Plastics — Epoxy resins — Part 2: Preparation of test specimens and determination of properties

ISO 3673-2:2007 specifies the methods of preparation of test specimens and the test methods to be used in determining the properties of epoxy resins. Requirements for handling test material and for conditioning both the test material before moulding and the specimens before testing are given. Properties of crosslinked epoxy resins have been selected from the general test methods in ISO 10350‑1:1998. Other test methods in wide use with, or of particular significance to, epoxy resins, particularly properties useful for the processing of non-crosslinked epoxy resins, are also included.

Plastiques — Résines époxydes — Partie 2: Préparation des éprouvettes et détermination des propriétés

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Status
Withdrawn
Publication Date
21-Aug-2007
Withdrawal Date
21-Aug-2007
Current Stage
9599 - Withdrawal of International Standard
Completion Date
09-Jul-2012
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ISO 3673-2:2007 - Plastics -- Epoxy resins
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INTERNATIONAL ISO
STANDARD 3673-2
Second edition
2007-09-01


Plastics — Epoxy resins —
Part 2:
Preparation of test specimens and
determination of properties
Plastiques — Résines époxydes —
Partie 2: Préparation des éprouvettes et détermination des propriétés




Reference number
ISO 3673-2:2007(E)
©
ISO 2007

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ISO 3673-2:2007(E)
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ii © ISO 2007 – All rights reserved

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ISO 3673-2:2007(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies
(ISO member bodies). The work of preparing International Standards is normally carried out through ISO
technical committees. Each member body interested in a subject for which a technical committee has been
established has the right to be represented on that committee. International organizations, governmental and
non-governmental, in liaison with ISO, also take part in the work. ISO collaborates closely with the
International Electrotechnical Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International Standards
adopted by the technical committees are circulated to the member bodies for voting. Publication as an
International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 3673-2 was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 12, Thermosetting
materials.
This second edition cancels and replaces the first edition (ISO 3673-2:1999), which has been technically
revised.
ISO 3673 consists of the following parts, under the general title Plastics — Epoxy resins:
⎯ Part 1: Designation
⎯ Part 2: Preparation of test specimens and determination of properties
© ISO 2007 – All rights reserved iii

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ISO 3673-2:2007(E)
Introduction
The purpose of this part of ISO 3673 is to designate procedures for the determination of intrinsic properties of
epoxy resins (EP). It specifies procedures and conditions for the preparation of test specimens of epoxy resins
in a specified state, and methods for measuring their properties. Those properties and test methods which are
suitable and necessary for characterizing epoxy resins are listed. Because of the specificity of thermosetting
resins like epoxy resins, contrary to other plastic products, a distinction is made between the presentation of
the properties before crosslinking (characteristics which are useful for processing) and after crosslinking
(intrinsic characteristics).

iv © ISO 2007 – All rights reserved

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INTERNATIONAL STANDARD ISO 3673-2:2007(E)

Plastics — Epoxy resins —
Part 2:
Preparation of test specimens and determination of properties
SAFETY STATEMENT — Persons using this document should be familiar with normal laboratory
practice, if applicable. This document does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user to establish appropriate safety and health
practices and to ensure compliance with any regulatory requirements.
1 Scope
This part of ISO 3673 specifies the methods of preparation of test specimens and the test methods to be used
in determining the properties of epoxy resins. Requirements for handling test material and for conditioning
both the test material before moulding and the specimens before testing are given.
Properties of crosslinked epoxy resins have been selected from the general test methods in
ISO 10350-1:1998. Other test methods in wide use with, or of particular significance to, epoxy resins,
particularly properties useful for the processing of non-crosslinked epoxy resins, are also included in this part
of ISO 3673.
In order to obtain reproducible and comparable test results, it is necessary to use the test methods, sample
preparation and conditioning, and specimen dimensions specified herein. Values determined will not
necessarily be identical to those obtained using test specimens of different dimensions or prepared using
different procedures.
Other standards exist concerning the determination of properties and preparation of test specimens for epoxy-
based products, to which reference will be made, if required.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.
ISO 62, Plastics — Determination of water absorption
ISO 75-2, Plastics — Determination of temperature of deflection under load — Part 2: Plastics and ebonite
ISO 178, Plastics — Determination of flexural properties
ISO 179-1, Plastics — Determination of Charpy impact properties — Part 1: Non-instrumented impact test
ISO 179-2, Plastics — Determination of Charpy impact properties — Part 2: Instrumented impact test
ISO 527-2, Plastics — Determination of tensile properties — Part 2: Test conditions for moulding and
extrusion plastics
ISO 760, Determination of water — Karl Fischer method (General method)
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ISO 3673-2:2007(E)
ISO 1183-1, Plastics — Methods for determining the density of non-cellular plastics — Part 1: Immersion
method, liquid pyknometer method and titration method
ISO 1523, Determination of flash point — Closed cup equilibrium method
ISO 1675, Plastics — Liquid resins — Determination of density by the pyknometer method
ISO 2555, Plastics — Resins in the liquid state or as emulsions or dispersions — Determination of apparent
viscosity by the Brookfield Test method
ISO 2577, Plastics — Thermosetting moulding materials — Determination of shrinkage
ISO 2592, Determination of flash and fire points — Cleveland open cup method
ISO 2719, Determination of flash point — Pensky-Martens closed cup method
ISO 2811 (all parts), Paints and varnishes — Determination of density
ISO 2818, Plastics — Preparation of test specimens by machining
ISO 3001, Plastics — Epoxy compounds — Determination of epoxy equivalent
ISO 3104, Petroleum products — Transparent and opaque liquids — Determination of kinematic viscosity and
calculation of dynamic viscosity
ISO 3105, Glass capillary kinematic viscometers — Specifications and operating instructions
ISO 3146, Plastics — Determination of melting behaviour (melting temperature or melting range) of semi-
crystalline polymers by capillary tube and polarizing-microscope methods
ISO 3167, Plastics — Multipurpose test specimens
ISO 3219, Plastics — Polymers/resins in the liquid state or as emulsions or dispersions — Determination of
viscosity using a rotational viscometer with defined shear rate
ISO 3521, Plastics — Unsaturated polyesters and epoxy resins — Determination of overall volume shrinkage
ISO 3679, Determination of flash point — Rapid equilibrium closed cup method
ISO 4589-2, Plastics — Determination of burning behaviour by oxygen index — Part 2: Ambient-temperature
test
ISO 4615, Plastics — Unsaturated polyesters and epoxide resins — Determination of total chlorine content
ISO 4625-1, Binders for paints and varnishes — Determination of softening point — Part 1: Ring-and-ball
method
ISO 4630-1, Clear liquids — Estimation of colour by the Gardner colour scale — Part 1: Visual method
ISO 4895, Plastics — Liquid epoxy resins — Determination of tendency to crystallize
ISO 6271-1, Clear liquids — Estimation of colour by the platinum-cobalt scale — Part 1: Visual method
ISO 7142, Binders for paints and varnishes — Epoxy resins — General methods of test
ISO 10350-1:1998, Plastics — Acquisition and presentation of comparable single-point data — Part 1:
Moulding materials
2 © ISO 2007 – All rights reserved

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ISO 3673-2:2007(E)
ISO 11357-2, Plastics — Differential scanning calorimetry (DSC) — Part 2: Determination of glass transition
temperature
ISO 11359-2, Plastics — Thermomechanical analysis (TMA) — Part 2: Determination of coefficient of linear
thermal expansion and glass transition temperature
ISO 12058-1, Plastics — Determination of viscosity using a falling-ball viscometer — Part 1: Inclined-tube
method
ISO 21627-1, Plastics — Epoxy resins — Determination of chlorine content — Part 1: Inorganic chlorine
ISO 21627-2, Plastics — Epoxy resins — Determination of chlorine content — Part 2: Easily saponifiable
chlorine
ISO 21627-3, Plastics — Epoxy resins — Determination of chlorine content — Part 3: Total chlorine
IEC 60093, Methods of test for volume resistivity and surface resistivity of solid electrical insulating materials
IEC 60112, Method for the determination of the proof and the comparative tracking indices of solid insulating
materials
IEC 60243-1, Electrical strength of insulating materials — Test methods — Part 1: Tests at power frequencies
IEC 60250, Recommended methods for the determination of the permittivity and dielectric dissipation factor of
electrical insulating materials at power, audio and rad
...

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