CEN ISO/TS 21357:2023
(Main)Nanotechnologies - Evaluation of the mean size of nano-objects in liquid dispersions by static multiple light scattering (SMLS) (ISO/TS 21357:2022)
Nanotechnologies - Evaluation of the mean size of nano-objects in liquid dispersions by static multiple light scattering (SMLS) (ISO/TS 21357:2022)
.
This document provides guidance and requirements for the determination of the mean (spherical) equivalent diameter of nano-objects (i.e. particles, droplets or bubbles) dispersed in liquids using the static multiple light scattering (SMLS) technique. The technique is applicable to a wide range of materials and does not require dilution of concentrated samples.
Nanotechnologien - Ermittlung der mittleren Größe von Nanoobjekten in flüssigen Dispersionen mit Hilfe von statischer Mehrfachlichtstreuung (SMLS) (ISO/TS 21357:2022)
Dieses Dokument enthält einen Leitfaden und Anforderungen für die Bestimmung des mittleren Äquivalent(kugel)durchmessers von Nanoobjekten (d. h. Partikeln, Tröpfchen oder Blasen), die in Flüssigkeiten dispergiert sind, mittels statischer Mehrfachlichtstreuung (SMLS). Das Verfahren ist für eine Vielzahl von Werkstoffen anwendbar und erfordert keine Verdünnung konzentrierter Proben.
Nanotechnologies - Évaluation de la taille moyenne des nano-objets dans les dispersions liquides par diffusion statique multiple de la lumière (DSML) (ISO/TS 21357:2022)
Nanotehnologije - Vrednotenje srednje velikosti nanoobjektov v tekočih disperzijah s statičnim večkratnim sipanjem svetlobe (SMLS) (ISO/TS 21357:2022)
Ta dokument vsebuje smernice in zahteve za določanje povprečnega (sferičnega) enakovrednega premera nanopredmetov (tj. delcev, kapljic ali mehurčkov), razpršenih v tekočino s tehniko statičnega mnogoternega razprševanja svetlobe (SMLS). Tehnika se uporablja za širok nabor materialov in ne zahteva redčenja koncentriranih vzorcev.
General Information
Standards Content (Sample)
SLOVENSKI STANDARD
01-maj-2023
Nanotehnologije - Vrednotenje srednje velikosti nanoobjektov v tekočih
disperzijah s statičnim večkratnim sipanjem svetlobe (SMLS) (ISO/TS 21357:2022)
Nanotechnologies - Evaluation of the mean size of nano-objects in liquid dispersions by
static multiple light scattering (SMLS) (ISO/TS 21357:2022)
Nanotechnologies - Évaluation de la taille moyenne des nano-objets dans les
dispersions liquides par diffusion statique multiple de la lumière (DSML) (ISO/TS
21357:2022)
Ta slovenski standard je istoveten z: CEN ISO/TS 21357:2023
ICS:
07.120 Nanotehnologije Nanotechnologies
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
CEN ISO/TS 21357
TECHNICAL SPECIFICATION
SPÉCIFICATION TECHNIQUE
March 2023
TECHNISCHE SPEZIFIKATION
ICS 07.120
English Version
Nanotechnologies - Evaluation of the mean size of nano-
objects in liquid dispersions by static multiple light
scattering (SMLS) (ISO/TS 21357:2022)
Nanotechnologies - Évaluation de la taille moyenne des
nano-objets dans les dispersions liquides par diffusion
statique multiple de la lumière (DSML) (ISO/TS
21357:2022)
This Technical Specification (CEN/TS) was approved by CEN on 17 March 2023 for provisional application.
The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to
submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard.
CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS
available promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in
parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS into an EN is reached.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2023 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN ISO/TS 21357:2023 E
worldwide for CEN national Members.
Contents Page
European foreword . 3
European foreword
The text of ISO/TS 21357:2022 has been prepared by Technical Committee ISO/TC 229
"Nanotechnologies” of the International Organization for Standardization (ISO) and has been taken over
as CEN ISO/TS 21357:2023 by Technical Committee CEN/TC 352 “Nanotechnologies” the secretariat of
which is held by AFNOR.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
Any feedback and questions on this document should be directed to the users’ national standards body.
A complete listing of these bodies can be found on the CEN website.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Türkiye and the
United Kingdom.
Endorsement notice
The text of ISO/TS 21357:2022 has been approved by CEN as CEN ISO/TS 21357:2023 without any
modification.
TECHNICAL ISO/TS
SPECIFICATION 21357
First edition
2022-01
Corrected version
2022-03
Nanotechnologies — Evaluation of the
mean size of nano-objects in liquid
dispersions by static multiple light
scattering (SMLS)
Nanotechnologies — Évaluation de la taille moyenne des nano-objets
dans les dispersions liquides par diffusion statique multiple de la
lumière (DSML)
Reference number
ISO/TS 21357:2022(E)
ISO/TS 21357:2022(E)
© ISO 2022
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
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Published in Switzerland
ii
ISO/TS 21357:2022(E)
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols and abbreviated terms.2
5 Principles . 3
5.1 Relevant theory . 3
5.2 Key measurands . 5
5.3 Method applicability and limitations . 6
5.3.1 General . 6
5.3.2 Sample concentration . 6
5.3.3 Mean equivalent particle diameter . 7
5.3.4 Sample homogeneity and stability . 7
5.4 Method characteristics . 7
6 Apparatus . 8
7 Measurement procedure . 9
7.1 Instrument preparation . 9
7.2 Sample handling . 9
7.3 System settings . 10
7.3.1 General . 10
7.3.2 Procedure to verify sample homogeneity . 10
7.3.3 Volume fraction . 10
7.3.4 Refractive index . 10
8 Performance qualification .11
9 Data record .11
10 Measurement uncertainty .11
Annex A (informative) I and I versus l* and l .13
BS T
Annex B (informative) I and I as a function of D for titanium dioxide and melamine resin
BS T
particles . . .14
Annex C (informative) Instrument qualification .16
Annex D (informative) Comparative analysis of Latex suspensions at various concentrations .17
Annex E (informative) Analysis of titanium dioxide suspensions at different concentrations .18
Annex F (informative) Results of an interlaboratory comparison study .20
Bibliography .23
iii
ISO/TS 21357:2022(E)
Foreword
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described in the ISO/IEC Directives, Part 1. In particular the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www.iso.org/patents).
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expressions related to conformity assessment, as well as information about ISO's adherence to
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www.iso.org/iso/foreword.html.
This document was prepared by Technical Committee ISO/TC 229, Nanotechnologies.
This corrected version of ISO/TS 21357:2022 incorporates the
...
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