ASTM F2489-06(2013)
(Guide)Standard Guide for Instrument and Precision Bearing Lubricants—Part 2 Greases
Standard Guide for Instrument and Precision Bearing Lubricants—Part 2 Greases
SIGNIFICANCE AND USE
4.1 The purpose of this guide is to report on the testing of, to discuss and compare the properties of, and to provide guidelines for the choice of lubricating greases for precision rolling element bearings (PREB). The PREB are, for the purposes of this guide, meant to include bearings of Annular Bearing Engineer's Committee (ABEC) 5 quality and above. This guide limits its scope to lubricating greases used in PREB.
4.2 The number of lubricating greases used in PREB increased dramatically from the early 1940s to the mid 1990s. In the beginning of this period, petroleum products were the only widely available base stocks. Later, synthetic base oils became available. They included synthetic hydrocarbons, esters, silicones, multiply alkylated cyclopentanes (MAC) and fluorinated materials, including perfluorinated ethers and the fluorosilicones. This broad spectrum of lubricant choices has led to the use of a large number of different lubricants in PREB applications. The U.S. Department of Defense, as a user of many PREB, has seen a significant increase in the logistics effort required to support the procurement and distribution of these items. In addition, as time has passed, some of the greases used in certain PREB are no longer available or require improved performances due to advanced bearing technology/requirements. This implies that replacement lubricating greases must be found, especially in this era of extending the lifetime of DoD assets, with the consequent and unprojected demand for sources of replacement parts.
4.3 One of the primary goals of this study was to take a broad spectrum of the lubricating greases used in PREB and do a comprehensive series of tests on them in order that their properties could be compared and, if necessary, potential replacement greases be identified. This study is also meant to be a design guide for choosing lubricating greases for future PREB applications. This guide represents a collective effort of many members of this co...
SCOPE
1.1 This guide is a tool to aid in the choice of lubricating grease for precision rolling element bearing applications. The recommendations in this guide are not intended for general purpose bearing applications There are two areas where this guide should have the greatest impact: (1) when lubricating grease is being chosen for a new bearing application and (2) when grease for a bearing has to be replaced because the original grease specified for the bearing can no longer be obtained. The Report (see Section 5) contains a series of tests on a wide variety of greases commonly used in bearing applications to allow comparisons of those properties of the grease that the committee thought to be most important when making a choice of lubricating grease. Each test was performed by the same laboratory. This guide contains a listing of the properties of greases by base oil type, that is, ester, perfluoropolyether (PFPE), polyalphaolefin (PAO), and so forth. This organization is necessary since the operational requirements in a particular bearing application may limit the choice of grease to a particular base oil type and thickener due to its temperature stability, viscosity index or temperature-vapor pressure characteristics, etc. The guide provides data to assist the user in selecting replacement greases for those greases tested that are no longer available. The guide also includes a glossary of terms used in describing/discussing the lubrication of precision and instrument bearings.
1.2 The lubricating greases presented in this guide are commonly used in precision rolling element bearings (PREB). These greases were selected for the testing based on the grease survey obtained from DoD, OEM and grease manufactures and evaluated according to the test protocol that was designed by Subcommittee F34 on Tribology. This test protocol covers the essential requirements identified for precision bearing greases. The performance requirem...
General Information
Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
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Designation: F2489 − 06 (Reapproved 2013)
Standard Guide for
Instrument and Precision Bearing Lubricants—Part 2
Greases
This standard is issued under the fixed designation F2489; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope life, and no contamination of surrounding components by the
bearing’s lubricant system. To increase the reliability of test
1.1 This guide is a tool to aid in the choice of lubricating
data, all tests were performed by a DoD laboratory and three
grease for precision rolling element bearing applications. The
independent testing laboratories. There were no grease manu-
recommendations in this guide are not intended for general
facturer’s data imported except for base oil viscosity. Most of
purpose bearing applications There are two areas where this
tests were performed by U.S. Army Tank–Automotive
guide should have the greatest impact: (1) when lubricating
Research, Development and Engineering Center (TARDEC)
grease is being chosen for a new bearing application and (2)
and three independent laboratories, and the results were moni-
when grease for a bearing has to be replaced because the
tored by the Naval Research Laboratory (NRL). This continu-
original grease specified for the bearing can no longer be
ity of testing should form a solid basis for comparing the
obtained. The Report (see Section 5) contains a series of tests
properties of the multitude of lubricating greases tested by
on a wide variety of greases commonly used in bearing
avoiding some of the variability introduced when greases are
applications to allow comparisons of those properties of the
tested by different laboratories using different or even the
grease that the committee thought to be most important when
“same” procedures. Additional test data will be considered for
makingachoiceoflubricatinggrease.Eachtestwasperformed
inclusion, provided the defined protocol is followed and the
by the same laboratory. This guide contains a listing of the
tests are performed by independent laboratories.
properties of greases by base oil type, that is, ester, perfluo-
ropolyether (PFPE), polyalphaolefin (PAO), and so forth. This 1.3 This study was a part of DoD Aging Aircraft Replace-
organization is necessary since the operational requirements in ment Program and supported by Defense Logistic Agent
a particular bearing application may limit the choice of grease (DLA) and Defense Supply Center Richmond (DSCR).
toaparticularbaseoiltypeandthickenerduetoitstemperature
1.4 The values stated in inch-pound units are to be regarded
stability, viscosity index or temperature-vapor pressure
as standard. No other units of measurement are included in this
characteristics,etc.Theguideprovidesdatatoassisttheuserin
standard.
selecting replacement greases for those greases tested that are
1.5 This standard does not purport to address all of the
nolongeravailable.Theguidealsoincludesaglossaryofterms
safety concerns, if any, associated with its use. It is the
used in describing/discussing the lubrication of precision and
responsibility of the user of this standard to establish appro-
instrument bearings.
priate safety and health practices and determine the applica-
1.2 The lubricating greases presented in this guide are
bility of regulatory limitations prior to use.
commonly used in precision rolling element bearings (PREB).
These greases were selected for the testing based on the grease
2. Referenced Documents
surveyobtainedfromDoD,OEMandgreasemanufacturesand
2.1 ASTM Standards:
evaluated according to the test protocol that was designed by
D217 Test Methods for Cone Penetration of Lubricating
Subcommittee F34 on Tribology. This test protocol covers the
Grease
essential requirements identified for precision bearing greases.
D972 Test Method for Evaporation Loss of Lubricating
The performance requirements of these greases are very
Greases and Oils
unique. They are dictated by the performance expectations of
precision bearings including high speed, low noise, extended
Rhee,In-Sik,“PrecisionBearingGreaseSelectionGuide,” U.S.Army TARDEC
Technical Report No. 15688, Defense Technical Information Center, 8725 John. J.
This guide is under the jurisdiction of ASTM Committee F34 on Rolling Kingman Rd., Suite 0944, Ft. Belvoir, VA 22060–6218.
Element Bearings For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Sept. 15, 2013. Published January 2014. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 2006. Last previous edition approved in 2006 as F2489–06. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/F2489-06R13. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
F2489 − 06 (2013)
D1264 Test Method for Determining the Water Washout Wet Shell Roll Test Method
Characteristics of Lubricating Greases
2.4 SAE Standard:
D1742 Test Method for Oil Separation from Lubricating
SAE-AMS-G-81937 Grease, Instrument, Ultra-Clean, Met-
Grease During Storage ric
D1743 Test Method for Determining Corrosion Preventive
3. Terminology
Properties of Lubricating Greases
D1831 Test Method for Roll Stability of Lubricating Grease
3.1 For definition of standard terms used in this guide, see
D2265 Test Method for Dropping Point of Lubricating
Terminology D4175 and F2488 or Compilation of ASTM
Grease Over Wide Temperature Range
Standard Definitions.
D2266 Test Method for Wear Preventive Characteristics of
3.2 Definitions of Terms Specific to This Standard:
Lubricating Grease (Four-Ball Method)
3.2.1 esters, n—esters are formed from the reaction of acids
D2596 Test Method for Measurement of Extreme-Pressure
and alcohols. Esters form a class of synthetic lubricants. Esters
Properties of Lubricating Grease (Four-Ball Method)
of higher alcohols with divalent fatty acids form diester
D3527 Test Method for Life Performance of Automotive
lubricants while esters of polyhydric alcohols are called the
Wheel Bearing Grease
polyolesterlubricants.Theselatterestershavehigherviscosity
D4048 Test Method for Detection of Copper Corrosion from
and are more heat-resistant than diesters.
Lubricating Grease
3.2.2 mineral oil, n—oils based on petroleum stocks. These
D4175 Terminology Relating to Petroleum, Petroleum
oils come in two types, naphthenic and paraffinic. The naph-
Products, and Lubricants
thenic oils contain unsaturated hydrocarbons, usually in the
D4289 Test Method for Elastomer Compatibility of Lubri-
form of aromatic species. The paraffinic oils are primarily
cating Greases and Fluids
saturated hydrocarbons with only low levels of unsaturation.
D4425 Test Method for Oil Separation from Lubricating
Grease by Centrifuging (Koppers Method) 3.2.3 perfluoropolyethers (PFPE or PFAE), n—fully fluo-
D4693 TestMethodforLow-TemperatureTorqueofGrease-
rinated long-chain aliphatic ethers. The perfluoropolyethers
Lubricated Wheel Bearings show some extraordinary properties like chemical inertness,
D5483 Test Method for Oxidation Induction Time of Lubri-
nonflammability, high thermal and oxidative resistance, very
catingGreasesbyPressureDifferentialScanningCalorim- good viscosity-temperature characteristics, and compatibility
etry
with a wide range of materials, including metals and plastics.
E1131 Test Method for CompositionalAnalysis by Thermo- The perfluoropolyethers, however, are not always suitable for
gravimetry
metal alloys at elevated temperatures (contact temperatures
F2161 Guide for Instrument and Precision Bearing higher than about 550°F). The perfluoropolyethers are not
Lubricants—Part 1 Oils
miscible with other types of synthetic fluids and mineral oils
F2488 Terminology for Rolling Element Bearings and cannot dissolve common lubricant additives.
3.2.4 silicone oils, n—synthetic fluids composed of organic
2.2 Government Documents:
Federal Standard Test Method 791C, 3005.4 Dirt Content of esters of long chain complex silicic acids. Silicone oils have
better physical properties than mineral oils. However, silicone
Grease
MIL-G-25537 Aircraft Helicopter Bearing Grease oils have poorer lubrication properties, lower load-carrying
MIL-PRF-23827 Aircraft and instrument Grease capacity, and a strong tendency to spread on surfaces (see
MIL-PRF-81322 Aircraft Wide Temperature Range Grease surface tension).
MIL-PRF-83261 Aircraft Extreme Pressure
3.2.5 synthetic fluids, n—lubricating fluids produced by
MIL-PRF-10924 Grease, Automotive and Artillery
chemical synthesis. The synthetic route to formulate these
MIL-G-27617 Grease, Aircraft and Instrument, Fuel and
lubricants allows the manufacturer to introduce those chemical
Oxidizer Resistant
structures into the lubricant molecule that will impart specific
MIL-G-21164 Molybdenum Disulfide Grease
properties into the resultant fluid such as very low pour point,
MIL-G-25760 Grease, Aircraft, Ball and Roller Bearing,
good viscosity-temperature relationship, low evaporation loss,
Wide Temperature Range
long lubricating lifetime, and so forth.
MIL-L-15719 High Temperature Electrical Bearing Grease
3.2.6 lubricating grease, n—a semi-fluid to solid product of
DoD-G-24508 Multipurpose Grease
a dispersion of a thickener in a liquid lubricant.
2.3 Industrial Standards:
4. Significance and Use
SKF Be-Quite Noise Test Method
TA Rheometry Procedure for Steady Shear Flow Curve
4.1 The purpose of this guide is to report on the testing of,
to discuss and compare the properties of, and to provide
guidelines for the choice of lubricating greases for precision
Available from Standardization Documents Order Desk, DODSSP, Bldg. 4,
Section D, 700 Robbins Ave., Philadelphia, PA 19111-5098
5 7
Available from SKF North American Technical Center, 46815 Port St., Available from Southwest Petro-Chem Division, Witco Corp., P.O. Box 1974,
Plymouth, MI 48170. Olathe, KS 66061.
6 8
Available from TA Instruments Company, 109 Lukens Drive, New Castle, DE Available from Society of Automotive Engineers (SAE), 400 Commonwealth
19720-2765. Dr., Warrendale, PA 15096-0001.
F2489 − 06 (2013)
rolling element bearings (PREB). The PREB are, for the bearing greases tested. Each grease tested was assigned a code
purposes of this guide, meant to include bearings of Annular tomasktheirsourcetomitigateanypotentialbiasinthetesting
Bearing Engineer’s Committee (ABEC) 5 quality and above. results. The tradename of each grease is listed in Research
ThisguidelimitsitsscopetolubricatinggreasesusedinPREB. Report RR:F34-1000. For the evaluation, each grease was
testedfordroppingpoint,consistency,waterandworkstability,
4.2 The number of lubricating greases used in PREB in-
oxidation stability, oil separation, evaporation loss, wear, EP
creased dramatically from the early 1940s to the mid 1990s. In
properties, corrosion prevention, low temperature
the beginning of this period, petroleum products were the only
characteristics, cleanliness, apparent viscosity, grease noise,
widely available base stocks. Later, synthetic base oils became
and grease life. Compatibility testing with elastomers incorpo-
available. They included synthetic hydrocarbons, esters,
rated into PREB and their environments were not done due to
silicones, multiply alkylated cyclopentanes (MAC) and fluori-
the large number of combinations that would require testing to
nated materials, including perfluorinated ethers and the fluo-
span the potential mixes of greases and elastomer components
rosilicones.This broad spectrum of lubricant choices has led to
that might occur in bearing applications. It is recommended
the use of a large number of different lubricants in PREB
that the user verify grease/elastomer compatibility when
applications. The U.S. Department of Defense, as a user of
needed.
many PREB, has seen a significant increase in the logistics
5.2 In these tables, some of the data may not agree with
effort required to support the procurement and distribution of
these items. In addition, as time has passed, some of the those of manufacturers due to the variation of the test methods
greasesusedincertainPREBarenolongeravailableorrequire and their test apparatuses (that is, noise test). All tests were
improved performances due to advanced bearing technology/ performed by a government laboratory and three independent
requirements.Thisimpliesthatreplacementlubricatinggreases laboratories. No grease manufacturers performed any of these
must be found, especially in this era of extending the lifetime tests except for the base oil viscosities of greases. To increase
of DoD assets, with the consequent and unprojected demand the availability of precision bearing greases, these tables will
for sources of replacement parts. be revised periodically to include new greases as long as the
manufacturer submits test results on their product following
4.3 One of the primary goals of this study was to take a
precisely the protocol defined in the document.
broadspectrumofthelubricatinggreasesusedinPREBanddo
a comprehensive series of tests on them in order that their
6. Application Considerations
properties could be compared and, if necessary, potential
replacement greases be identified. This study is also meant to 6.1 This guide applies only to precision bearing greases.
be a design guide for choosing lubricating greases for future The other types of greases such as industrial greases or
PREB applications. This guide represents a collective effort of automotive general purpose greases are not covered by this
manymembersofthiscommunitywhospanthespectrumfrom guide.
bearing manufacturers, original equipment manufactures 6.1.1 Precision bearing greases contain base oil to which a
(OEMs), grease manufacturers and suppliers, procurement thickener has been added to prevent oil migration from the
specialists, and quality assurance representatives (QARs) from lubrication site and various additives to improve its operating
DoD and end users both inside and outside DoD. performance.Currently,manytechnicalarticlesoftendesignate
types of lubricating greases based on their thickeners.
4.4 Itisstronglyrecommendthat,priortoreplacingagrease
However, the operative properties of precision bearing greases
in a PREB, all of the existing grease should be removed from
depend on the combination of base oil, thickener, and additive
the bearing. Reactions may occur between incompatible
formulation. This guide distinguishes lubricating greases by
greas
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