ISO 18731:2025
(Main)Spices and condiments — Seasoning oil of Zanthoxyli pericarpium — Specification
Spices and condiments — Seasoning oil of Zanthoxyli pericarpium — Specification
This document specifies requirements for the seasoning oil of Zanthoxyli pericarpium.
Épices et condiments — Huile d'assaisonnement de Zanthoxyli pericarpium — Specification
General Information
Standards Content (Sample)
International
Standard
ISO 18731
First edition
Spices and condiments — Seasoning
2025-09
oil of Zanthoxyli pericarpium —
Specification
Épices et condiments — Huile d'assaisonnement de Zanthoxyli
pericarpium — Specification
Reference number
© ISO 2025
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ii
Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Requirements . 2
4.1 Sensory requirements.2
4.2 Physicochemical requirements .2
4.3 Contaminant limits .3
4.4 Mycotoxin limits .3
4.5 Pesticide residue limits .3
5 Packaging and marking . 3
5.1 Packaging .3
5.2 Marking .3
5.3 Storage and transport .4
Annex A (normative) Requirements relating to storage and transport conditions . 5
Annex B (normative) Ultraviolet spectrophotometry method for testing amides . 6
Annex C (normative) Method for testing residual hexa-alkane . 8
iii
Foreword
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This document was prepared by Technical Committee ISO/TC 34, Food products, Subcommittee SC 7, Spices,
culinary herbs and condiments.
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iv
Introduction
With the growth of global population and economic development, the demand for the quantities and varieties
of condiments is increasing, which promotes the significant growth of international trade volume and
types of condiments, including seasoning oil of Zanthoxyli pericarpium. Although the condiments industry
is developing rapidly, due to the lack of a unified standard for product quality and safety assurance, the
international trade of seasoning oil of Zanthoxyli pericarpium has not reached its potential.
This document standardizes the characteristics of seasoning oil of Zanthoxyli pericarpium, and provides
corresponding qualitative and quantitative methods to help with detection and identification, product
grading, scaling, standardized production, reducing trade and communication barriers, meeting increasing
demand in the international market, and promoting the commercialization and trade of seasoning oil of
Zanthoxyli pericarpium.
v
International Standard ISO 18731:2025(en)
Spices and condiments — Seasoning oil of Zanthoxyli
pericarpium — Specification
1 Scope
This document specifies requirements for the seasoning oil of Zanthoxyli pericarpium.
2 Normative references
The following documents are referred to in the text in such a way that some or all of their content constitutes
requirements of this document. For dated references, only the edition cited applies. For undated references,
the latest edition of the referenced document (including any amendments) applies.
ISO 660, Animal and vegetable fats and oils — Determination of acid value and acidity
ISO 662, Animal and vegetable fats and oils — Determination of moisture and volatile matter content
ISO 3960, Animal and vegetable fats and oils — Determination of peroxide value — Iodometric (visual) endpoint
determination
ISO 9832, Animal and vegetable fats and oils — Determination of residual technical hexane content
ISO 15302, Animal and vegetable fats and oils — Determination of benzo[a]pyrene — Reverse-phase high
performance liquid chromatography method
ISO 16050, Foodstuffs — Determination of aflatoxin B1, and the total content of aflatoxins B1, B2, G1 and G2 in
cereals, nuts and derived products — High-performance liquid chromatographic method
CXS 193, General standard for contaminants and toxins in food and feed
Codex Pesticides Residues in Food Online Database. Available at : https:// www .fao .org/ fao -who
-codexalimentarius/ codex -texts/ dbs/ pestres/ en/
3 Terms and definitions
For the purposes of this document, the terms and definitions given in ISO 9832 and the following apply.
ISO and IEC maintain terminology databases for use in standardization at the following addresses:
— ISO Online browsing platform: available at https:// www .iso .org/ obp
— IEC Electropedia: available at https:// www .electropedia .org/
3.1
seasoning oil of Zanthoxyli pericarpium
oil made from Zanthoxyli pericarpium fruits as the main raw material, using vegetable oil extraction, filtration
or supercritical CO extraction, cold pressing and other methods, via diluting with vegetable oil and filtering
Note 1 to entry: Zanthoxyli pericarpium includes red prickly ash pepper (Zanthoxylum bungeanum Maxim. Syn.
Zanthoxylum bungei Planch), green prickly ash pepper (Zanthoxylum schinifolium Sieb.et Zucc.), bamboo prickly ash
pepper (Zanthoxylum armatum DC.), Chinese pepper (Zanthoxylum acanthopodium DC.), Japanese pepper (Zanthoxylum
piperitum DC.).
3.2
residual solvent content
content of volatile hydrocarbons such as those remaining in fats following processing involving the use of
hydrocarbon solvents
Note 1 to entry: The residual solvent is determined according to the method specified in this document.
Note 2 to entry: The content is expressed as milligrams of volatile hydrocarbons per kilogram of sample.
[SOURCE: ISO 9832:2002, 3.1, modified — Term changed from “residual technical hexane content”. Last part
of the definition moved to a note to entry.]
3.3
matrix oil
vegetable oil used for dilution of oil of Zanthoxyli pericarpium to make its seasoning oil, when used for
purpose of analysis of the product
Note 1 to entry: The matrix oil is obtained by refining processes such as deodorization and decolorization or by
ultrasonic degassing at room temperature.
4 Requirements
4.1 Sensory requirements
The seasoning oil of Zanthoxyli pericarpium shall conform to the sensory requirements given in Table 1.
Table 1 — Sensory requirements
Characteristics Requirements Method of test
Appearance Oily liquid, clear, no visible foreign matter.
Place an appropriate sample in a 50 ml
beaker; observe appearance and colour
Colour Seasoning oil shall have the characteristics colour
under sunlight.
of the spice or oil depending on the process used.
Flavour The flavour contains the characteristic of Zanthox-
Pour the sample into a 150 ml beaker.
yli pericarpium fruit. The product shall be free from
Heat the water bath to 50 °C. Stir the
foreign flavours.
contents quickly with a glass stick and
Taste The taste contains the characteristic of Zanthoxyli
smell it. Gargle with warm water and
pericarpium fruit. The product shall be free from
then taste it.
foreign taste.
4.2 Physicochemical requirements
The seasoning oil of Zanthoxyli pericarpium shall conform to the physicochemical requirements given in
Table 2.
Table 2 — Physicochemical requirements
Requirements
Characteristics Method of test
Grade I Grade II
Acid value (KOH) (mg/g), max. 3,0 3,0 ISO 660
Peroxide value (meq/kg), max. 20,0 20,0 ISO 3960
Moisture content (g/100 g), max. 0,8 0,8 ISO 662
Amides (mg/g), min. 5,0 4,0 Annex B
Annex C, when using
hexa-alkane solvent as the
extraction solvent.
20,0 (for solvent 20,0 (for solvent
extracted oil) extracted oil)
ISO 9832, when using
Residual solvent (mg/kg), max.
technical hexane solvent
as the extraction solvent.
Not detectable Not detectable
Annex C or ISO 9832
a a
(for pressed oil) (for pressed oil)
a
When the detection value is less than 10 mg/kg, it is regarded as not detected.
4.3 Contaminant limits
The seasoning oil of Zanthoxyli pericarpium shall conform to the contaminant limits requirements given in
Table 3.
Table 3 — Contaminant limits requirements
Characteristics Requirements Method of test
Lead (mg/kg), max. 0,08 CXS 193
Arsenic (mg/kg), max. 0,1 CXS 193
benzo[a]pyrene (μg/kg), max. 2,0 ISO 15302
4.4 Mycotoxin limits
Aflatoxin shall be tested in accordance with the testing methods specified in ISO 16050. Total aflatoxin
limits shall not exceed 10 μg/kg.
4.5 Pesticide residue limits
All ingredients in the seasoning oil of Zanthoxyli pericarpium shall comply with maximum pesticide residue
limits specified in the Codex Pesticide Residues in Food Online Database.
5 Packaging and marking
5.1 Packaging
The seasoning oil of Zanthoxyli pericarpium shall be packed in sealed, clean and sound containers made of
material which does not affect the product quality and which protects it from environmental effects. The
packing material shall not permit the ingress of moisture and air.
5.2 Marking
The con
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