ISO/DTS 16774-2

Test methods for repair materials for water-leakage cracks in underground concrete structures — Part 2: Test method for chemical resistance

Méthodes d'essai pour matériaux de réparation pour fissures dues à l'eau dans les structures en béton souterraines — Partie 2: Méthode d'essai de la résistance chimique

General Information

• Status: Not Published
• ICS: 91.080.40 - Concrete structures
• Technical Committee: ISO/TC 71/SC 7 - Maintenance and repair of concrete structures
• Drafting Committee: ISO/TC 71/SC 7/WG 3 - Leakage due to Cracks
• Current Stage: 5020 - FDIS ballot initiated: 2 months. Proof sent to secretariat
• Start Date: 19-Jan-2023
• Completion Date: 19-Jan-2023

Relations

• Revises: ISO/TS 16774-2:2016 - Test methods for repair materials for water-leakage cracks in underground concrete structures — Part 2: Test method for chemical resistance
• Effective Date: 08-May-2020

Standards Content (Sample)

TECHNICAL SPECIFICATION
ISO /DTS/TS 16774-2 Ed.2:2023(E)
2022-12Date: 2023-01-05
ISO/ TC 71/SC 7
Secretariat: KATS

Test methods for repair materials for water-leakage cracks in underground concrete structures

— Part 2: Test method for chemical resistance
Part 2:
Test method for chemical resistance
RECIPIENTS OF THIS DRAFT ARE INVITED TO
SUBMIT, WITH THEIR COMMENTS,
NOTIFICATION OF ANY RELEVANT PATENT
RIGHTS OF WHICH THEY ARE AWARE AND TO
PROVIDE SUPPORT- ING DOCUMENTATION IN
ADDITION TO THEIR EVALUATION AS BEING
ACCEPTABLE FOR INDUSTRIAL, TECHNO-
LOGICAL, COMMERCIAL AND USER PURPOSES,
DRAFT INTERNATIONAL STANDARDS MAY ON
OCCASION HAVE TO BE CONSIDERED IN THE
LIGHT OF THEIR POTENTIAL TO BECOME STAN-
DARDS TO WHICH REFERENCE MAY BE MADE
IN NATIONAL REGULATIONS.
---------------------- Page: 1 ----------------------
ISO/TS 26774-2:2016(E)
© ISO 2023

All rights reserved. Unless otherwise specified, or required in the context of its implementation, no

part of this publication may be reproduced or utilized otherwise in any form or by any means,

electronic or mechanical, including photocopying, or posting on the internet or an intranet, without

prior written permission. Permission can be requested from either ISO at the address below or ISO’s

member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: [phone]
Fax: [phone]
Email: [e-mail]
Website: www.iso.org
Published in Switzerland
© ISO 2016
---------------------- Page: 2 ----------------------
ISO DTS/TS 16774-2:2022(Ed.2)
Contents Page

Foreword................................................................................................................................................................ v

1 Scope…................................................................................................................................................................ 1

2 Normative references.................................................................................................................................... 1

3 Terms and Definitions…............................................................................................................................... 1

4 Principle ........................................................................................................................................................... 1

5 Apparatus ........................................................................................................................................................ 2

5.1 Container...................................................................................................................................................... 2

5.2 Others ........................................................................................................................................................... 2

6 Preparation .................................................................................................................................................... 2

6.1 Test specimens ........................................................................................................................................... 2

6.2 Chemical substance .................................................................................................................................. 2

6.3 Ambient Conditions ................................................................................................................................... 2

Procedure .........................................................................................................................................../...........................................

........................................................................................................................ 2

8 Expression of results .................................................................................................................................... 3

9 Test report ....................................................................................................................................................... 3

9.1 Information on the repair material of the test target ................................................................... 3

9.1.1 General …………......................................................................................................................................... 3

9.1.2 Other information ….............................................................................................................................. 3

9.2 Information on the test ........................................................................................................................... 3

Bibliography....................................................................................................................................................... 4

Annex.................................................................................................................................................................... 5

iii
© ISO 20162020
---------------------- Page: 3 ----------------------
ISO/TS 26774-2:2016(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national

standards bodies (ISO member bodies). The work of preparing International Standards is normally

carried out through ISO technical committees. Each member body interested in a subject for which a

technical committee has been established has the right to be represented on that committee.

International organizations, governmental and non-governmental, in liaison with ISO, also take part in

the work. ISO collaborates closely with the International Electrotechnical Commission (IEC) on all

matters of electrotechnical standardization.

The procedures used to develop this document and those intended for its further maintenance are

described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the

different types of ISO documents should be noted. This document was drafted in accordance with the

editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directiveswww.iso.org/directives).

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of

any patent rights identified during the development of the document will be in the Introduction

and/or on the ISO list of patent declarations received (see www.iso.org/patentswww.iso.org/patents).

Any trade name used in this document is information given for the convenience of users and does not

constitute an endorsement.

For an explanation onof the voluntary nature of standards, the meaning of ISO specific terms and

expressions related to conformity assessment, as well as information about ISO's adherence to the

World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT)), see the

following URL: www.iso.org/iso/foreword.htmlwww.iso.org/iso/foreword.html.

The committee responsible for thisThis document iswas prepared by Technical Committee ISO/TC 71,

Concrete, reinforced concrete and pre-stressed concrete, Subcommittee SC 7, Maintenance and repair of

concrete structures.

This second edition cancels and replaces the first edition (ISO/TS 16774 consist-2:2016) which has

been technically revised.
The main changes are as follows:
— ambient conditions in 6.3 and A.3.3 have been modified;
— some clarifications have been made in Clause 7 and 9.2;
— some editorial corrections have been made.

A list of the followingall parts, under in the general title Test methods for repair materials for water-

leakage cracks in underground concrete structures:ISO 16774 series can be found on the ISO website.

— Part 1: Test method for thermal stability
— Part 2: Test method for chemical resistance
— Part 3: Test method for water (wash out) resistance
— Part 4: Test method for adhesion on wet concrete surface
— Part 5: Test method for watertightness
© ISO 2016
---------------------- Page: 4 ----------------------
ISO DTS/TS 16774-2:2022(Ed.2)
— Part 6: Test method for response to the substrate movement
© ISO 20162020
---------------------- Page: 5 ----------------------
ISO/DTS 16774-2:2023(E)

Any feedback or questions on this document should be directed to the user’s national standards body.

A complete listing of these bodies can be found at www.iso.org/members.html.
ii © ISO 2023 – All rights reserved
---------------------- Page: 6 ----------------------
ISO/DTS 16774-2:2023(E)
Introduction

This Technical Specificationdocument is linked to ISO/TR 16475. ISO/TR 16475 outlines 6six basic

properties and the required performance levels of water leakage repair materials, and the

ISO/TS 16774 series proposes sample testing methods that are capable of evaluating the respective

properties of the repair materials.

The test methods in this Technical Specificationdocument are intended to serve as a reference for

nations that have not yet developed a test method on the 6six required performance properties of

water leakage repair materials. If other forms of test methods that are simpler, more accurate or more

organized are available, such methods are recommended for use instead. Many of the dependent

variables outlined in the reference test methods of this Technical Specificationdocument are subject to

change in accordance with the environmental conditions (temperature and humidity, chemical

solution and concentration, width of movement activity, water pressure or water flow velocity, etc.)

outlined in the standards used in respective countries.

For ISO/TS 16774-1, ISO/TS 16774-5 and ISO/TS 16774-6, for the purpose of objectively comparing

the performance of injected repair materials, artificial cracks of same width, height, and volume were

used to control the usage of repair materials for each testing cycle and enable repetition of the same

test methods under the same conditions.
iii
© ISO 2020
© ISO 2023 – All rights reserved iii
---------------------- Page: 7 ----------------------
TECHNICAL SPECIFICATION ISO/DTS 16774-2:2023(E)

Test methods for repair materials for water-leakage cracks in underground concrete structures

— Part 2: Test method for chemical resistance
1 Scope

This part of ISO/TS 16774document specifies a laboratory test method for the qualitative

determination of the retention level of chemical resistance of repair materials in repaired cracks of

concrete structures in conditions where the material is either underwater or in contact with water

that maycan have various chemical components present.
2 Normative references

The following documents, are referred to in wholethe text in such a way that some or in part, are

normatively referenced inall of their content constitutes requirements of this document and are

indispensable for its application. For dated references, only the edition cited applies. For undated

references, the latest edition of the referenced document (including any amendments) applies.

ISO/TR 16475, GuidelinesGeneral practices for the repair of water-leakage cracks in concrete structures

3 Terms and definitions

For the purposes of this document, the terms and definitions given in ISO/TR 16475 and the following

apply.

ISO and IEC maintain terminology databases for use in standardization at the following addresses:

— ISO Online browsing platform: available at https://www.iso.org/obp
— IEC Electropedia: available at https://www.electropedia.org/
3.1
water leakage repair material for water-leakage cracks
grouting materials used to prevent water- leakages in concrete cracks

Note 1 to entry: In this Technical Specificationdocument, target ingredients are limited to injection materials

outlined in ISO/TR 16475.
4 Principle

A repair material’s resistance to chemical attacks is one of the fundamental properties that water-

leakage repair materials should possess. Repair materials can undergo chemical property changes

due to chemical attack. Harmful chemical substances can also corrode the repair material and reduce

their ability to prevent water leakage. This test method evaluates a water- leakage repair material’s

chemical resistance performance by determining if the tested material can maintain as closely as

possible its original mass after being exposed to various types of chemical substances as a means to

evaluate the material’s resistance against chemical corrosion. In this method, comparing the mass

difference of water leakage repair materials before and after chemical exposure can be used to

determine the repair material’s chemical resistance level. An example test method is provided in

Annex A.
© ISO 2023 – All rights reserved 1
---------------------- Page: 8 ----------------------
ISO/DTS 16774-2:2023(E)

The tested repair material sample prepared in a Petri dish is placed in a container and completely

immersed in chemical solutions for predetermined number of hours or days (values subject to change

in accordance towith different national standards). The concentration of the tested chemical solution

follows the condition of the applied environment belonging to different national standards, meaning

test chemical substances that represent common chemical substances that are exposed to concrete

material and repair materials, as well as exposure time and chemical concentration range values

should reflect the applicable environmental conditions.

Test specimens are treated so that they remain in a stable state prior to immersion in chemical

substance so that physical factors such as swelling, pore-filling, or bubbling do not affect the principles

of this test method. The mass of the test specimen after immersion in chemical substance is measured

using an electronic scale
...

FINAL
TECHNICAL ISO/DTS
DRAFT
SPECIFICATION 16774-2
ISO/TC 71/SC 7
Test methods for repair materials for
Secretariat: KATS
water-leakage cracks in underground
Voting begins on:
2023-01-19 concrete structures —
Voting terminates on:
Part 2:
2023-03-16
Test method for chemical resistance
Méthodes d'essai pour matériaux de réparation pour fissures dues à
l'eau dans les structures en béton souterraines —
Partie 2: Méthode d'essai de la résistance chimique
RECIPIENTS OF THIS DRAFT ARE INVITED TO
SUBMIT, WITH THEIR COMMENTS, NOTIFICATION
OF ANY RELEVANT PATENT RIGHTS OF WHICH
THEY ARE AWARE AND TO PROVIDE SUPPOR TING
DOCUMENTATION.
IN ADDITION TO THEIR EVALUATION AS
Reference number
BEING ACCEPTABLE FOR INDUSTRIAL, TECHNO-
ISO/DTS 16774-2:2023(E)
LOGICAL, COMMERCIAL AND USER PURPOSES,
DRAFT INTERNATIONAL STANDARDS MAY ON
OCCASION HAVE TO BE CONSIDERED IN THE
LIGHT OF THEIR POTENTIAL TO BECOME STAN-
DARDS TO WHICH REFERENCE MAY BE MADE IN
NATIONAL REGULATIONS. © ISO 2023
---------------------- Page: 1 ----------------------
ISO/DTS 16774-2:2023(E)
FINAL
TECHNICAL ISO/DTS
DRAFT
SPECIFICATION 16774-2
ISO/TC 71/SC 7
Test methods for repair materials for
Secretariat: KATS
water-leakage cracks in underground
Voting begins on:
concrete structures —
Voting terminates on:
Part 2:
Test method for chemical resistance
Méthodes d'essai pour matériaux de réparation pour fissures dues à
l'eau dans les structures en béton souterraines —
Partie 2: Méthode d'essai de la résistance chimique
COPYRIGHT PROTECTED DOCUMENT
© ISO 2023

All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may

be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting on

the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address below

or ISO’s member body in the country of the requester.
RECIPIENTS OF THIS DRAFT ARE INVITED TO
ISO copyright office
SUBMIT, WITH THEIR COMMENTS, NOTIFICATION
OF ANY RELEVANT PATENT RIGHTS OF WHICH
CP 401 • Ch. de Blandonnet 8
THEY ARE AWARE AND TO PROVIDE SUPPOR TING
CH-1214 Vernier, Geneva
DOCUMENTATION.
Phone: [phone]
IN ADDITION TO THEIR EVALUATION AS
Reference number
Email: [e-mail]
BEING ACCEPTABLE FOR INDUSTRIAL, TECHNO-
ISO/DTS 16774-2:2023(E)
Website: www.iso.org
LOGICAL, COMMERCIAL AND USER PURPOSES,
DRAFT INTERNATIONAL STANDARDS MAY ON
Published in Switzerland
OCCASION HAVE TO BE CONSIDERED IN THE
LIGHT OF THEIR POTENTIAL TO BECOME STAN-
DARDS TO WHICH REFERENCE MAY BE MADE IN
© ISO 2023 – All rights reserved
NATIONAL REGULATIONS. © ISO 2023
---------------------- Page: 2 ----------------------
ISO/DTS 16774-2:2023(E)
Contents Page

Foreword ........................................................................................................................................................................................................................................iv

Introduction .................................................................................................................................................................................................................................v

1 Scope ................................................................................................................................................................................................................................. 1

2 Normative references ..................................................................................................................................................................................... 1

3 Terms and definitions .................................................................................................................................................................................... 1

4 Principle ........................................................................................................................................................................................................................ 1

5 Apparatus .................................................................................................................................................................................................................... 2

5.1 Container. .................................................................................................................................................................................................... 2

5.2 Others. ............................................................................................................................................................................................................ 2

6 Preparation ............................................................................................................................................................................................................... 2

6.1 Test specimens........................................................................................................................................................................................ 2

6.2 Chemical substance ............................................................................................................................................................................ 2

6.3 Ambient conditions............................................................................................................................................................................. 3

7 Procedure ....................................................................................................................................................................................................................3

8 Expression of results ....................................................................................................................................................................................... 3

9 Test report .................................................................................................................................................................................................................. 4

9.1 Information on the repair material of the test target .......................................................................................... 4

9.1.1 General ........................................................................................................................................................................................ 4

9.1.2 Other information ............................................................................................................................................................. 4

9.2 Information on the test ................................................................................................................................................................... 4

Annex A (informative) Example test method ............................................................................................................................................. 5

Bibliography ................................................................................................................................................................................................................................ 8

iii
© ISO 2023 – All rights reserved
---------------------- Page: 3 ----------------------
ISO/DTS 16774-2:2023(E)
Foreword

ISO (the International Organization for Standardization) is a worldwide federation of national standards

bodies (ISO member bodies). The work of preparing International Standards is normally carried out

through ISO technical committees. Each member body interested in a subject for which a technical

committee has been established has the right to be represented on that committee. International

organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.

ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of

electrotechnical standardization.

The procedures used to develop this document and those intended for its further maintenance are

described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the

different types of ISO documents should be noted. This document was drafted in accordance with the

editorial rules of the ISO/IEC Directives, Part 2 (see www.iso.org/directives).

Attention is drawn to the possibility that some of the elements of this document may be the subject of

patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of

any patent rights identified during the development of the document will be in the Introduction and/or

on the ISO list of patent declarations received (see www.iso.org/patents).

Any trade name used in this document is information given for the convenience of users and does not

constitute an endorsement.

For an explanation of the voluntary nature of standards, the meaning of ISO specific terms and

expressions related to conformity assessment, as well as information about ISO's adherence to

the World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT), see

www.iso.org/iso/foreword.html.

This document was prepared by Technical Committee ISO/TC 71, Concrete, reinforced concrete and pre-

stressed concrete, Subcommittee SC 7, Maintenance and repair of concrete structures.

This second edition cancels and replaces the first edition (ISO/TS 16774-2:2016) which has been

technically revised.
The main changes are as follows:
— ambient conditions in 6.3 and A.3.3 have been modified;
— some clarifications have been made in Clause 7 and 9.2;
— some editorial corrections have been made.
A list of all parts in the ISO 16774 series can be found on the ISO website.

Any feedback or questions on this document should be directed to the user’s national standards body. A

complete listing of these bodies can be found at www.iso.org/members.html.
© ISO 2023 – All rights reserved
---------------------- Page: 4 ----------------------
ISO/DTS 16774-2:2023(E)
Introduction

This document is linked to ISO/TR 16475. ISO/TR 16475 outlines six basic properties and the required

performance levels of water leakage repair materials, and the ISO/TS 16774 series proposes sample

testing methods that are capable of evaluating the respective properties of the repair materials.

The test methods in this document are intended to serve as a reference for nations that have not yet

developed a test method on the six required performance properties of water leakage repair materials.

If other forms of test methods that are simpler, more accurate or more organized are available, such

methods are recommended for use instead. Many of the dependent variables outlined in the reference

test methods of this document are subject to change in accordance with the environmental conditions

(temperature and humidity, chemical solution and concentration, width of movement activity, water

pressure or water flow velocity, etc.) outlined in the standards used in respective countries.

For ISO/TS 16774-1, ISO/TS 16774-5 and ISO/TS 16774-6, for the purpose of objectively comparing the

performance of injected repair materials, artificial cracks of same width, height, and volume were used

to control the usage of repair materials for each testing cycle and enable repetition of the same test

methods under the same conditions.
© ISO 2023 – All rights reserved
---------------------- Page: 5 ----------------------
TECHNICAL SPECIFICATION ISO/DTS 16774-2:2023(E)
Test methods for repair materials for water-leakage cracks
in underground concrete structures —
Part 2:
Test method for chemical resistance
1 Scope

This document specifies a laboratory test method for the qualitative determination of the retention

level of chemical resistance of repair materials in repaired cracks of concrete structures in conditions

where the material is either underwater or in contact with water that can have various chemical

components present.
2 Normative references

The following documents are referred to in the text in such a way that some or all of their content

constitutes requirements of this document. For dated references, only the edition cited applies. For

undated references, the latest edition of the referenced document (including any amendments) applies.

ISO/TR 16475, General practices for the repair of water-leakage cracks in concrete structures

3 Terms and definitions

For the purposes of this document, the terms and definitions given in ISO/TR 16475 and the following

apply.

ISO and IEC maintain terminology databases for use in standardization at the following addresses:

— ISO Online browsing platform: available at https:// www .iso .org/ obp
— IEC Electropedia: available at https:// www .electropedia .org/
3.1
water leakage repair material
grouting materials used to prevent water leakages in concrete cracks

Note 1 to entry: In this document, target ingredients are limited to injection materials outlined in ISO/TR 16475.

4 Principle

A repair material’s resistance to chemical attacks is one of the fundamental properties that water

leakage repair materials should possess. Repair materials can undergo chemical property changes due

to chemical attack. Harmful chemical substances can also corrode the repair material and reduce their

ability to prevent water leakage. This test method evaluates a water leakage repair material’s chemical

resistance performance by determining if the tested material can maintain as closely as possible its

original mass after being exposed to various types of chemical substances as a means to evaluate the

material’s resistance against chemical corrosion. In this method, comparing the mass difference of

water leakage repair materials before and after chemical exposure can be used to determine the repair

material’s chemical resistance level. An example test method is provided in Annex A.

The tested repair material sample prepared in a Petri dish is placed in a container and completely

immersed in chemical solutions for predetermined number of hours o
...