ASTM D1513-05(2017)

Standard Test Method for Carbon Black, Pelleted—Pour Density

SIGNIFICANCE AND USE
4.1 Pour density is a function of the degree of compaction during pelletization. It is strongly influenced by and inversely proportional to structure (OAN). Pour density of carbon black is useful for estimating the weight-to-volume relationship for certain applications, such as automatic batch loading systems, and for estimating weights of bulk shipments.
SCOPE
1.1 This test method covers the determination of the pour density of pelleted carbon blacks.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

• Status: Historical
• Publication Date: 30-Nov-2017
• ICS: 83.040.20 - Rubber compounding ingredients
• Technical Committee: D24 - Carbon Black
• Drafting Committee: D24.51 - Carbon Black Pellet Properties

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D1513 − 05 (Reapproved 2017)
Standard Test Method for
1
Carbon Black, Pelleted—Pour Density
This standard is issued under the fixed designation D1513; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 4. Significance and Use
1.1 This test method covers the determination of the pour 4.1 Pour density is a function of the degree of compaction
density of pelleted carbon blacks. during pelletization. It is strongly influenced by and inversely
proportional to structure (OAN). Pour density of carbon black
1.2 The values stated in SI units are to be regarded as the
is useful for estimating the weight-to-volume relationship for
standard. The values given in parentheses are for information
certain applications, such as automatic batch loading systems,
only.
and for estimating weights of bulk shipments.
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
5. Apparatus
responsibility of the user of this standard to establish appro-
3
5.1 Cylindrical Container, 1000 or 624-cm capacity, hav-
priate safety, health, and environmental practices and deter-
ing a uniform height and no pouring lip or deformation of the
mine the applicability of regulatory limitations prior to use.
wall. A stainless steel beaker 100 6 5 mm (4 6 0.2 in.) in
1.4 This international standard was developed in accor-
diameter is acceptable.
dance with internationally recognized principles on standard-
NOTE 1—A satisfactory container can be made by pouring 1000 or 624
ization established in the Decision on Principles for the
3 3
cm of water at 20°C into a 1000 or 1200-cm stainless steel beaker 100
Development of International Standards, Guides and Recom-
6 5 mm (4 6 0.2 in.) in diameter, marking the water level and then cutting
mendations issued by the World Trade Organization Technical
at the mark after chucking firmly in a lathe.
Barriers to Trade (TBT) Committee.
5.2 Straightedge or Spatula, at least 150 mm (6 in.) in
length.
2. Referenced Documents
2 5.3 Balance, torsion or trip, with a sensitivity of 0.1 g.
2.1 ASTM Standards:
D1799 Practice for Carbon Black—Sampling Packaged
6. Sampling
Shipments
6.1 Samples shall be taken in accordance with Practice
D1900 Practice for Carbon Black—Sampling Bulk Ship-
D1799 or Practice D1900.
ments
D4483 Practice for Evaluating Precision for Test Method
7. Procedure
Standards in the Rubber and Carbon Black Manufacturing
7.1 Pour the carbon black into the center of the tared
Industries
container from a height not more than 50 mm (2 in.) above the
rim. A large enough excess should be used to form a cone
3. Summary of Test Method
above the rim of the cylindrical container. Level the surface
3.1 Pour density is determined by measuring the mass of
with a single sweep of the straightedge or spatula held
carbon black in a known volume.
perpendicular to and in firm contact with the lip of the
container. Record the mass of the carbon black to the nearest
gram.
1
This test method is under the jurisdiction of ASTM Committee D24 on Carbon
Black and is the direct responsibility of Subcommittee D24.51 on Carbon Black
8. Calculation
Pellet Properties.
3
8.1 Calculate the pour density to the nearest kg/m as
Current edition approved Dec. 1, 2017. Published December 2017. Originally
approved in 1957. Last previous edition approved in 2012 as D1513 – 05 (2012).
follows:
3
DOI: 10.1520/D1513-05R17.
8.1.1 Using a 1000-cm container:
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM
D 5 W (1)
1000
Standards volume information, refer to the standard’s Document Summary page on
3
the ASTM website. 8.1.2 Using a 624-cm container:
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D1513 − 05 (2017)
TABLE 1 Test Method Precision—Type 1: Pour Density
A A
Within Laboratory Between Laboratory
Mean Level
Material
3 3
kg/m (lb ⁄ft )
S r (r) S R (R)
r R
C 380 (23.8) 2.8 (0.18) 7.9 (0.50) 2.1 4.5 (0.28) 12.9 (0.80) 3.4
B 434 (27.1) 2.2 (0.14) 6.2 (0.39) 1.4 6.3 (0.39) 17.7 (1.11) 4.1
A 540 (33.7) 3.3 (0.20) 9.2 (0.57) 1.7 6.5 (0.41) 18.5 (1.16) 3.4
Pooled or 452 (28.2) 2.8 (0.17) 7.9 (0.50) 1.7 5.9 (0.39) 16.6 (1.03) 3.7
Average values
A
Symbols are defined as follows:
S = within laboratory standard deviation
r
3 3
r = repeatability in measurement un
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D1513 − 05 (Reapproved 2012) D1513 − 05 (Reapproved 2017)
Standard Test Method for
1
Carbon Black, Pelleted—Pour Density
This standard is issued under the fixed designation D1513; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope
1.1 This test method covers the determination of the pour density of pelleted carbon blacks.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D1799 Practice for Carbon Black—Sampling Packaged Shipments
D1900 Practice for Carbon Black—Sampling Bulk Shipments
D4483 Practice for Evaluating Precision for Test Method Standards in the Rubber and Carbon Black Manufacturing Industries
3. Summary of Test Method
3.1 Pour density is determined by measuring the mass of carbon black in a known volume.
4. Significance and Use
4.1 Pour density is a function of the degree of compaction during pelletization. It is strongly influenced by and inversely
proportional to structure (OAN). Pour density of carbon black is useful for estimating the weight-to-volume relationship for certain
applications, such as automatic batch loading systems, and for estimating weights of bulk shipments.
5. Apparatus
3
5.1 Cylindrical Container, 1000 or 624-cm capacity, having a uniform height and no pouring lip or deformation of the wall.
A stainless steel beaker 100 6 5 mm (4 6 0.2 in.) in diameter is acceptable.
3 3
NOTE 1—A satisfactory container can be made by pouring 1000 or 624 cm of water at 20°C into a 1000 or 1200-cm stainless steel beaker 100 6
5 mm (4 6 0.2 in.) in diameter, marking the water level and then cutting at the mark after chucking firmly in a lathe.
5.2 Straightedge or Spatula, at least 150 mm (6 in.) in length.
5.3 Balance, torsion or trip, with a sensitivity of 0.1 g.
6. Sampling
6.1 Samples shall be taken in accordance with Practice D1799 or Practice D1900.
1
This test method is under the jurisdiction of ASTM Committee D24 on Carbon Black and is the direct responsibility of Subcommittee D24.51 on Carbon Black Pellet
Properties.
Current edition approved June 1, 2012Dec. 1, 2017. Published November 2012December 2017. Originally approved in 1957. Last previous edition approved in 20052012
ε2
as D1513 – 05 (2012). . DOI: 10.1520/D1513-05R12.10.1520/D1513-05R17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D1513 − 05 (2017)
7. Procedure
7.1 Pour the carbon black into the center of the tared container from a height not more than 50 mm (2 in.) above the rim. A
large enough excess should be used to form a cone above the rim of the cylindrical container. Level the surface with a single sweep
of the straightedge or spatula held perpendicular to and in firm contact with the lip of the container. Record the mass of the carbon
black to the nearest gram.
8. Calculation
3
8.1 Calculate the pour density to the nearest kg/m as follows:
3
8.1.1 Using a 1000-cm container:
D 5 W (1)
1000
3
8.1.2 Using a 624-cm container:
TABLE 1 Test Method Precision—Type 1: Pour Density
A A
Within Laboratory Between Laboratory
Mean Level
Material
3 3
kg/m (lb ⁄ft )
S r (r) S R (R)
r R
C 380 (23.8) 2.8 (0.18) 7.9 (0.50) 2.1 4.5 (0.2
...