
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
´1
Designation: D7928 − 21
Standard Test Method for
Particle-Size Distribution (Gradation) of Fine-Grained Soils
1
Using the Sedimentation (Hydrometer) Analysis
This standard is issued under the fixed designation D7928; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
ε NOTE—Summary of Changes section was editorially added in June 2021.
1. Scope* 1.5 The sedimentation analysis is based on the concept that
larger particles will fall through a fluid faster than smaller
1.1 This test method covers the quantitative determination
particles. Stokes’ Law gives a governing equation used to
of the distribution of particle sizes of the fine-grained portion
determine the terminal velocity of a spherical particle falling
of soils. The sedimentation by hydrometer method is used to
through a stationary liquid. The terminal velocity is propor-
determine the particle-size distribution (gradation) of the
tionaltothesquareoftheparticlediameter.Therefore,particles
material that is finer than the No. 200 (75-µm) sieve and larger
are sorted by size in both time and position when settling in a
than about 0.2-µm. The test is performed on material passing
container of liquid.
theNo.10(2.0-mm)orfinersieveandtheresultsarepresented
1.5.1 Stokes’ Law has several assumptions which are: the
as the mass percent finer of this fraction versus the log of the
particles are spherical and smooth; there is no interference
particle diameter.
between the particles; there is no difference between the
1.2 This method can be used to evaluate the fine-grained
current in the middle of the container and the sides; flow is
fraction of a soil with a wide range of particle sizes by
laminar; and the particles have the same density. These
combining the sedimentation results with results from a sieve
assumptions are applied to soil particles of various shapes and
analysis using D6913 to obtain the complete gradation curve.
sizes.
The method can also be used when there are no coarse-grained
1.6 A hydrometer is used to measure the fluid density and
particles or when the gradation of the coarse-grained material
determine the quantity of particles in suspension at a specific
is not required or not needed.
time and position. The density of the soil-water suspension
NOTE 1—The significant digits recorded in this test method preclude
depends upon the concentration and specific gravity of the soil
obtaining the grain size distribution of materials that do not contain a
particlesandtheamountofdispersantadded.Eachhydrometer
significant amount of fines. For example, clean sands will not yield
measurement at an elapsed time is used to calculate the
detectable amounts of silt and clay sized particles, and therefore should
not be tested with this method. The minimum amount of fines in the percentageofparticlesfinerthanthediametergivenbyStokes’
sedimentation specimen is 15 g.
Law.Theseriesofreadingsprovidethedistributionofmaterial
mass as a function of particle size.
1.3 When combining the results of the sedimentation and
sieve tests, the procedure for obtaining the material for the
1.7 This test method does not cover procurement of the
sedimentation analysis and calculations for combining the
sample or processing of the sample prior to obtaining the
results will be provided by the more general test method, such
reduced sample in any detail. It is assumed that the sample is
as Test Methods D6913 (Note 2).
obtained using appropriate methods and is representative of
site materials or conditions. It is also assumed that the sample
NOTE 2—Subcommittee D18.03 is currently developing a new test
method “Test Method for Particle-Size Analysis of Soils Combining the has been processed such that the reduced sample accurately
Sieve and Sedimentation Techniques.”
reflects the particle-size distribution (gradation) of this finer
fraction of the material.
1.4 The terms “soil” and “material” are used interchange-
ably throughout the standard.
1.8 Material Processing—Material is tested in the moist or
as-received state unless the material is received in an air-dried
state. The moist preparation method shall be used to obtain a
1
sedimentation test specimen from the reduced sample. Air-
ThistestmethodisunderthejurisdictionofASTMCommitteeD18onSoiland
Rock andisthedirectresponsibilityofSubcommitteeD18.03onTexture, Plasticity
driedpreparationisonlyallowedwhenthematerialisreceived
and Density Characteristics of Soils.
in the air-dried state. The met
...

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SIGNIFICANCE AND USE
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1.1.1 For limitations see Section 5 on Interferences.  
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5.1 The ring shear test is suited to the relatively rapid determination of drained residual shear strength because of the short drainage path through the thin specimen, the constant cross-sectional area of the shear surface during shear, unlimited rotational displacement in one direction, and the capability of testing one specimen under different effective normal stresses to obtain clay particles that are oriented parallel to the direction of shear to obtain residual shear strength envelope.  
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Standard Test Method for In-Place Density (Unit Weight) and Water Content of Soil Using an Electromagnetic Soil Density Gauge

SIGNIFICANCE AND USE
5.1 The method described determines wet density and gravimetric water content by correlating complex impedance measurement data to an empirically developed model. The empirical model is generated by comparing the electrical properties of typical soils encountered in civil construction projects to their wet densities and gravimetric water contents determined by other accepted methods.  
5.2 The test method described is useful as a rapid, non-destructive technique for determining the in-place total density and gravimetric water content of soil and soil-aggregate mixtures and the determination of dry density.  
5.3 This method may be used for quality control and acceptance of compacted soil and soil-aggregate mixtures as used in construction and also for research and development. The non-destructive nature allows for repetitive measurements at a single test location and statistical analysis of the results.
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Standard Test Method for In-Place Estimation of Density and Water Content of Soil and Aggregate by Correlation with Complex Impedance Method

SIGNIFICANCE AND USE
5.1 CIMI measurements as described in this Standard Test Method are applicable to measurements of compacted soils intended for roads and foundations.  
5.2 The test method is used for estimating in-place values of density and water content of soils and soil-aggregates based on electrical measurements.  
5.3 The test method may be used for quality control and acceptance testing of compacted soil and soil aggregate mixtures as used in construction and also for research and development. The minimal disturbance nature of the methodology allows repetitive measurements in a single test location and statistical analysis of the results.  
5.4 Limitations:  
5.4.1 This test method provides an overview of the CIMI measurement procedure using a controlling console connected to a soil sensor unit which applies a 3.0 MHz RF voltage to an in-place soil via metallic probes that are driven into the soil at a prescribed distance apart. This test method does not discuss the details of the CIMI electronics, computer, or software that utilize on-board algorithms for estimating the soil density and water content  
5.4.2 It is difficult to address an infinite variety of soils in this standard. However, data presented in X3.1 provides a list of soil types that are applicable for the CIMI use.  
5.4.3 The procedures used to specify how data are collected, recorded, or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures prescribed in this standard do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analytical methods for engineering design.
Note 1: Notwithstanding th...
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1.1 Purpose and Application—This test method describes the procedure, equipment, and interpretation methods for estimating in-place soil dry density and water content using a Complex-Impedance Measuring Instrument (CIMI).  
1.1.1 The purpose and application of this test method is for testing porous material such as used in roadway base or building foundations that may be deployed in the field at various test sites. The test apparatus includes electrodes that contact the porous material under test and a sensor unit that supplies electromagnetic signals to the porous material. Response signals reveal electrical parameters such as complex impedance which can be equated to material properties such as density and moisture content.  
1.1.2 CIMI measurements as described in this test method are applicable to measurements of compacted soils intended for roads and foundations.  
1.1.3 This test method describes the procedure for estimating in-place density and water content of soils and soil-aggregates by use of a CIMI. The electrical properties of the soil are measured using a radio frequency (RF) voltage source connected to soil electrical probes driven into the soils and soil-aggregates to be tested, in a prescribed pattern and depth. Certain algorithms of these properties are related to wet density and water content. This correlation between electrical measurements, and density and water content is accomplished using a calibration methodology. In the calibration methodology, density and water content are determined by other ASTM Test Standards that measure soil density and water content, thereafter correlating the corresponding measured electrical properties to the soil physical properties.  
1.2 Units—The values stated in SI units are to be regarded as standard. The inch-pound units given in parentheses are mathematical conversions which are provided for information purposes only and are not considered standard.  
1.2.1...

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ASTM
ASTM D6572-21(Test Method)
Standard Test Methods for Determining Dispersive Characteristics of Clayey Soils by the Crumb Test

SIGNIFICANCE AND USE
5.1 The crumb test provides a simple, quick method for field or laboratory identification of a dispersive clayey soil. The internal erosion failures of a number of homogeneous earth dams, erosion along channel or canal banks, and rainfall erosion of earthen structures have been attributed to colloidal erosion along cracks or other flow channels formed in masses of dispersive clay (5).  
5.2 The crumb test, as originally developed by Emerson (6), was called the aggregate coherence test and had seven different categories of soil-water reactions. Sherard (5) later simplified the test by combining some soil-water reactions so that only four categories, or grades, of soil dispersion are observed during the test. The crumb test is a relatively accurate positive indicator of the presence of dispersive properties in a soil. The crumb test, however, is not a completely reliable negative indicator that soils are not dispersive. The crumb test can seldom be relied upon as a sole test method for determining the presence of dispersive clays. The double-hydrometer test (Test Method D4221) and pinhole test (Test Method D4647/D4647M) are test methods that provide valuable additional insight into the probable dispersive behavior of clay soils.
Note 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depends on several factors; Practice D3740 provides a means of evaluating some of those factors.
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1.1 Two test methods are provided to give a qualitative indication of the natural dispersive characteristics of clayey soils: Method A and Method B.  
1.1.1 Method A—Procedure for Natural Soil Crumbs described in 10.1.  
1.1.2 Method B—Procedure for Remolded Soil Crumbs described in 10.2.  
1.2 The crumb test, while a good, quick indication of dispersive soil, should usually be run in conjunction with a pinhole test and a double hydrometer test, Test Methods D4647/D4647M and D4221, respectively. Since this test method may not identify all dispersive clay soils, other tests such as, pinhole dispersion (Test Methods D4647/D4647M), double hydrometer (Test Method D4221) and the analysis of pore water extraction (Test Methods D4542) may be performed individually or used together to help verify dispersion.  
1.3 The crumb test has some limitations in its usefulness as an indicator of dispersive soil. A dispersive soil may sometimes give a non-dispersive reaction in the crumb test. Soils containing kaolinite with known field dispersion problems, have shown non-dispersive reactions in the crumb test (1).2 However, if the crumb test indicates dispersion, the soil is probably dispersive.  
1.4 These test methods are applicable only to soils where the position of the plasticity index versus liquid limit plots (Test Methods D4318) falls on or above the “A” line (Practice D2487) and more than 12 % of the soil fraction is finer than 2-μm as determined in accordance with Test Method D7928.  
1.5 Oven-dried soil should not be used to prepare crumb test specimens, as irreversible changes could occur to the soil pore-water physicochemical properties responsible for dispersion (2).
Note 1: In some cases, the results of the pinhole, crumb, and double-hydrometer test methods may disagree. The crumb test is a better indicator of dispersive soils than of non-dispersive soils (3).  
1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.7 All observed and calculated values shall conform to the guidelines for significant digits and rounding establish...

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ASTM
ASTM D7263-21(Test Method)
Standard Test Methods for Laboratory Determination of Density and Unit Weight of Soil Specimens

SIGNIFICANCE AND USE
5.1 Density is a key element in the phase relations, phase relationships, or mass-volume relationships of soil and rock (Appendix X1). When particle density, that is, specific gravity (Test Methods D854) is also known, dry density can be used to calculate porosity and void ratio (see Appendix X1). Dry density measurements are also useful for determining degree of soil compaction. Since water content is variable, total/moist soil density provides little useful information except to estimate the weight of soil per unit volume, for example, grams per cubic centimeter, at the time of sampling. Since soil volume shrinks with drying of swelling soils, total density will vary with water content. Hence, the water content of the soil should be determined at the time of sampling.  
5.2 Densities and unit weights of remolded/reconstituted specimens are commonly used to evaluate the degree of compaction of earthen fills, embankments, and the like. Dry density values are used to calculate dry unit weight values to create a compaction curve (Test Methods D698 and D1557).
Note 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on several factors; Practice D3740 provides a means of evaluating some of these factors.
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1.1 These test methods describe two ways of determining the total/moist/bulk density, dry density, and dry unit weight of intact, disturbed, remolded, and reconstituted (compacted) soil specimens (Note 1). Intact specimens may be obtained from thin-walled sampling tubes, block samples, or clods. Specimens that are remolded by dynamic or static compaction procedures are also measured by these methods. These methods apply to soils that will retain their shape during the measurement process and may also apply to other materials such as soil-cement, soil-lime, soil-bentonite or solidified soil-bentonite-cement slurries. It is common for the density to be less than the value based on tube or mold volumes, or of in situ conditions after removal of the specimen from sampling tubes and compaction molds. This change is due to the specimen swelling after removal of lateral pressures.
Note 1: The adjectives total, moist, wet or bulk are used to represent the density condition. In some professions, such as Soil Science and Geology, the term “bulk density” usually has the same meaning as dry density. In the Geotechnical and Civil Engineering professions, the preferred adjective is total over moist and bulk when referring to the total mass of partially saturated or saturated soil or rock per unit total volume. For more detailed information regarding the term density, refer to Terminology D653.  
1.1.1 Method A (Water Displacement)—A specimen is coated in wax and then placed in water to measure the volume by determining the quantity of water displaced. The density and unit weight are then calculated based on the mass and volume measurements. Do not use this method if the specimen is susceptible to surface wax intrusion.  
1.1.2 Method B (Direct Measurement)—The dimensions and mass of a specimen are measured. The density and unit weight are then calculated using these direct measurements. Usually, the specimen has a cylindrical or cuboid shape. Intact and reconstituted/remolded specimens may be tested by this method in conjunction with strength, permeability/hydraulic conductivity (air/water) and compressibility determinations.  
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard. ...

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ASTM
ASTM D5778-20(Test Method)
Standard Test Method for Electronic Friction Cone and Piezocone Penetration Testing of Soils

SIGNIFICANCE AND USE
5.1 Tests performed using this test method provide a detailed record of cone tip resistance, which is useful for evaluation of site stratigraphy, engineering properties, homogeneity and depth to firm layers, voids or cavities, and other discontinuities. The use of a friction sleeve and pore water pressure element can provide an estimate of soil classification, and correlations with engineering properties of soils. When properly performed at suitable sites, the test provides a rapid means for determining subsurface conditions.  
5.2 This test method provides data used for estimating engineering properties of soil intended to help with the design and construction of earthworks, the foundations for structures, and the behavior of soils under static and dynamic loads.  
5.3 This method tests the soil in situ and soil samples are not obtained during the test. The interpretation of the results from this test method provides estimates of the types of soil penetrated. Engineers may obtain soil samples from parallel borings for correlation purposes but prior information or experience may preclude the need for borings.
Note 2: The quality of the results produced by this standard is dependent on the competence of the personal performing the test, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors and Practice D3740 provides a means of evaluating some of those factors.
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1.1 This test method covers the procedure for determining the resistance of a friction cone or a piezocone as it is advanced into subsurface soils at a steady rate.  
1.2 This test method applies to electronic friction cones and does not include hydraulic, pneumatic, or free-fall cones, although many of the procedural requirements herein could apply to those cones. Also, offshore/marine Cone Penetration Testing (CPT) systems may have procedural differences because of the difficulties of testing in those environments (for example, tidal variations, salt water and waves). Field tests using mechanical-type cones are covered elsewhere by Test Method D3441.  
1.3 This test method can be used to determine pore water pressures developed during the penetration when using a properly saturated piezocone. Pore water pressure dissipation, after a push, can also be monitored for correlation to time rate of consolidation and permeability.  
1.4 Additional sensors, such as inclinometer, seismic (Test Methods D7400), resistivity, electrical conductivity, dielectric, and temperature sensors, may be included in the cone to provide additional information. The use of an inclinometer is recommended since it will provide information on potentially damaging situations during the sounding process.  
1.5 CPT data can be used to interpret subsurface stratigraphy, and through use of site specific correlations, they can provide data on engineering properties of soils intended for use in design and construction of earthworks and foundations for structures.  
1.6 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this test method  
1.7 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this test method.  
1.7.1 The procedures used to specify how data are collected/recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider materi...

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