Determination of density by volumetric displacement — Skeleton density by gas pycnometry

ISO 12154:2014 specifies a method for rapid and efficient determination of the skeleton density of solid material samples of regular or irregular shape, whether powdered or in one piece, by means of a gas displacement pycnometer.

Détermination de la masse volumique par déplacement volumétrique — Masse volumique du squelette mesurée par pycnométrie à gaz

General Information

Status
Published
Publication Date
18-Mar-2014
Current Stage
9020 - International Standard under periodical review
Start Date
15-Apr-2024
Completion Date
15-Apr-2024
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INTERNATIONAL ISO
STANDARD 12154
First edition
2014-04-01
Determination of density by
volumetric displacement — Skeleton
density by gas pycnometry
Détermination de la masse volumique par déplacement
volumétrique — Masse volumique du squelette mesurée par
pycnométrie à gaz
Reference number
ISO 12154:2014(E)
©
ISO 2014

---------------------- Page: 1 ----------------------
ISO 12154:2014(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2014
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
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Published in Switzerland
ii © ISO 2014 – All rights reserved

---------------------- Page: 2 ----------------------
ISO 12154:2014(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols and abbreviated terms . 2
5 Principle of the method . 2
6 Apparatus and procedure . 3
6.1 Apparatus . 3
6.2 Sample pre-treatment and determination of sample mass . 4
6.3 Determination of the solid skeleton volume of the sample . 5
6.4 Calculation of skeleton density . 6
6.5 Calibration procedure . 6
7 Test report . 8
Annex A (informative) Interferences . 9
Bibliography .11
© ISO 2014 – All rights reserved iii

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ISO 12154:2014(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison wit
...

DRAFT INTERNATIONAL STANDARD ISO/DIS 12154
ISO/TC 24/SC 4 Secretariat: DIN
Voting begins on Voting terminates on

2012-05-04 2012-10-04
INTERNATIONAL ORGANIZATION FOR STANDARDIZATION  •  МЕЖДУНАРОДНАЯ ОРГАНИЗАЦИЯ ПО СТАНДАРТИЗАЦИИ  •  ORGANISATION INTERNATIONALE DE NORMALISATION


Determination of density by volumetric displacement —
Skeleton density by gas pycnometry
Détermination de la masse volumique par déplacement volumétrique — Masse volumique du squelette
mesurée par pycnométrie à gaz
ICS 19.120













To expedite distribution, this document is circulated as received from the committee
secretariat. ISO Central Secretariat work of editing and text composition will be undertaken at
publication stage.
Pour accélérer la distribution, le présent document est distribué tel qu'il est parvenu du
secrétariat du comité. Le travail de rédaction et de composition de texte sera effectué au
Secrétariat central de l'ISO au stade de publication.



THIS DOCUMENT IS A DRAFT CIRCULATED FOR COMMENT AND APPROVAL. IT IS THEREFORE SUBJECT TO CHANGE AND MAY NOT BE
REFERRED TO AS AN INTERNATIONAL STANDARD UNTIL PUBLISHED AS SUCH.
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THEY ARE AWARE AND TO PROVIDE SUPPORTING DOCUMENTATION.
©  International Organization for Standardization, 2012

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ISO/DIS 12154

Copyright notice
This ISO document is a Draft International Standard and is copyright-protected by ISO. Except as permitted
under the applicable laws of the user’s country, neither this ISO draft nor any extract from it may be
reproduced, stored in a retrieval system or transmitted in any form or by any means, electronic,
photocopying, recording or otherwise, without prior written permission being secured.
Requests for permission to reproduce should be addressed to either ISO at the address below or ISO’s
member body in the country of the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Reproduction may be subject to royalty payments or a licensing agreement.
Violators may be prosecuted.

ii © ISO 2012 – All rights reserved

---------------------- Page: 2 ----------------------
ISO/DIS 12154
Contents Page
Foreword . iv
Introduction . iv
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Symbols and abbreviated terms . 2
5 Principle of the method . 2
6 Apparatus and procedure . 3
6.1 Apparatus . 3
6.2 Sample pre-treatment and determination of sample mass . 4
6.3 Determination of the solid skeleton volume of the sample . 5
6.3.1 Pycnometric measurement . 5
6.3.2 Calculation of the skeleton volume of the sample . 6
6.4 Calculation of skeleton density . 6
6.5 Calibration procedure . 6
6.5.1 General remarks .
...

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