ASTM E1521-93(1998)
(Test Method)Standard Test Method for Liquid Holding Capacity of Granular Carriers
Standard Test Method for Liquid Holding Capacity of Granular Carriers
SCOPE
1.1 This test method is used to determine the liquid holding capacity (LHC) of clay granular carriers.
1.2 The values stated in either SI or inch-pound units are to be regarded as standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 5.
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NOTICE: This standard has either been superseded and replaced by a new version or
withdrawn. Contact ASTM International (www.astm.org) for the latest information.
Designation: E 1521 – 93 (Reapproved 1998)
AMERICAN SOCIETY FOR TESTING AND MATERIALS
100 Barr Harbor Dr., West Conshohocken, PA 19428
Reprinted from the Annual Book of ASTM Standards. Copyright ASTM
Standard Test Method for
Liquid Holding Capacity (LHC) of Clay Granular Carriers
This standard is issued under the fixed designation E 1521; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope and vapors. Take care to prevent contamination of the sur-
rounding area. Always wear the appropriate safety equipment
1.1 This test method is used to determine the liquid holding
and, where indicated, wear respiratory devices approved by
capacity (LHC) of clay granular carriers.
NIOSH for the product being tested.
1.2 The values stated in either SI or inch-pound units are to
be regarded as standard. The values given in parentheses are
6. Procedure
for information only.
6.1 Weigh 7.0 6 0.1 g of granular carrier for LHC deter-
1.3 This standard does not purport to address all of the
mination into a 29.6-mL glass bottle.
safety concerns, if any, associated with its use. It is the
6.2 From a buret, add kerosene as follows: 0.5-mL incre-
responsibility of the user of this standard to establish appro-
ments until 2.0 mL is reached, shaking between increments by
priate safety and health practices and determine the applica-
hand or mechanical shaker until completely absorbed. (A few
bility of regulatory limitations prior to use. For specific
sharp taps with the heel of the hand may be necessary to break
precautionary statements, see Section 5.
up a saturated portion.) Shaking should not exceed 2 min.
2. Summary of Test Method 6.3 After the first 2.0 mL is added, decrease the increments
to 0.2 mL and proceed as described in 6.2 until the end point
2.1 Incremental amounts of kerosene are added to a known
is reached. The end point is indicated by two or more of the
weight of granular carrier. The point at which the granules stick
following:
to the sides of the container allows calculation of the LHC.
6.3.1 Clay darkens or appears wet.
3. Significance and Use 6.3.2 Granules cease to be free flowing.
6.3.3 Granules stick to sides of bottle.
3.1 This test method has been designed principally for clay
6.3.4 Granules stick to bottom of bottle when inverted
granular carriers. Its accuracy with other materials has not been
slowly.
determined.
6.4 An alternate procedure is to use 50 g of clay. Follow the
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SIGNIFICANCE AND USE
3.1 This test method has been designed principally for granular carriers with LHC greater than 5.0 %. The incremental amount of suitable fluid added can be adjusted down as needed for carriers with LHC less than 5.0 %.
3.2 This test method has been designed principally for granular carriers with a relatively rapid absorption of liquid. Some materials may absorb liquids more slowly than the described times in the method. If such is the case, the time limit of two (2) min. may be extended.
3.3 This test method is applicable to granules in the range from 4 to 100 mesh (4.75 to 0.150 mm).
SCOPE
1.1 This test method is used to determine the liquid holding capacity (LHC) of granular carriers.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 5.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The water content of a soil is used throughout professional practice both in the laboratory and in the field. The use of Test Methods D2216 for water content determination can be time consuming and there are occasions when a more expedient method is desirable. Drying by direct heating is one such method. Results of this test method have been demonstrated to be of satisfactory accuracy for use in field control testing, such as in the determination of water content, and in the determination of in-place dry unit weight of soils.
5.2 The principal objection to the use of the direct heating for water content determination is the possibility of overheating the soil, thereby yielding a water content higher than would be determined by Test Methods D2216. While not eliminating this possibility, the incremental drying procedure in this test method will reduce its effects. Some heat sources have settings or controls that can also be used to reduce overheating. Loose fitting covers or enclosures can also be used to reduce overheating while assisting in uniform heat distribution.
5.3 The behavior of a soil when subjected to direct heating is dependent on its mineralogical composition, and as a result, no one procedure is applicable for all types of soils or heat sources. The general procedure of this test method applies to all soils, but test details may need to be tailored to the soil being tested.
5.4 When this test method is to be used repeatedly on the same or similar soil from a given site, a correction factor can usually be determined by making several comparisons between the results of this test method and Test Methods D2216. A correction factor is valid when the difference is consistent for several comparisons, and is reconfirmed on a regular specified basis.
5.5 This test method is not appropriate when precise results are required, or when minor variations in water content will affect the results of other test methods, such as borderline situations where...
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1.1 This test method covers procedures for determining the water content of soils by drying with direct heat, such as using a hotplate, stove or a blowtorch, where the heat is applied to the container and not directly to the soils.
1.2 This test method can be used as a substitute for Test Methods D2216 when more rapid results are desired to expedite other phases of testing and less accurate results are acceptable.
1.3 When questions of accuracy between this test method and Test Methods D2216 arise, the results of Test Methods D2216 will be used.
1.4 This test method is applicable for most soil types. For some soils, such as those containing significant amounts of halloysite, mica, montmorillonite, gypsum, or other hydrated materials, highly organic soils or soils that contain dissolved solids, (such as salt in the case of marine deposits), this test method may not yield reliable water content values due to the potential for heating above 110°C or lack of means to account for the presence of precipitated solids that were previously dissolved.
1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measure are included in this standard. The sieve designations are identified using the “standard” system in accordance with Specification E11, such as 2.0-mm and 19-mm, followed by the “alternative” system of No. 10 and 3/4-in., respectively, in parentheses. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.
1.6 All observed and calculated values must conform to the guidelines for significant digits and rounding established in Practice D6026, unless otherwise superseded by this standard.
1.6.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained....
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SIGNIFICANCE AND USE
4.1 The purpose of this practice is to standardize the routine description of peat and other organic soils for various uses (such as, peatland inventories and resource evaluations). This practice should be used to supplement other field information, such as, site location, surface morphology, surface vegetation, water table, moisture content, fiber content, wood content, and visually identifiable plant types and parts.
Note 1: This standard is a visual/manual method and is not meant to replace the more precise method of laboratory classification of peat (see Classification D4427). It should also be noted, this practice is independent of the determination of whether an articluar deposit contains peat that is defined in Classification D4427 on the basis of laboratory determination of ash content (see Test Method D2974).
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1.1 This practice covers the visual determination of the degree of humification of peat and other highly organic soils by visually evaluating the color of the water expelled upon compression. This practice is not used for the determination of the degree of organic decomposition of organic matter in mineral soils.
1.2 This practice offers a set of instructions for performing one or more specific operations. This document cannot replace education or experience and should be used in conjunction with professional judgment. Not all aspects of this practice may be applicable in all circumstances. This ASTM standard is not intended to represent or replace the standard of care by which the adequacy of a given professional service must be judged, nor should this document be applied without consideration of a project’s many unique aspects. The word “Standard” in the title of this document means only that the document has been approved though the ASTM consensus process.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The soil permittivity probe is used for the following purposes:
5.1.1 The test method described is useful as a rapid, nondestructive technique for bulk measurements of the water mass per unit volume of soil and soil-aggregate which may, in conjunction with an independent bulk density determination, be used in the determination of dry density.
5.1.2 The test method is used for quality control and acceptance testing of compacted soil and soil-aggregate mixtures as used in construction and also for research and development. The nondestructive nature allows repetitive measurements at a single test location and statistical analysis of the results.
5.1.3 Volumetric Water Content—The fundamental assumptions inherent in the test method are that the dielectric constants value measured by the system in a given test site composed of soil or soil-aggregate are directly correlated to the volumetric water content of the soil or soil-aggregate, and that the material is homogeneous. (See 6, “Interferences.”)
Note 2: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
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1.1 This test method describes the procedures for measuring the water mass per unit volume of soil and soil-aggregate by use of an in situ permittivity probe. Measurements are taken at a depth beneath the surface of the soil determined by the design of the probe.
1.1.1 For limitations see Section 6 on Interferences.
1.2 The permittivity probe is inserted into a hole drilled or punched into the soil being measured. As its name indicates, the probe measures the dielectric permittivity of the soil into which it is placed. Two electrodes, connected to an oscillating circuit, are mounted a predetermined distance apart. These electrodes act as the plates of a capacitor, with the soil between the plates forming the capacitor dielectric.
1.2.1 The probe circuit creates an oscillating electric field in the soil. Changes in the dielectric permittivity of the soil are indicated by changes in the circuit’s operating frequency. Since water has a much higher dielectric constant (80) than the surrounding soil (typically around 4), the water content can be related by a mathematical function to the change in dielectric permittivity, and, consequently, the changes in the circuit’s operating frequency.
1.2.2 The construction, deployment, and operating principle of the device described in this test method differ from other methods that measure the dielectric constant, bulk electrical conductivity, complex impedance, or electromagnetic impedance (see Test Methods D6780/D6780M, D7698, and D7830/D7830M) of the soil and relate the results to water mass per unit volume and/or water content.
1.2.3 The water content of the soil measured by the permittivity probe is the volumetric water content, expressed as the ratio of the volume of water to the total volume occupied by the soil. This quantity is often converted, and displayed, by the probe in units of mass of water per volume of soil, or water mass per unit volume. This conversion is performed by multiplying the water content (in volume of water per volume of soil) by the density of water.
1.3 Water content most prevalent in engineering and construction activities is known as the gravimetric water content, ω, and is the ratio of the mass of the water in pore spaces to the total mass of solids, expressed as a percentage. To determine this quantity, the bulk density of the soil under measurement must ...
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SIGNIFICANCE AND USE
5.1 This test method is useful as a rapid, nondestructive technique for the measurement of the in-place water mass per unit volume of soil and rock at desired depths below the surface.
5.2 This test method is useful for informational and research purposes. The information acquired from this test method is best used for quality control and acceptance testing when correlated to actual water mass per unit volume using procedures and methods described in A1.2.3.
5.3 The non-destructive nature of this test method allows repetitive measurements to be made at a single test location for statistical analysis and to monitor changes over time.
5.4 The fundamental assumptions inherent in this test method are that the material under test is homogeneous and hydrogen present is in the form of water as defined by Test Method D2216.
Note 1: The quality of the result produced by this standard test method is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection, and the like. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
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1.1 This test method covers the measurement of the water mass per unit volume of soil and rock by thermalization or slowing of fast neutrons, where the neutron source and the thermal neutron detector are placed at the desired depth in the bored hole lined by an access tube.
1.1.1 For limitations see Section 6 on Interferences.
1.2 The water mass per unit volume, expressed as mass per unit volume of the material under test, is determined by comparing the thermal neutron count rate with previously established calibration data (see Annex A1).
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined. Within the text of this standard, SI units appear first followed by the inch-pound (or other non-SI) units in brackets.
1.3.1 Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.
1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.
1.4.1 The procedures used to specify how data are collected, recorded, and calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that should generally be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazards are given in Section 8.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade ...
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SIGNIFICANCE AND USE
4.1 This test method is used to measure one-dimensional flow of aqueous solutions (for example, landfill leachates, liquid wastes and byproducts, single and mixed chemicals, etc., from hereon referred to as the permeant liquid) through initially saturated soils under an applied hydraulic gradient and effective stress. Interactions between some permeant liquids and some clayey soils have resulted in significant increases in the hydraulic conductivity of the soils relative to the hydraulic conductivity of the same soils permeated with water (1).4 This test method is used to evaluate the presence and effect of potential interactions between the soil specimen being permeated and the permeant liquid on the hydraulic conductivity of the soil specimen. Test programs may include comparisons between the hydraulic conductivity of soils permeated with water relative to the hydraulic conductivity of the same soils permeated with aqueous solutions to determine variations in the hydraulic conductivity of the soils due to the aqueous solutions.
4.2 Flexible-wall hydraulic conductivity testing is used to determine flow characteristics of aqueous solutions through soils. Hydraulic conductivity testing using flexible-wall cells is usually preferred over rigid-wall cells for testing with aqueous solutions due to the potential for sidewall leakage problems with rigid-wall cells. Excessive sidewall leakage may occur, for example, when a test soil shrinks during permeation with the permeant liquid due to interactions between the soil and the permeant liquid in a rigid-wall cell. In addition, the use of a rigid-wall cell does not allow for control of the effective stresses that exist in the test specimen.
4.3 Darcy’s law describes laminar flow through a test soil. Laminar flow conditions and, therefore, Darcy’s law may not be valid under certain test conditions. For example, interactions between a permeating liquid and a soil may cause severe channeling/cracking of the soil such tha...
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1.1 This test method covers hydraulic conductivity compatibility testing of saturated soils in the laboratory with aqueous solutions that may alter hydraulic conductivity (for example, waste related liquids) using a flexible-wall permeameter. A hydraulic conductivity test is conducted until both hydraulic and chemical equilibrium are achieved such that potential interactions between the soil specimen being permeated and the aqueous solution are taken into consideration with respect to the measured hydraulic conductivity.
1.2 This test method is applicable to soils with hydraulic conductivities less than approximately 1 × 10–8 m/s.
1.3 In addition to hydraulic conductivity, intrinsic permeability can be determined for a soil if the density and viscosity of the aqueous solution are known or can be determined.
1.4 This test method can be used for all specimen types, including undisturbed, reconstituted, remolded, compacted, etc. specimens.
1.5 A specimen may be saturated and permeated using three methods. Method 1 is for saturation with water and permeation with aqueous solution. Method 2 is for saturation and permeation with aqueous solution. Method 3 is for saturation with water, initial permeation with water, and subsequent permeation with aqueous solution.
1.6 The amount of flow through a specimen in response to a hydraulic gradient generated across the specimen is measured with respect to time. The amount and properties of influent and effluent liquids are monitored during the test.
1.7 The hydraulic conductivity with an aqueous solution is determined using procedures similar to determination of hydraulic conductivity of saturated soils with water as described in Test Methods D5084. Several test procedures can be used, including the falling headwater-rising tailwater, the constant-head, the falling headwater-constant tailwater, or the constant rate-of-flow test procedures.
1.8 Units—The values stat...
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SIGNIFICANCE AND USE
3.1 This test method has been designed principally for granular carriers with LHC greater than 5.0 %. The incremental amount of suitable fluid added can be adjusted down as needed for carriers with LHC less than 5.0 %.
3.2 This test method has been designed principally for granular carriers with a relatively rapid absorption of liquid. Some materials may absorb liquids more slowly than the described times in the method. If such is the case, the time limit of two (2) min. may be extended.
3.3 This test method is applicable to granules in the range from 4 to 100 mesh (4.75 to 0.150 mm).
SCOPE
1.1 This test method is used to determine the liquid holding capacity (LHC) of granular carriers.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 5.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Understanding the mechanical properties of frozen soils is of primary importance to permafrost engineering. Data from creep tests are necessary for the design of most foundation elements embedded in, or bearing on frozen ground. They make it possible to predict the time-dependent settlements of piles and shallow foundations under service loads, and to estimate their short- and long-term bearing capacity. Creep tests also provide quantitative parameters for the stability analysis of underground structures that are created for permanent use.
5.2 It must be recognized that the structure of frozen soil in situ and its behavior under load may differ significantly from that of an artificially prepared specimen in the laboratory. This is mainly due to the fact that natural permafrost ground may contain ice in many different forms and sizes, in addition to the pore ice contained in a small laboratory specimen. These large ground-ice inclusions (such as ice lenses, a dominant horizontal, lens-shaped body of ice of any dimension) will considerably affect the time-dependent behavior of full-scale engineering structures.
5.3 In order to obtain reliable results, high-quality intact representative permafrost samples are required for creep tests. The quality of the sample depends on the type of frozen soil sampled, the in situ thermal condition at the time of sampling, the sampling method, and the transportation and storage procedures prior to testing. The best testing program can be ruined by poor-quality samples. In addition, one must always keep in mind that the application of laboratory results to practical problems requires much caution and engineering judgment.
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1.1 This test method covers the determination of the creep behavior of cylindrical specimens of frozen soil, subjected to uniaxial compression. It specifies the apparatus, instrumentation, and procedures for determining the stress-strain-time, or strength versus strain rate relationships for frozen soils under deviatoric creep conditions.
1.2 Although this test method is one that is most commonly used, it is recognized that creep properties of frozen soil related to certain specific applications, can also be obtained by some alternative procedures, such as stress-relaxation tests, simple shear tests, and beam flexure tests. Creep testing under triaxial test conditions will be covered in another standard.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.
1.4.1 For the purposes of comparing, a measured or calculated value(s) with specified limits, the measured or calculated value(s) shall be rounded to the nearest decimal or significant digits in the specified limits.
1.4.2 The procedures used to specify how data are collected/recorded or calculated in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.
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SIGNIFICANCE AND USE
5.1 The injectivity of a water is best determined by measurements as near to the well as possible to minimize changes in water properties due to air contact and time. This practice describes how core flow tests are carried out near the well.
5.2 This practice permits the differentiation of permeability losses from the effects of chemical interaction of water and rock and from the effects of plugging by suspended solids. The procedure can be utilized to estimate the chemical and filtration requirements for the full-scale injection project.
5.3 Application of the test results to injection wells requires consideration of test core selection and geometry effects.
5.4 This practice as described assumes that the water does not contain free oil or other immiscible hydrocarbons. The presence of free oil would require the method to be modified to account for the effect of oil saturation in the test cores on the water permeability.
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1.1 This practice covers a procedure for conducting on-site core flood tests to determine the filtration and chemical treatment requirements for subsurface injection of water.2, 3
1.2 This practice applies to water disposal, secondary recovery, and enhanced oil recovery projects and is applicable to injection waters with all ranges of total dissolved solids contents.
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses are mathematical conversions to inch-pound units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 The water content of soil is used throughout geotechnical engineering practice, both in the laboratory and in the field. Results are sometimes needed within a short time period and in locations where it is not practical to install an oven or to transport samples to an oven. This test method is used for these occasions.
5.2 The results of this test have been used for field control of compacted embankments or other earth structures such as in the determination of water content for control of soil moisture and dry density within a specified range.
5.3 This test method requires specimens consisting of soil having all particles smaller than the 4.75 mm (No. 4) sieve size.
5.4 This test method may not be as accurate as other accepted methods such as Test Method D2216. Inaccuracies may result because specimens are too small to properly represent the total soil, from clumps of soil not breaking up to expose all the available water to the reagent and from other inherent procedural, equipment or process inaccuracies. Therefore, other methods may be more appropriate when highly accurate results are required, or when the use of test results is sensitive to minor variations in the values obtained.
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SCOPE
1.1 This test method outlines procedures for determining the water (moisture) content of soil by chemical reaction using calcium carbide as a reagent to react with the available water in the soil producing a gas. A measurement is made of the gas pressure produced when a specified mass of wet or moist soil is placed in a testing device with an appropriate volume of reagent and mixed.
1.2 This test method is not intended as a replacement for Test Method D2216; but as a supplement when rapid results are required, when testing is done in field locations, or where an oven is not practical for use. Test Method D2216 is to be used as the test method to compare for accuracy checks and correction.
1.3 This test method is applicable for most soils. Calcium carbide, used as a reagent, reacts with water as it is mixed with the soil by shaking and agitating with the aid of steel balls in the apparatus. To produce accurate results, the reagent must react with all the water which is not chemically hydrated with soil minerals or compounds in the soil. Some highly plastic clay soils or other soils not friable enough to break up may not produce representative results because some of the water may be trapped inside soil clods or clumps which cannot come in contact with the reagent. There may be some soils containing certain compounds or chemicals that will react unpredictably with the reagent and give erroneous results. Any such problem will become evident as calibration or check tests with Test Method D2216 are made. Some soils containing compounds or minerals that dehydrate with heat (such as gypsum) which are to have special temperature control with Test Method D2216 may not be affected (dehydrated) in this test method.
1.4 This test method is limited to using calcium carbide moisture test equipment made for 20 g, or larger, soil specimens and to testing soil which contains particles no larger than the 4.75 mm (No. 4) Standard sieve size.
1.5 The values stated in SI units are to be regarded as standard. The inch-pound units given in parentheses are mathematical conversions, which are provided for information purposes only and are not considered standard.
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