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ASTM D1607-91(2005)

(Test Method)

Standard Test Method for Nitrogen Dioxide Content of the Atmosphere (Griess-Saltzman Reaction)

Standard Test Method for Nitrogen Dioxide Content of the Atmosphere (Griess-Saltzman Reaction)

SIGNIFICANCE AND USE
Nitrogen dioxide plays an important role in photochemical smog-forming reactions and, in sufficient concentrations, is deleterious to health, agriculture, materials, and visibility.
In combustion processes, significant amounts of nitric oxide (NO) may be produced by combination of atmospheric nitrogen and oxygen; at ambient temperatures NO can be converted to NO2 by oxygen and other atmospheric oxidants. Nitrogen dioxide may also be generated from processes involving nitric acid, nitrates, the use of explosives, and welding.
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1.1 This test method covers the manual determination of nitrogen dioxide (NO2) in the atmosphere in the range from 4 to 10 000 g/m3 (0.002 to 5 ppm(v)) when sampling is conducted in fritted-tip bubblers.
1.2 For concentrations of NO2 in excess of 10 mg/m3 (5 ppm(v)), as occur in industrial atmospheres, gas burner stacks, or automotive exhaust, or for samples relatively high in sulfur dioxide content, other methods should be applied. See for example Test Method D 1608.
1.3 The maximum sampling period is 60 min at a flow rate of 0.4 L/min.
1.4 The values stated in SI units are to be regarded as standard. The values given in brackets are for information only.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See also for other precautions.

General Information

Status
Historical
Publication Date
30-Sep-2005
ICS
13.040.20 - Ambient atmospheres
Technical Committee
D22 - Air Quality
Drafting Committee
D22.03 - Ambient Atmospheres and Source Emissions
Current Stage
Ref Project

Relations

Replaces
ASTM D1607-91(2000)e1 - Standard Test Method for Nitrogen Dioxide Content of the Atmosphere (Griess-Saltzman Reaction)
Effective Date
01-Oct-2005
Replaced By
ASTM D1607-91(2011) - Standard Test Method for Nitrogen Dioxide Content of the Atmosphere (Griess-Saltzman Reaction)
Effective Date
01-Oct-2011

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ASTM D1607-91(2005) - Standard Test Method for Nitrogen Dioxide Content of the Atmosphere (Griess-Saltzman Reaction)ASTM D1607-91(2005) - Standard Test Method for Nitrogen Dioxide Content of the Atmosphere (Griess-Saltzman Reaction)
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ASTM D1607-91(2005) - Standard Test Method for Nitrogen Dioxide Content of the Atmosphere (Griess-Saltzman Reaction)
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D1607–91(Reapproved 2005)
Standard Test Method for
Nitrogen Dioxide Content of the Atmosphere (Griess-
1
Saltzman Reaction)
This standard is issued under the fixed designation D1607; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope D1357 Practice for Planning the Sampling of the Ambient
2 Atmosphere
1.1 This test method covers the manual determination of
D1608 Test Method for Oxides of Nitrogen in Gaseous
nitrogen dioxide (NO ) in the atmosphere in the range from 4
2
3
Combustion Products (Phenol-Disulfonic Acid Proce-
to 10 000 µg/m (0.002 to 5 ppm(v)) when sampling is
dures)
conducted in fritted-tip bubblers.
3
D3195 Practice for Rotameter Calibration
1.2 For concentrations of NO in excess of 10 mg/m (5
2
D3609 Practice for Calibration Techniques Using Perme-
ppm(v)), as occur in industrial atmospheres, gas burner stacks,
ation Tubes
or automotive exhaust, or for samples relatively high in sulfur
D3631 Test Methods for Measuring Surface Atmospheric
dioxide content, other methods should be applied. See for
Pressure
example Test Method D1608.
E1 Specification for ASTM Liquid-in-Glass Thermometers
1.3 The maximum sampling period is 60 min at a flow rate
E128 Test Method for Maximum Pore Diameter and Per-
of 0.4 L/min.
meability of Rigid Porous Filters for Laboratory Use
1.4 The values stated in SI units are to be regarded as
standard.Thevaluesgiveninbracketsareforinformationonly.
3. Terminology
1.5 This standard does not purport to address all of the
3.1 For definitions of terms used in this test method, refer to
safety concerns, if any, associated with its use. It is the
Terminology D1356.
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
4. Summary of Test Method
bility of regulatory limitations prior to use. See also 7.2.2 for
4.1 The NO is absorbed in an azo-dye-forming reagent
2
other precautions.
4
(1). Ared-violet color is produced within 15 min, the intensity
2. Referenced Documents of which is measured spectrophotometrically at 550 nm.
3
2.1 ASTM Standards:
5. Significance and Use
D1071 Test Methods for Volumetric Measurement of Gas-
5.1 Nitrogendioxideplaysanimportantroleinphotochemi-
eous Fuel Samples
cal smog-forming reactions and, in sufficient concentrations, is
D1193 Specification for Reagent Water
deleterious to health, agriculture, materials, and visibility.
D1356 Terminology Relating to Sampling and Analysis of
5.2 In combustion processes, significant amounts of nitric
Atmospheres
oxide (NO) may be produced by combination of atmospheric
nitrogen and oxygen; at ambient temperatures NO can be
converted to NO by oxygen and other atmospheric oxidants.
2
1
This test method is under the jurisdiction of ASTM Committee D22 on Air
Nitrogendioxidemayalsobegeneratedfromprocessesinvolv-
Quality and is the direct responsibility of Subcommittee D22.03 on Ambient
ing nitric acid, nitrates, the use of explosives, and welding.
Atmospheres and Source Emissions.
Current edition approved Oct. 1, 2005. Published January 2006. Originally
6. Interferences
´1
approved in 1958. Last previous edition approved in 2000 as D1607 - 91(2000) .
DOI: 10.1520/D1607-91R05.
6.1 Aten-foldratioofsulfurdioxide(SO )toNO produces
2 2
2
Adapted from “Selected Methods for the Measurement ofAir Pollutants,” PHS
no effect. A thirty-fold ratio slowly bleaches the color to a
Publication No 999-AP-11, May 1965. A similar version has been submitted to the
slight extent. The addition of acetone to the reagent retards the
Intersociety Committee.
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
4
Standards volume information, refer to the standard’s Document Summary page on The boldface numbers in parentheses refer to the list of references appended to
the ASTM website. this method.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D1607–91 (2005)
fadingbyformingatemporaryadditionproductwithSO .This 7.2.3 Rinse the bubbler thoroughly with water and allow to
2
permits reading the color intensity within 4 to 5 h (instead of dry before using.
the 45 min required without the acetone) without appreciable 7.3 Mist Eliminator or Gas Drying Tube, filled with acti-
losses. vated charcoal or soda lime is used to prevent damage to the
6.2 A five-fold rat
...

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1.3 Procedures for random sampling of units within dwellings having multiple units are not included.  
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1.5 The values stated in SI units are to be regarded as the standard.  
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3.5 Values of units in the left column may be converted to values of units in the right column merely by multiplying by the conversion factor provided in the center column.  (A) For specific applications and exceptions, see Terminology D1356.
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5.3 It is anticipated that the main users of this practice will be manufacturers, developers, and distributors of outdoor air quality sensors, air quality agenc...
SCOPE
1.1 This practice establishes standardized tests for the performance evaluation of sensor-based continuous instruments for ambient outdoor air quality measurements. It describes both laboratory and field tests that provide information on candidate sensor repeatability, sensitivity, linearity, cross-interferences, drift, and comparability against reference instruments.  
1.2 This practice does not apply to sensors or instruments that remotely measure atmospheric pollutants using open path, lidar, or imaging technology.  
1.3 The evaluation procedures contained in this practice are for sensors that alone or in combination measure outdoor criteria pollutants in ambient air: particulate matter (PM2.5 and PM10), sulfur dioxide (SO2), ozone (O3), carbon monoxide (CO), or nitrogen dioxide (NO2) at concentrations that are relevant to public health.  
1.4 Testing is to be performed by a competent entity able to demonstrate that it operates in conformity with internationally accepted test laboratory quality standards such as ISO/IEC 17025.  
1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D2914-15(2022)(Test Method)
Standard Test Methods for Sulfur Dioxide Content of the Atmosphere (West-Gaeke Method)

SIGNIFICANCE AND USE
5.1 Sulfur dioxide is a major air pollutant, commonly formed by the combustion of sulfur-bearing fuels. The Environmental Protection Agency (EPA) has set primary and secondary air quality standards (7) that are designed to protect the public health and welfare.  
5.2 The Occupational Safety and Health Administration (OSHA) has promulgated exposure limits for sulfur dioxide in workplace atmospheres (8).  
5.3 These methods have been found satisfactory for measuring sulfur dioxide in ambient and workplace atmospheres over the ranges pertinent in 5.1 and 5.2.  
5.4 Method A has been designed to correspond to the EPA-Designated Reference Method (7) for the determination of sulfur dioxide.
SCOPE
1.1 These test methods cover the bubbler collection and colorimetric determination of sulfur dioxide (SO2) in the ambient or workplace atmosphere.  
1.2 These test methods are applicable for determining SO2 over the range from approximately 25 μg/m3 (0.01 ppm(v)) to 1000 μg/m3 (0.4 ppm(v)), corresponding to a solution concentration of 0.03 μg SO2/mL to 1.3 μg SO2/mL. Beer's law is followed through the working analytical range from 0.02 μg SO2/mL to 1.4 μg SO2/mL.  
1.3 The lower limit of detection is 0.075 μg SO2/mL (1),2 representing an air concentration of 25 μg SO2/m3 (0.01 ppm(v)) in a 30-min sample, or 13 μg SO2/m3 (0.005 ppm(v)) in a 24-h sample.  
1.4 These test methods incorporate sampling for periods between 30 min and 24 h.  
1.5 These test methods describe the determination of the collected (impinged) samples. A Method A and a Method B are described.  
1.6 Method A is preferred over Method B, as it gives the higher sensitivity, but it has a higher blank. Manual Method B is pH-dependent, but is more suitable with spectrometers having a spectral band width greater than 20 nm.
Note 1: These test methods are applicable at concentrations below 25 μg/m3 by sampling larger volumes of air if the absorption efficiency of the particular system is first determined, as described in Annex A4.
Note 2: Concentrations higher than 1000 μg/m3 can be determined by using smaller gas volumes, larger collection volumes, or by suitable dilution of the collected sample with absorbing solution prior to analysis.  
1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.8 Warning—Mercury has been designated by many regulatory agencies as a hazardous material that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Safety Data Sheet (SDS) for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.  
1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see 8.3.1, Section 9, and A3.1.3.  
1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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