Advanced technical ceramics - Methods of test for ceramic coatings - Part 13: Determination of wear rate by the pin-on-disk method

1.1   This part of EN 1071 describes a method for evaluating the wear of ceramic coatings by use of a test in which a flat or spherically ended pin is brought, under load, into contact with the flat surface of a disk and the two are set in relative motion such that the pin describes a circular path on the disk. Depending on the conditions being simulated, either the pin or disk or both may be coated with the material under test, with the other member of the couple being selected for its relevance to the system under evaluation.
1.2   Where suitable equipment is available, the test may be used to determine the friction generated in the sliding contact.
1.3   The method is suitable for evaluating coatings in the thickness range from 1 to more than 100μm, and with suitable choice of conditions might also be applicable to testing thinner coatings.
1.4   Testing may be under either dry or lubricated conditions. However, the test is not designed for evaluating the properties of lubricants except in so far as they affect the wear behaviour of the materials being tested. Related methods for testing lubricants using a reciprocating motion are given in references [4] – [6].
1.5   Testing a materials couple under a range of loading conditions might provide information about the adhesive and/or cohesive strength of the coating, in addition to its wear behaviour.

Hochleistungskeramik - Verfahren zur Prüfung keramischer Schichten - Teil 13: Bestimmung der Verschleißrate mittels Stift-Scheibe-Prüfung

1.1   In diesem Teil von EN 1071 wird ein Prüfverfahren zur Bewertung des Verschleißes keramischer Schichten festgelegt, bei dem ein Prüfstift mit flachem oder kugelförmigem Ende unter Krafteinwirkung mit der ebenen Oberfläche einer Scheibe in Kontakt gebracht und die beiden so relativ zueinander bewegt werden, dass der Stift auf der Scheibe einen kreisförmigen Weg durchläuft. In Abhängigkeit von den zu simulierenden Bedingungen dürfen entweder der Stift oder die Scheibe oder beide mit dem zu prüfenden Werkstoff beschichtet sein, wobei das andere Element der Werkstoffpaarung hinsichtlich seiner Relevanz für das zu untersuchende System ausgewählt wird.
1.2   Wenn eine geeignete Prüfeinrichtung verfügbar ist, darf die Prüfung zur Bestimmung der beim Gleit-kontakt auftretenden Reibung angewendet werden.
1.3   Dieses Verfahren ist zur Bewertung von Schichten mit Dicken von 1 µm bis größer 100 µm geeignet; durch Auswahl entsprechender Bedingungen ist das Verfahren auch auf dünnere Schichten anwendbar.
1.4   Die Prüfung darf trocken oder mit Schmierung durchgeführt werden. Die Prüfung ist jedoch nicht zur Bewertung der Schmierstoffeigenschaften vorgesehen, außer insoweit, wie Schmierstoffe das Verschlei߬ver-halten der zu prüfenden Werkstoffe beeinflussen. Verfahren zur Prüfung von Schmierstoffen unter Anwen-dung einer Hin  und Herbewegung werden in [4] bis [6] angegeben.
1.5   Die Prüfung einer Werkstoffpaarung unter unterschiedlichen Beanspruchungsbedingungen kann außer Informationen zum Verschleißverhalten der Schicht auch Angaben zu ihrer Haft  und/oder Kohäsionsfestigkeit liefern.

Céramiques techniques avancées - Méthodes d'essai pour revêtements céramiques - Partie 13 : Détermination du taux d'usure selon la méthode pin-on-disk

1.1 Cette norme européenne décrit une méthode d’évaluation de l’usure des revêtements céramiques à
l’aide d’un essai dans lequel une broche à extrémité plate ou sphérique, sous charge, en contact avec un
disque plat, est mise en mouvement relatif avec ce dernier de sorte que la broche décrive un chemin circulaire
sur la surface plane du disque. Selon les conditions simulées, la broche ou le disque, ou les deux, peuvent
être revêtues du matériau soumis à essai, l’autre membre du couple étant sélectionné pour sa pertinence par
rapport au système soumis à évaluation.
1.2 Lorsque les équipements appropriés sont disponibles, l’essai peut être utilisé pour déterminer le
frottement généré dans le contact de glissement.
1.3 La méthode est adaptée à l’évaluation des revêtements dans une plage d’épaisseur comprise entre
1 μm et plus de 100 μm, et en choisissant des conditions appropriées, elle peut également s’appliquer aux
essais réalisés sur des revêtements plus minces.
1.4 Les essais peuvent être effectués à l'état sec ou lubrifié. Néanmoins, les essais ne sont pas destinés à
évaluer les propriétés des lubrifiants, sauf dans la mesure où celles-ci influencent le comportement à l'usure
des matériaux soumis à essai. Les méthodes d’essai associées des lubrifiants par un mouvement de va-etvient
sont données dans les références [4] à [6].
1.5 L’essai effectué sur un couple de matériaux dans une plage de conditions de charge peut fournir des
informations relatives à la résistance adhésive et/ou cohésive du revêtement, outre son comportement à
l’usure.

Sodobna tehnična keramika - Metode za preskušanje keramičnih prevlek - 13. del: Ugotavljanje stopnje obrabe (metoda pin-on-disk)

Ta evropski standard opisuje metodo za ocenjevanje obrabe keramičnih prevlek z uporabo preskusa, pri katerem plosko ali kroglasto zaključeno iglo privedemo v stik, pod obtežbo, z ravno površino diska, nato pa oba poženemo v relativno gibanje tako, da igla opiše krožno pot na disku. V odvisnosti od simuliranih pogojev sta lahko bodisi igla ali disk, ali oba, prevlečena z materialom, ki se preskuša, pri čemer je drugi del para izbran zaradi svoje pomembnosti za sistem, ki se ocenjuje. Kadar je na voljo ustrezna oprema, se preskus lahko uporablja za določevanje trenja, ki nastaja pri drsečem stiku. Metoda je primerna za ocenjevanje prevlek v razponu debeline od 1 μm do več kot 100 μm, z ustreznim izborom pogojev pa se lahko uporablja tudi za preskušanje tanjših prevlek. Preskus se lahko opravi bodisi pod suhimi ali mazanimi pogoji. Vendar pa preskus ni zasnovan za ocenjevanje lastnosti maziv, razen v kolikor vplivajo na obnašanje preskušanih materialov pri obrabi. Povezane metode za preskušanje maziv z uporabo izmeničnega gibanja so podane v referencah [4] - [6]. Preskušanje para materialov pod razponom obtežbenih pogojev lahko zagotovi podatke o sprijemni in/ali kohezijski trdnosti prevleke, poleg njegovega obnašanja glede obrabe.

General Information

Status
Published
Publication Date
23-Mar-2010
Withdrawal Date
29-Sep-2010
Current Stage
9060 - Closure of 2 Year Review Enquiry - Review Enquiry
Start Date
02-Sep-2025
Completion Date
02-Sep-2025

Overview

EN 1071-13:2010 - published by CEN - specifies a standardized pin-on-disk test method for determining the wear rate of ceramic coatings. The procedure evaluates wear and, where instrumentation is available, friction in sliding contacts where a flat or spherically-ended pin is loaded against a rotating flat disk. The method applies to coatings from about 1 µm to >100 µm (and potentially thinner coatings with adapted conditions) and supports testing under dry or lubricated conditions. Results can be reported as mass wear rate or volume wear rate and are intended to help predict coating performance in tribological applications.

Key topics and requirements

  • Test configuration: pin (flat or spherically ended) sliding on a flat disk; either or both members may be coated depending on the tribosystem being simulated.
  • Wear metrics:
    • Volume wear rate - volume removed per 1 m sliding distance under 1 N normal load.
    • Mass wear rate - mass removed per 1 m sliding distance under 1 N normal load.
    • Instantaneous coefficient of friction - friction force divided by applied load.
  • Apparatus essentials:
    • Holders for pin and disk, drive system for relative motion, loading mechanism, and means to determine total sliding distance.
    • Optional lubricant delivery/collection and friction measurement (e.g., load cell, spring deflection, torque). Friction measurement accuracy recommended at about ±1% of applied load.
    • For flat-ended pins, means to ensure reproducible contact conformance between pin and disk.
  • Measurement methods: weight loss, profilometry, linear measurement, or combinations; annexes describe profilometry for pins and ball-crater techniques for disks.
  • Testing conditions: orientation (horizontal/vertical) must be reported; tests may be used to probe adhesive/cohesive strength by varying load.
  • Reporting and repeatability: procedures for setup, wear-scars evaluation, calculation of wear coefficients and reporting are defined to ensure consistent results.

Applications

  • Evaluating wear resistance and friction of advanced ceramic coatings used in stamping, molding, blanking, tooling, and sliding machine components.
  • Screening coating formulations and deposition processes for tribological performance.
  • Supporting product development, quality control, failure analysis, and comparative benchmarking of coatings.

Who uses this standard

  • Materials scientists, tribologists, and mechanical engineers
  • Coating manufacturers and process engineers
  • Testing and calibration laboratories (aligned with EN ISO/IEC 17025)
  • Product designers and OEMs assessing coating durability in sliding contacts

Related standards

  • Other parts of the EN 1071 series (e.g., Part 6 micro-abrasion, Part 12 reciprocating wear) provide complementary test methods.
  • EN ISO/IEC 17025 is referenced for laboratory competence.

Keywords: EN 1071-13:2010, pin-on-disk, ceramic coatings, wear rate, advanced technical ceramics, tribology, friction measurement, profilometry, CEN.

Frequently Asked Questions

EN 1071-13:2010 is a standard published by the European Committee for Standardization (CEN). Its full title is "Advanced technical ceramics - Methods of test for ceramic coatings - Part 13: Determination of wear rate by the pin-on-disk method". This standard covers: 1.1 This part of EN 1071 describes a method for evaluating the wear of ceramic coatings by use of a test in which a flat or spherically ended pin is brought, under load, into contact with the flat surface of a disk and the two are set in relative motion such that the pin describes a circular path on the disk. Depending on the conditions being simulated, either the pin or disk or both may be coated with the material under test, with the other member of the couple being selected for its relevance to the system under evaluation. 1.2 Where suitable equipment is available, the test may be used to determine the friction generated in the sliding contact. 1.3 The method is suitable for evaluating coatings in the thickness range from 1 to more than 100μm, and with suitable choice of conditions might also be applicable to testing thinner coatings. 1.4 Testing may be under either dry or lubricated conditions. However, the test is not designed for evaluating the properties of lubricants except in so far as they affect the wear behaviour of the materials being tested. Related methods for testing lubricants using a reciprocating motion are given in references [4] – [6]. 1.5 Testing a materials couple under a range of loading conditions might provide information about the adhesive and/or cohesive strength of the coating, in addition to its wear behaviour.

1.1 This part of EN 1071 describes a method for evaluating the wear of ceramic coatings by use of a test in which a flat or spherically ended pin is brought, under load, into contact with the flat surface of a disk and the two are set in relative motion such that the pin describes a circular path on the disk. Depending on the conditions being simulated, either the pin or disk or both may be coated with the material under test, with the other member of the couple being selected for its relevance to the system under evaluation. 1.2 Where suitable equipment is available, the test may be used to determine the friction generated in the sliding contact. 1.3 The method is suitable for evaluating coatings in the thickness range from 1 to more than 100μm, and with suitable choice of conditions might also be applicable to testing thinner coatings. 1.4 Testing may be under either dry or lubricated conditions. However, the test is not designed for evaluating the properties of lubricants except in so far as they affect the wear behaviour of the materials being tested. Related methods for testing lubricants using a reciprocating motion are given in references [4] – [6]. 1.5 Testing a materials couple under a range of loading conditions might provide information about the adhesive and/or cohesive strength of the coating, in addition to its wear behaviour.

EN 1071-13:2010 is classified under the following ICS (International Classification for Standards) categories: 81.060.30 - Advanced ceramics. The ICS classification helps identify the subject area and facilitates finding related standards.

You can purchase EN 1071-13:2010 directly from iTeh Standards. The document is available in PDF format and is delivered instantly after payment. Add the standard to your cart and complete the secure checkout process. iTeh Standards is an authorized distributor of CEN standards.

Standards Content (Sample)


2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Hochleistungskeramik - Verfahren zur Prüfung keramischer Schichten - Teil 13: Bestimmung der Verschleißrate mittels Stift-Scheibe-PrüfungCéramiques techniques avancées - Méthodes d'essai pour revêtements céramiques - Partie 13 : Détermination du taux d'usure selon la méthode pin-on-diskAdvanced technical ceramics - Methods of test for ceramic coatings - Part 13: Determination of wear rate by the pin-on-disk method81.060.30Sodobna keramikaAdvanced ceramics25.220.99Druge obdelave in prevlekeOther treatments and coatingsICS:Ta slovenski standard je istoveten z:EN 1071-13:2010SIST EN 1071-13:2010en,de01-maj-2010SIST EN 1071-13:2010SLOVENSKI
STANDARD
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 1071-13
March 2010 ICS 81.060.30 English Version
Advanced technical ceramics - Methods of test for ceramic coatings - Part 13: Determination of wear rate by the pin-on-disk method
Céramiques techniques avancées - Méthodes d'essai pour revêtements céramiques - Partie 13 : Détermination du taux d'usure selon la méthode pin-on-disk
Hochleistungskeramik - Verfahren zur Prüfung keramischer Schichten - Teil 13: Bestimmung der Verschleißrate mittels Stift-Scheibe-Prüfung This European Standard was approved by CEN on 30 January 2010.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation under the responsibility of a CEN member into its own language and notified to the CEN Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre:
Avenue Marnix 17,
B-1000 Brussels © 2010 CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Members. Ref. No. EN 1071-13:2010: ESIST EN 1071-13:2010

Methods for the determination of coating properties likely to be relevant to coating performance in a pin-on-disk wear test . 18A.1 Relevant properties . 18A.2 Phase composition and preferred orientation. . 18A.3 Residual stress . 18A.4 Hardness . 18Annex B (informative)
Determination of volume loss from the pin using profilometry . 19Annex C (informative)
Determination of wear of coated disk by ball crater technique . 20Bibliography . 23 SIST EN 1071-13:2010

Advanced technical ceramics
Methods of test for ceramic coatings, consists of the following 13 parts:  Part1: Determination of coating thickness by contact probe filometer  Part 2: Determination of coating thickness by the crater grinding method  Part 3: Determination of adhesion and other mechanical failure modes by a scratch test  Part 4: Determination of chemical composition by electron probe microanalysis (EPMA)  Part 5: Determination of porosity (withdrawn)  Part 6: Determination of the abrasion resistance of coatings by a micro-abrasion wear test  Part 7: Determination of hardness and Young's modulus by instrumented indentation (withdrawn)  Part 8: Rockwell indentation test for evaluation of adhesion  Part 9: Determination of fracture strain  Part 10: Determination of coating thickness by cross sectioning  Part 11: Determination of internal stress by the Stoney formula  Part 12: Reciprocating wear test  Part 13: Determination of wear rate by the pin-on-disk method Part 7 was a Technical Specification and Parts 8 to 11 are Technical Specifications. According to the CEN/CENELEC Internal Regulations, the national standards organizations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland and the United Kingdom. SIST EN 1071-13:2010

Introduction The determination of the wear resistance of thin ceramic coatings used in sliding contacts is of high importance in several industrial fields such as stamping, moulding, blanking and in many situations where two mechanical components slide on each other. This part of EN 1071 describes a method for evaluating the wear of ceramic coatings by use of a test in which a flat or spherically ended pin is brought, under load, into contact with a flat disk and the two are set in relative motion such that the pin describes a circular path on the flat surface of the disk. Depending on the information required, either the disk or pin or both may be coated with the material under test, with the other member of the couple being selected for its relevance to the tribosystem under evaluation. Wear is determined by weight loss, by profilometry, by linear measurement or by a combination of these.
Testing may be carried out under dry or lubricated conditions. Where suitable instrumentation is available, the test can provide important information about the friction generated in the system. In addition to providing data on the frictional interaction in the system, monitoring of the friction can, by detecting changes in the level or trend of the friction force, provide important information about changes occurring during the test, e.g. removal or fracture of the coating, changes in wear mechanisms, etc. The test for use with bulk materials sliding under non-lubricated conditions is well described in [1]. This standard identifies the basic equipment requirements and the test critical parameters for testing ceramic coatings, and provides for appropriate operating procedures and measurement protocols to ensure their proper control. In addition, it provides for consistency in the analysis of data and in the treatment of errors.
This part of EN 1071 complements parts 6 [2] and 12 [3], which describe techniques for micro-scale abrasion wear testing and reciprocating wear testing of ceramic coatings respectively. SIST EN 1071-13:2010

1 Scope 1.1 This European Standard describes a method for evaluating the wear of ceramic coatings by use of a test in which a flat or spherically ended pin is brought, under load, into contact with the flat surface of a disk and the two are set in relative motion such that the pin describes a circular path on the disk. Depending on the conditions being simulated, either the pin or disk or both may be coated with the material under test, with the other member of the couple being selected for its relevance to the system under evaluation.
1.2 Where suitable equipment is available, the test may be used to determine the friction generated in the sliding contact. 1.3 The method is suitable for evaluating coatings in the thickness range from 1 µm to more than 100 µm, and with suitable choice of conditions might also be applicable to testing thinner coatings. 1.4 Testing may be under either dry or lubricated conditions. However, the test is not designed for evaluating the properties of lubricants except insofar as they affect the wear behaviour of the materials being tested. Related methods for testing lubricants using a reciprocating motion are given in references [4] – [6]. 1.5 Testing a materials couple under a range of loading conditions might provide information about the adhesive and/or cohesive strength of the coating, in addition to its wear behaviour. 2 Normative references The following referenced documents are indispensable for the application of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN ISO/IEC 17025, General requirements for the competence of testing and calibration laboratories (ISO/IEC 17025:2005) ISO 31-0, Quantities and units
Part 0: General principles 3 Terms and definitions For the purposes of this document, the following terms and definitions apply.
3.1
volume wear rate
volume wear coefficient
specific wear rate volume of material removed from a surface in a sliding distance of 1 m under a normal load of 1 N 3.2
mass wear rate
mass wear coefficient mass of material removed from a surface in a sliding distance of 1 m under a normal load of 1 N 3.3
instantaneous coefficient of friction instantaneous value of the friction force divided by the instantaneous value of the applied load
NOTE This is often approximated to the instantaneous value of the friction force divided by the mean applied load. SIST EN 1071-13:2010

Although it is relatively easy in a pin-on-disk wear test to reproduce the contact stress experienced in a specific tribological contact, it might be necessary to use additional heating to ensure that the contact temperature approximates to that of the contact being simulated. The recommended test conditions in this standard should be used when the objective of the testing is to compare the performance of materials in the absence of well defined application conditions. 5 Principle The test consists in sliding a loaded pin against a flat disk such that the pin describes a circular path on the disk, and determining the wear of one or both. Depending on the wearing system being simulated, either the pin or disk or both may be coated with the ceramic coating under test, and testing may be either with or without lubrication. The pin contact face may have either a flat or rounded geometry. If the former is chosen, great care is necessary in order to ensure that the contact faces of pin and disk both lie in the same plane, as any variation from this will produce substantially different contact conditions from those expected for a plane contact. The high contact stress generated by misalignment can be particularly damaging to brittle ceramic materials and can lead to spurious and un-reproducible results. If a rounded geometry is chosen, then the contact conditions will vary throughout the test and affect the analysis of the results. 6 Apparatus
6.1 Pin-on-disk method testing apparatus
The testing apparatus shall consist of:  the holders for the disk and for the pin;  the drive system for rotating the disk or for letting the pin slide in a circular path on the fixed disk surface;  the loading mechanism for pushing the pin and the disk onto each other;
 means to determine the total sliding distance travelled by the pin over the surface of the disk during the test, e.g. rev counter, timer, etc. Depending on the equipment selected, the test face of the disk may be oriented in either a horizontal or vertical plane and, for the former the pin may be positioned either above or below the disk. Report the orientation used for the test. SIST EN 1071-13:2010

Where flat-ended pins are to be used, means shall be provided to ensure conformance between the pin and the disk so that the contact conditions are reproducible and the contact stress can be calculated, if required. NOTE 2 One technique that has been used to ensure conformance between a flat ended pin and the surface of the disk has been to grind a flat onto a spherical ball and to mount the ball into a spherical cavity, of the same diameter as the ball, which has been machined into the end of the pin – see Figure 1. Contacting the flat on the ball with the surface of the disk will ensure that conformance is obtained. The use of a pin with a spherical cavity will enable a ball of the same radius of curvature to be accommodated and to act as a ball-ended pin.
In all cases where the geometry referred to in Note 2 is used, the centre of curvature of the cavity shall lie on the, extended, axis of the pin. Equipment may be provided with a means to deliver lubricant to the contact zone and means to collect used lubricant to enable the isolation and analysis of wear debris. The testing apparatus may also have a mechanism for measuring the friction force during the test. This can be done e.g. by means of a load cell, a distortion measurement of a leaf spring, or a measurement of rotational torque. The measurement method should not affect any of the test conditions including the frictional condition and the applied load. It is recommended that the accuracy of friction measurement be ± 1 %, or better, of the applied load. The test system may also be fitted with a normal load cell to measure the applied normal load. The introduction of a normal load cell should not affect any of the test conditions. 12 Key 1 Cylindrical pin with spherical cavity of same radius as ball and centred on extended axis of pin 2 Ball with ground flat Figure 1
Diagram showing possible arrangement to obtain conformity between flat ended pin and disk 6.2 Test apparatus design requirements The apparatus shall be rigid such that during operation, the axis of the pin remains orthogonal to the plane of the test surface of the disk at all times. Any fluctuations in the position of the test surface of the disk relative to the mean position of the pin will result in fluctuations in the testing conditions and in particular in the applied load. Any such fluctuations in the applied load shall be less than 1 % of the nominal applied load. SIST EN 1071-13:2010

Although precise temperature and humidity conditions are not prescribed in this standard, typical ambient operating conditions are: temperature = (23 ± 2) °C; and humidity = (50 ±10) %.
NOTE 2
The use of a constant environment is necessary to help ensure the stable operation of the test equipment. It should not be considered a requirement of this standard that the tribological contact itself should be maintained under the same fixed conditions. Indeed, there are many situations where additional heating of the contact will be necessary to help ensure the conditions approximate to those in the contact being simulated.
NOTE 3
It has been found for some ceramic materials, see [7] and [8], that variations in humidity, particularly at low levels of humidity (< 40 %), can have far greater influence on the test results than variations in temperature. Report the conditions used during the test in the test report. 7 Preparation of test pieces 7.1 Substrate material and preparation Where the test is used to simulate the working conditions in a mechanical device it is recommended that the substrate materials chosen for both pin and plate be representative of the couple in that device. The materials should, where practical, have the same heat-treatment and surface preparation as the components being simulated so as to ensure that they possess the same load bearing capacity and surface texture.
In cases where the test is being used to rank coatings without a specific application in mind, both pin and plate shall be made from materials that will have minimum elastic and zero plastic deformation under the test conditions used. Depending on the test conditions to be investigated, suitable materials might be cemented carbide, cermets, SiC, alumina (> 96 %), hardened and tempered high speed steel, e.g. UNS T 11302 (AISI M2), hardened and tempered bearing steel, e.g. UNS G52986 (AISI E 52100 or 100Cr6), or stainless steel, e.g. UNS S41000 (AISI 410) but this list is by no means exhaustive and other materials might also be suitable. The materials shall be selected with due consideration to the influence of the subsequent coating operation on the final hardness.
Where a flat-ended pin is used, the flat end shall be orthogonal to the axis of the pin. Where a spherically-ended pin is used, the centre of curvature of the contact face shall lie on the axis of the pin. NOTE 2 Where a spherically-ended (ball-ended) pin is used, the ball radius should be selected so that, at the nominal applied load, the necessary contact pressure is produced. NOTE 3 Balls may be used in place of spherically-ended pins provided that they are held rigidly throughout the duration of the test. Pin and disk dimensions shall be such that no bending of the pin or test surface of the disk occurs during the test. 7.2 Coating deposition Where the test is being used to simulate the working conditions in a mechanical device, the substrate cleaning and deposition conditions selected for the coating shall be as near as practical the same as those that would be used for the components in that device. In particular, those process conditions that might influence the adhesion, chemical phase, preferred orientation or residual stress of the material being deposited shall be carefully monitored and controlled. In all cases, all relevant deposition conditions shall be recorded and this record shall form part of the test report. NOTE 1 In view of the likely influence of the adhesion, chemical phase, preferred orientation and residual stress on the coating performance, it is recommended that determination of these properties of the coating be made and the results reported. Techniques for determining these additional properties of ceramic coatings are reviewed in Annex A. In cases where the test is being used to rank coatings without a specific application in mind, deposition of the coating should follow procedures previously established for the material under investigation. If no established conditions exist, for example because the test forms part of a coatings development programme, then care should be taken to ensure that the conditions used are reproducible. Coating thickness should, where practical, be the same as that used in the device being simulated.
NOTE 2 If no device is being simulated then, depending on the purpose of the test, it is recommended that a range of coating thickness be evaluated. 7.3 Post-coating preparation In some instances, e.g. where the deposited coating is rough, the surface of the coating should be prepared in some way, e.g. by polishing, following its deposition. All procedures that modify the surface of the coating shall be documented in such a way that they are completely reproducible and this record shall form part of the test report. Where post-deposition preparation of the coating surface is used, care should be taken to remove all extraneous materials from the surface after treatment. SIST EN 1071-13:2010

Care should be taken to minimise material removal during any polishing operatio
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

Loading comments...

Die Norm EN 1071-13:2010 bietet eine umfassende Methodik zur Bestimmung der Abnutzungsrate von keramischen Beschichtungen, wobei der Pin-on-Disk-Test im Vordergrund steht. Der Umfang dieser Norm umfasst die Bewertung von Verschleißverhalten unter definierten Testbedingungen, bei denen ein stiftförmiger Prüfkörper mit einer flachen oder sphärisch endenden Oberfläche unter Last in Kontakt mit einer sich drehenden Platte gebracht wird. Diese Standardisierung ist besonders relevant für die Industrie, die sich mit fortschrittlichen technischen Keramiken und deren Anwendung in verschiedenen Bereichen beschäftigt. Ein hervorzuhebender Vorteil dieser Norm ist die Flexibilität, die sie bei der Wahl der Testparameter bietet. Die Möglichkeit, sowohl den Prüfstift als auch die Platte zu beschichten, erlaubt eine zielgenaue Anpassung an spezifische Anforderungen und Systeme. Dies ist besonders wichtig, um realistische Anwendungsbedingungen zu simulieren und relevante Testergebnisse zu erzielen. Darüber hinaus ist die Norm in der Lage, Beschichtungen in einer Dicke von 1 bis über 100 μm zu bewerten, was ihre Breite in der Anwendung erheblich erhöht. Ein weiterer Stärke der EN 1071-13:2010 ist die Option, sowohl unter trockenen als auch geschmierten Bedingungen zu testen, auch wenn sie nicht primär zur Beurteilung von Schmierstoffen konzipiert ist. Diese Flexibilität ermöglicht es, die Abnutzungsverhalten unter verschiedenen realen Einsatzbedingungen zu überprüfen. Bei Bedarf kann die Norm auch zur Analyse der adhäsiven oder kohäsiven Festigkeit von Beschichtungen eingesetzt werden, was zusätzlich wertvolle Informationen zur Materialauswahl und -anwendung liefert. Insgesamt ist die EN 1071-13:2010 ein bedeutendes Dokument für Fachleute im Bereich der Prüfung keramischer Beschichtungen. Ihre Methoden sind sowohl technisch fundiert als auch praktisch anwendbar und tragen zur Verbesserung der Leistungsfähigkeit und Zuverlässigkeit von Materialien in industriellen Anwendungen bei.

SIST EN 1071-13:2010 표준은 세라믹 코팅의 마모를 평가하기 위한 시험 방법을 명확히 규정하고 있으며, 주요 특징으로는 핀-디스크 방법을 통한 마모 속도 측정이 있습니다. 이 표준의 범위는 세라믹 코팅의 마모 특성을 다루고 있으며, 마모 특성의 평가에 있어 중요한 역할을 합니다. 이 표준의 강점 중 하나는 다양한 조건에서의 시험을 통해 세라믹 코팅의 내구성을 평가할 수 있는 점입니다. 특히, 시험에서 사용되는 핀과 디스크의 접촉 조건을 조절하여 세라믹 코팅의 마모 행동을 상세히 분석할 수 있습니다. 1μm부터 100μm 이상의 두께를 가진 코팅을 평가하는 데 적합하며, 조건에 따라 더 얇은 코팅에도 적용할 수 있는 유연성을 제공합니다. 또한, 이 표준은 마찰력을 측정할 수 있는 장비가 있는 경우, 슬라이딩 접촉에서 발생하는 마찰을 결정하는 데에도 활용될 수 있어, 세라믹 코팅의 전체적인 성능을 평가하는 데 기여합니다. 마모 이외에도 다양한 하중 조건에서의 시험을 통해 코팅의 접착 및 응집 강도에 대한 정보를 제공할 수 있어, 코팅의 전반적인 특성을 이해하는 데 도움이 됩니다. SIST EN 1071-13:2010 표준은 건조 또는 윤활 조건에서의 시험을 모두 수용할 수 있으며, 윤활제의 성질을 평가하기 위한 것이 아니라는 점에서 명확한 경계를 가지고 있습니다. 이로 인해, 세라믹 코팅의 마모 특성을 유연하게 평가할 수 있는 유용한 도구로 자리잡고 있습니다. 이러한 점에서 이 표준은 최신 기술과 연구에 기반하여 세라믹 코팅의 적용 가능성을 확장하는 데 있어 매우 중요한 공헌을 하고 있습니다.

The EN 1071-13:2010 standard outlines a comprehensive approach for evaluating the wear rate of ceramic coatings using the pin-on-disk method. Its scope encompasses a detailed methodology for assessing the wear performance of various ceramic coatings, making it a significant reference in the field of advanced technical ceramics. One of the principal strengths of this standard lies in its versatility. It accommodates a range of thicknesses, from 1μm to over 100μm, making it applicable to coatings of various specifications and applications. Additionally, it acknowledges the practicality of using both dry and lubricated conditions for testing, which is crucial as it provides a realistic simulation of operational environments. However, it is important to note that while lubricants are not the focus of the testing protocol, their interaction with the coating's wear behavior is recognized, allowing for a nuanced evaluation of materials in real-world applications. The method's ability to inform users about the adhesive and/or cohesive strength of the coatings under different loading conditions is another significant advantage. By understanding the wear behavior through the pin-on-disk approach, researchers and manufacturers can make informed decisions regarding material selection and application for various engineering and industrial needs. Overall, EN 1071-13:2010 serves as a vital standard for manufacturers and researchers dealing with ceramic coatings, offering a robust platform for wear evaluation. Its relevance in advancing the technical capabilities of ceramic materials cannot be overstated, providing a benchmark for quality and performance assessment that is essential in ensuring the longevity and durability of ceramic-based products.

標準EN 1071-13:2010は、セラミックコーティングの摩耗率を評価する手法を詳細に規定しています。この文書は、試験方法の標準化を図ることにより、セラミックコーティングの性能を正確に測定し、比較するための基盤を提供しています。 この標準の範囲は、平坦または球状のピンを用いて、ディスクの平面表面との接触を持たせ、相対運動を行うことによって摩耗を評価する方法を定義しています。これにより、テスト対象となるコーティングの摩耗特性を多角的に検証できる点が大きな強みです。また、テスト対象のコーティングが厚さ1μmから100μm以上まで対応しているため、さまざまな用途に適応できる柔軟性も加味されています。 さらに、摩擦の生成を評価するための適切な装置があれば、スライディングコンタクトにおける摩擦を測定することもできる点が、この標準の関連性を高めています。摩耗試験は乾燥条件または潤滑条件の下で実施できるため、実際の運用環境を模擬することが可能です。 また、さまざまな荷重条件で材料のペアを試験することで、コーティングの付着強度や内的強度に関する情報が得られるため、機械的性質の把握も可能です。これにより、材料の選定やコーティング技術の改善に寄与することが期待されます。 全体として、EN 1071-13:2010はセラミックコーティングの摩耗特性を科学的に評価するための信頼性の高い手法を提供し、セラミック業界における製品開発や品質管理において非常に重要な役割を果たしています。この標準の採用により、製品の競争力を向上させることができるでしょう。

La norme SIST EN 1071-13:2010 se concentre sur les méthodes d'essai pour les revêtements céramiques, en particulier pour la détermination du taux d'usure par la méthode du pin sur disque. Cette norme est d'une grande importance dans le domaine des céramiques techniques avancées, car elle fournit un cadre standardisé pour évaluer l'usure des revêtements céramiques dans des conditions contrôlées. L'un des principaux atouts de cette norme est sa capacité à tester des revêtements de céramique de différentes épaisseurs, allant de 1 à plus de 100 μm, ce qui la rend extrêmement polyvalente. De plus, en fonction des conditions choisies pour l'essai, il est possible d'appliquer ce test à des revêtements plus fins, ce qui élargit son champ d'application. Ce facteur est crucial pour les industries qui nécessitent des revêtements céramiques ultra-fins pour des applications spécifiques. La norme stipule également que le test peut être effectué dans des conditions sèches ou lubrifiées, offrant ainsi une flexibilité dans les modalités d'évaluation. Bien qu'il ne soit pas conçu spécifiquement pour tester les propriétés des lubrifiants, il permet de prendre en compte l'impact des lubrifiants sur le comportement d'usure des matériaux évalués. Cela montre que la norme intègre des scénarios pratiques du monde réel, rendant les résultats plus pertinents pour les applications industrielles. Un autre aspect important est que le test peut fournir des informations sur la force adhésive et/ou cohesive du revêtement, en plus de son comportement d'usure. Cela permet d'obtenir une compréhension complète des performances du revêtement dans des conditions d'utilisation réelles. En résumé, la norme SIST EN 1071-13:2010 démontre une solide pertinence dans l'évaluation des revêtements céramiques, grâce à sa méthodologie bien pensée, sa flexibilité d'application et sa capacité à fournir des données cruciales sur les comportements d'usure et d'adhésion.