Air quality - Assessment of air quality monitoring equipment - Part 4: Performance criteria and test procedures for portable automated measuring systems for periodic measurements of emissions from stationary sources

This document specifies the general performance criteria and test procedures for the performance test of portable automated measuring systems (P-AMS) used for periodic measurements of stationary source emissions. It applies to the performance test of P-AMS based on measurement techniques specified by the standard reference method (SRM) or an alternative method (AM).
The performance test is based on the general performance criteria and test procedures specified in this document and on the specific requirements specified for the SRM or AM. This includes testing of the applicability and correct implementation of the QA/QC procedures specified for the SRM or AM.
This document supports the requirements of particular EU Directives.

Luftbeschaffenheit - Beurteilung von Einrichtungen zur Überwachung der Luftbeschaffenheit - Teil 4: Mindestanforderungen und Prüfprozeduren für portable automatische Messeinrichtungen für wiederkehrende Messungen von Emissionen aus stationären Quellen

Dieses Dokument legt Mindestanforderungen und Prüfprozeduren für die Eignungsprüfung von portablen automatischen Messeinrichtungen (P-AMS), die für wiederkehrende Messungen von Emissionen aus stationären Quellen eingesetzt werden, fest. Es gilt für die Eignungsprüfung von P-AMS, die auf Messprinzipien beruhen, die durch das Standardreferenzverfahren (SRM) oder ein Alternativverfahren (AM) festgelegt sind.
Die Eignungsprüfung basiert auf den in diesem Dokument festgelegten allgemeinen Mindestanforderungen und Prüfprozeduren und auf den spezifischen Anforderungen, die für das SRM oder AM festgelegt sind. Dies beinhaltet die Prüfung der Anwendbarkeit und richtige Umsetzung der Verfahren zur Qualitätssicherung und Qualitätslenkung (QA/QC), die für das SRM oder AM festgelegt sind.
Dieses Dokument unterstützt die Anforderungen von bestimmten EU-Richtlinien.

Qualité de l'air - Évaluation des équipements de surveillance de la qualité de l'air - Partie 4 : Spécifications de performance et modes opératoires d'essai des systèmes de mesurage automatisés portables pour le mesurage périodique des émissions de source

Le présent document définit les critères de performance généraux et les modes opératoires des essais de performance des systèmes de mesurage automatisés portables (P-AMS) destinés au mesurage périodique des émissions de sources fixes. Il s’applique aux essais de performance des P-AMS basés sur les techniques de mesurage spécifiées par une méthode de référence normalisée (SRM) ou une méthode alternative (AM).
Les essais de performance sont basés sur des critères de performance généraux et des modes opératoires d’essai spécifiés dans le présent document et sur des exigences spécifiques prescrites pour la SRM ou l’AM. Ceci inclut les essais d’applicabilité et de mise en œuvre correcte des modes opératoires d’AQ/CQ spécifiés pour la SRM ou l’AM.
Le présent document vient à l’appui des exigences de Directives UE spécifiques.

Kakovost zraka - Ocenjevanje opreme za monitoring kakovosti zraka - 4. del: Merila za delovanje in postopki preskušanja prenosnih avtomatskih merilnih sistemov (P-AMS) za periodične meritve emisij iz nepremičnih virov

General Information

Status
Not Published
Public Enquiry End Date
02-Oct-2022
Technical Committee
Current Stage
4020 - Public enquire (PE) (Adopted Project)
Start Date
10-Jul-2022
Due Date
27-Nov-2022
Completion Date
28-Oct-2022

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SLOVENSKI STANDARD
oSIST prEN 15267-4:2022
01-september-2022
Kakovost zraka - Ocenjevanje opreme za monitoring kakovosti zraka - 4. del:
Merila za delovanje in postopki preskušanja prenosnih avtomatskih merilnih
sistemov (P-AMS) za periodične meritve emisij iz nepremičnih virov

Air quality - Assessment of air quality monitoring equipment - Part 4: Performance criteria

and test procedures for portable automated measuring systems for periodic
measurements of emissions from stationary sources
Luftbeschaffenheit - Beurteilung von Einrichtungen zur Überwachung der

Luftbeschaffenheit - Teil 4: Mindestanforderungen und Prüfprozeduren für portable

automatische Messeinrichtungen für wiederkehrende Messungen von Emissionen aus
stationären Quellen

Qualité de l'air - Évaluation des équipements de surveillance de la qualité de l'air - Partie

4 : Spécifications de performance et modes opératoires d'essai des systèmes de

mesurage automatisés portables pour le mesurage périodique des émissions de source

Ta slovenski standard je istoveten z: prEN 15267-4
ICS:
03.120.20 Certificiranje proizvodov in Product and company
podjetij. Ugotavljanje certification. Conformity
skladnosti assessment
13.040.99 Drugi standardi v zvezi s Other standards related to air
kakovostjo zraka quality
oSIST prEN 15267-4:2022 en,fr,de

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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oSIST prEN 15267-4:2022
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oSIST prEN 15267-4:2022
DRAFT
EUROPEAN STANDARD
prEN 15267-4
NORME EUROPÉENNE
EUROPÄISCHE NORM
August 2022
ICS 13.040.99 Will supersede EN 15267-4:2017
English Version
Air quality - Assessment of air quality monitoring
equipment - Part 4: Performance criteria and test
procedures for portable automated measuring systems for
periodic measurements of emissions from stationary
sources

Qualité de l'air - Évaluation des équipements de Luftbeschaffenheit - Beurteilung von Einrichtungen zur

surveillance de la qualité de l'air - Partie 4 : Überwachung der Luftbeschaffenheit - Teil 4:

Spécifications de performance et modes opératoires Mindestanforderungen und Prüfprozeduren für

d'essai des systèmes de mesurage automatisés portable automatische Messeinrichtungen für

portables pour le mesurage périodique des émissions wiederkehrende Messungen von Emissionen aus

de source stationären Quellen

This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee

CEN/TC 264.

If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations

which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.

This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other

language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC

Management Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,

Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,

Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and

United Kingdom.

Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are

aware and to provide supporting documentation.

Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without

notice and shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels

© 2022 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 15267-4:2022 E

worldwide for CEN national Members.
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prEN 15267-4:2022 (E)
Contents Page

European foreword ....................................................................................................................................................... 5

Introduction .................................................................................................................................................................... 6

1 Scope .................................................................................................................................................................... 9

2 Normative references .................................................................................................................................... 9

3 Terms and definitions ................................................................................................................................... 9

4 Symbols and abbreviations ...................................................................................................................... 17

5 General requirements ................................................................................................................................ 19

5.1 Application of performance criteria ..................................................................................................... 19

5.2 Ranges to be tested ...................................................................................................................................... 19

5.2.1 Certification range ....................................................................................................................................... 19

5.2.2 Supplementary ranges ............................................................................................................................... 20

5.2.3 Lower limit of ranges .................................................................................................................................. 20

5.2.4 Expression of performance criteria with respect to ranges ......................................................... 20

5.2.5 Ranges of optical in situ P-AMS with variable optical length ....................................................... 21

5.3 Performance testing of P-AMS based on certified AMS previously tested according to

prEN 15267-3 ................................................................................................................................................. 21

5.4 Equivalence with the SRM ......................................................................................................................... 21

5.5 Manufacturing consistency and changes to P-AMS design ............................................................ 21

5.6 Qualifications of testing laboratories ................................................................................................... 21

6 Common performance criteria for the laboratory test .................................................................. 21

6.1 P-AMS for testing .......................................................................................................................................... 21

6.2 CE labelling ..................................................................................................................................................... 21

6.3 Output ranges and zero-point ................................................................................................................. 22

6.4 Operational status signals......................................................................................................................... 22

6.5 Degrees of protection provided by enclosures ................................................................................. 22

6.6 Response time ............................................................................................................................................... 22

6.7 Repeatability standard deviation at zero point ................................................................................ 22

6.8 Repeatability standard deviation at span point ............................................................................... 22

6.9 Lack of fit ......................................................................................................................................................... 22

6.10 Short-term drift at zero point and at span point .............................................................................. 23

6.11 Set-up time after transport and influence of ambient temperature ......................................... 23

6.12 Influence of supply voltage variations ................................................................................................. 23

6.13 Influence of vibration ................................................................................................................................. 23

6.14 Influence of sample gas pressure ........................................................................................................... 23

6.15 Influence of sample gas flow for extractive P-AMS .......................................................................... 23

6.16 Cross-sensitivity ........................................................................................................................................... 23

6.17 Converter efficiency for P-AMS measuring NO ................................................................................ 24

6.18 Converter efficiency for P-AMS measuring Hg ................................................................................... 24

6.19 Response factors for P-AMS measuring TOC ...................................................................................... 24

6.20 Influences on P-AMS with in-stack sampling chamber ................................................................... 24

6.21 Influences related to storage and transportation ............................................................................ 24

7 Common performance criteria for the field test ............................................................................... 24

7.1 Response time ............................................................................................................................................... 24

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7.2 Short-term drift at zero point and at span point ............................................................................... 25

7.3 Reproducibility .............................................................................................................................................. 25

8 Specific performance criteria for measured components ............................................................. 25

8.1 General ............................................................................................................................................................. 25

8.2 P-AMS measuring gaseous measured components .......................................................................... 25

8.2.1 Performance criteria ................................................................................................................................... 25

8.2.2 P-AMS measuring TOC................................................................................................................................. 27

8.2.3 P-AMS measuring Hg ................................................................................................................................... 28

8.3 P-AMS measuring particulate matter .................................................................................................... 28

9 General test requirements ........................................................................................................................ 29

10 Test procedures for the laboratory test ............................................................................................... 30

10.1 P-AMS for testing ........................................................................................................................................... 30

10.2 CE labelling ...................................................................................................................................................... 30

10.3 Output ranges and zero point .................................................................................................................. 31

10.4 Operational status signals ......................................................................................................................... 31

10.5 Degrees of protection provided by enclosures .................................................................................. 31

10.6 Response time ................................................................................................................................................ 31

10.7 Repeatability standard deviation at zero point ................................................................................. 33

10.8 Repeatability standard deviation at span point ................................................................................ 34

10.9 Lack of fit .......................................................................................................................................................... 34

10.10 Short-term drift at zero point and at span point ............................................................................... 36

10.11 Set-up time after transportation and influence of ambient temperature ................................ 36

10.12 Influence of supply voltage variations .................................................................................................. 37

10.13 Influence of vibration .................................................................................................................................. 38

10.14 Influence of sample gas pressure............................................................................................................ 39

10.15 Influence of sample gas flow for extractive P-AMS ........................................................................... 39

10.16 Cross-sensitivity ............................................................................................................................................ 40

10.17 Converter efficiency for P-AMS measuring NO ................................................................................. 41

10.18 Converter efficiency for P-AMS measuring Hg ................................................................................... 42

10.19 Response factors for P-AMS measuring TOC ....................................................................................... 42

10.20 Influences on P-AMS with in-stack sampling chamber ................................................................... 43

10.21 Influences related to storage and transportation ............................................................................. 43

11 Requirements for the field test ................................................................................................................ 43

12 Common test procedures for the field test .......................................................................................... 44

12.1 Response time ................................................................................................................................................ 44

12.2 Short-term drift at zero point and at span point ............................................................................... 44

12.3 Reproducibility .............................................................................................................................................. 45

13 Equivalence with the SRM ......................................................................................................................... 46

14 Measurement uncertainty ......................................................................................................................... 46

15 Test report ...................................................................................................................................................... 46

Annex A (informative) European standard reference methods (SRM) and reference

methods (RM)................................................................................................................................................. 48

Annex B (normative) Minimum requirements for a test bench ................................................................ 49

Annex C (normative) Interferents ....................................................................................................................... 50

Annex D (informative) Example for the determination of the expanded uncertainty ..................... 51

D.1 Determination of uncertainty contributions ...................................................................................... 51

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D.2 Elements required for the uncertainty determinations ................................................................ 51

D.3 Example of an uncertainty calculation for a P-AMS measuring CO ............................................ 53

D.4 Determination of uncertainty contributions by use of sensitivity coefficients ..................... 55

Annex E (normative) Test of linearity ............................................................................................................... 57

E.1 Description of the test procedure .......................................................................................................... 57

E.2 Establishment of the regression line .................................................................................................... 57

E.3 Calculation of the residuals of the average concentrations .......................................................... 58

Annex F (informative) Elements of a performance test report ................................................................ 59

Bibliography ................................................................................................................................................................. 62

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European foreword

This document (prEN 15267-4:2022) has been prepared by Technical Committee CEN/TC 264 “Air

quality”, the secretariat of which is held by DIN.
This document is currently submitted to the CEN Enquiry.
This document will supersede EN 15267-4:2017.

In comparison with the previous edition, the following technical modifications have been made:

a) The title of the revised EN 15267 series has been clarified to avoid the impression that all parts deal

with the certification of automated measuring systems. The title has been generalized so that

specifically Part 1 and Part 2 are also applicable to other air quality monitoring equipment.

b) The title of revised EN 15267-4 has been clarified to make it clear that Part 4 deals with portable

automated measuring systems for periodic measurements of emissions from stationary sources.

c) The performance criteria test and procedures were adapted to the state of the art in measurement

technology.

d) Requirements for portable automated measuring systems measuring mercury have been added.

e) References have been updated.
This document is Part 4 of a series of European Standards:

— EN 15267-1, Air quality — Assessment of air quality monitoring equipment — Part 1: General

principles of certification

— EN 15267-2, Air quality — Assessment of air quality monitoring equipment — Part 2: Initial assessment

of the manufacturer’s quality management system and post certification surveillance for the

manufacturing process

— EN 15267-3, Air quality — Assessment of air quality monitoring equipment — Part 3: Performance

criteria and test procedures for stationary automated measuring systems for continuous monitoring of

emissions from stationary sources

— EN 15267-4, Air quality — Assessment of air quality monitoring equipment — Part 4: Performance

criteria and test procedures for portable automated measuring systems for periodic measurements of

emissions from stationary sources
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Introduction
0.1 General

The assessment of air quality monitoring equipment (AQME) supports the requirements of certain

Directives of the European Union (EU), which require, either directly or indirectly, that this equipment

complies with performance criteria, maximum permissible measurement uncertainties and test

requirements. These Directives include the Directive 2010/75/EU on industrial emissions (IED),

Directive (EU) 2015/2193 on medium combustion plants and the Directive 2008/50/EC on ambient air

quality and cleaner air for Europe.
The assessment of AQME consists of the following sequential stages:
a) performance testing;
b) initial assessment of the manufacturer’s quality management system (QMS);
c) certification;
d) surveillance for the manufacturing process.

This document specifies the performance criteria and test procedures for performance testing of portable

automated measuring systems (P-AMS) used for periodic measurements of stationary source emissions.

Testing applies to complete measuring systems.

NOTE 1 Portable electrical apparatus designed to measure combustion flue gas parameters of heating appliances

are specified in EN 50379–1 to EN 50379–3.

The application of P-AMS for periodic measurements of stationary source emissions is based on

— specification of the standard reference method (SRM) and validation of the SRM;

— specification of the alternative method (AM) if the P-AMS is based on an AM;

— certification of the P-AMS in accordance with EN 15267-1, EN 15267-2 and EN 15267-4 including

demonstration of equivalence with the SRM in the field if the P-AMS is based on an AM;

— on-going quality management by the user of the P-AMS in line with EN ISO/IEC 17025.

NOTE 2 Examples for SRM and AM for different measured components are listed in Annex A.

The overall assessment for the purposes of certification is conformity testing, while the evaluation of

performance against specified performance criteria is performance testing.
0.2 Legal drivers
This document supports at least the requirements of the following EU Directives:
— Directive 2010/75/EU on industrial emissions;

— Directive (EU) 2015/2193 on the limitation of emissions of certain pollutants into the air from

medium combustion plants;

— Directive 2003/87/EC establishing a system for greenhouse gas emission allowance trading.

However, this document can also be applied to the monitoring requirements specified in other

EU Directives.
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0.3 Periodic measurements

Certified P-AMS can be used as SRM or AM for periodic measurements of stationary source emissions.

0.4 Relationship to EN 14181

Certified P-AMS can be used as SRM or AM for the calibration and validation of stationary AMS for QAL2

and AST purposes.
0.5 Processes

Field testing of P-AMS is ordinarily carried out on industrial processes representative of the range of

application of the SRM or AM. The premise is that if the P-AMS performs acceptably on these processes,

then experience has shown that the P-AMS generally performs well on the majority of other processes.

However, there are always exceptions and it is the responsibility of the user to ensure that the P-AMS

performs adequately on a specific process.
The necessary field test of P-AMS is specified in this document.
0.6 Performance characteristics

A combination of laboratory test and field test is detailed within this document. The laboratory test is

designed to assess whether P-AMS can meet, under controlled conditions, the relevant performance

criteria. The field test is designed to assess whether P-AMS can continue to work and meet the relevant

performance criteria in real applications including transportation to the measurement site, set-up of the

P-AMS and measurement.
The main P-AMS performance characteristics are:
— response time;
— repeatability standard deviation;
— lack of fit (linearity);
— short-term drift;
— influence of ambient temperature;
— influence of supply voltage variations;
— influence of vibration;
— influence of sample gas pressure;
— influence of sample gas flow for extractive P-AMS;

— cross-sensitivity to likely interferents contained in the waste gas other than the measured

component;
— converter efficiency for P-AMS measuring NO ;
— converter efficiency of P-AMS measuring Hg;
— response factors for P-AMS measuring TOC;
— reproducibility;
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— trueness and precision of the P-AMS against the SRM under field conditions if the P-AMS is based on

an AM.

Additional performance characteristics specific to the SRM or AM are included in the performance test.

The quality assurance and quality control (QA/QC) procedures to be applied by the user of the P-AMS are

also assessed in the performance test.

This document is an application and elaboration of EN ISO 9169 with additional and alternative

provisions for the performance test of P-AMS. Where this document appears to differ from EN ISO 9169,

it either elaborates upon the requirements of EN ISO 9169 or differs in minor ways owing to the necessity

to conduct the performance test of P-AMS.
0.7 Relationship to prEN 15267-3

This document is based on prEN 15267-3, which specifies the performance test of stationary AMS for the

continuous monitoring of emissions from stationary sources. Many requirements of this document are

identical to those of prEN 15267-3. This document deviates from prEN 15267-3 only where the portable

use and the use as SRM or AM require different or additional requirements. Therefore, this document

allows a combined testing according to prEN 15267-3 and prEN 15267-4 where an AMS is designed for

stationary and portable use. It also allows a reduced performance test of P-AMS, which have been already

certified according to prEN 15267-3 for stationary use.
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1 Scope

This document specifies the general performance criteria and test procedures for the performance test

of portable automated measuring systems (P-AMS) used for periodic measurements of stationary source

emissions. It applies to the performance test of P-AMS based on measurement techniques specified by

the standard reference method (SRM) or an alternative method (AM).

The performance test is based on the general performance criteria and test procedures specified in this

document and on the specific requirements specified for the SRM or AM. This includes testing of the

applicability and correct implementation of the QA/QC procedures specified for the SRM or AM.

This document supports the requirements of particular EU Directives.
2 Normative references

The following documents are referred to in the text in such a way that some or all of their content

constitutes requirements of this document. For dated references, only the edition cited applies. For

undated references, the latest edition of the referenced document (including any amendments) applies.

EN 14793, Stationary source emissions - Demonstration of equivalence of an alternative method with a

reference method

EN 15259, Air quality - Measurement of stationary source emissions - Requirements for measurement

sections and sites and for the measurement objective, plan and report

EN 50160, Voltage characteristics of electricity supplied by public electricity networks

EN 60068-2-6, Environmental testing - Part 2-6: Tests - Test Fc: Vibration (sinusoidal) (IEC 60068-2-6)

EN 60529, Degrees of protection provided by enclosures (IP Code)

EN ISO 14956, Air quality - Evaluation of the suitability of a measurement procedure by comparison with a

required measurement uncertainty (ISO 14956)
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.

ISO and IEC maintain terminological databases for use in standardization at the following addresses:

— ISO Online browsing platform: available at https://www.iso.org/obp
— IEC Electropedia: available at https://www.electropedia.org/
3.1
air quality monitoring equipment
AQME
automated measuring system or data acquisition and handling system
[SOURCE: prEN 15267-1:2021, 3.1]
3.2
automated measuring system
AMS

entirety of all measuring instruments and additional devices for obtaining a result of measurement

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Note 1 to entry: The term “automated measuring system” applies to stationary and portable AMS.

Note 2 to entry: Apart from the actual measuring device (the a
...

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