ASTM D421-85(2002)
(Practice)Standard Practice for Dry Preparation of Soil Samples for Particle-Size Analysis and Determination of Soil Constants
Standard Practice for Dry Preparation of Soil Samples for Particle-Size Analysis and Determination of Soil Constants
SCOPE
1.1 This practice covers the dry preparation of soil samples as received from the field for particle-size analysis and the determination of the soil constants.
1.2 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D421–85(Reapproved2002)
Standard Practice for
Dry Preparation of Soil Samples for Particle-Size Analysis
and Determination of Soil Constants
This standard is issued under the fixed designation D 421; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope
No. 4 (4.75-mm)
No. 10 (2.00-mm)
1.1 This practice covers the dry preparation of soil samples
No. 40 (425-µm)
as received from the field for particle-size analysis and the
4.4 Sampler—A riffle sampler or sample splitter, for quar-
determination of the soil constants.
tering the samples.
1.2 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
5. Sampling
responsibility of the user of this standard to establish appro-
5.1 Expose the soil sample as received from the field to the
priate safety and health practices and determine the applica-
air at room temperature until dried thoroughly. Break up the
bility of regulatory limitations prior to use.
aggregations thoroughly in the mortar with a rubber-covered
2. Referenced Documents pestle. Select a representative sample of the amount required to
perform the desired tests by the method of quartering or by the
2.1 ASTM Standards:
use of a sampler. The amounts of material required to perform
D 2217 Practice for Wet Preparation of Soil Samples for
the individual tests are as follows:
Particle-Size Analysis and Determination of Soil Con-
5.1.1 Particle-Size Analysis—For the particle-size analysis,
stants
material passing a No. 10 (2.00-mm) sieve is required in
E 11 Specification for Wire-Cloth Sieves for Testing Pur-
3 amounts equal to 115 g of sandy soils and 65 g of either silt or
poses
clay soils.
3. Significance and Use 5.1.2 Tests for Soil Constants—For the tests for soil con-
stants, material passing the No. 40 (425-µm) sieve is required
3.1 This practice can be used to prepare samples for
in total amount of 220 g, allocated as follows:
particle-sizeandplasticitytestswhereitisdesiredtodetermine
Test Grams
test values on air-dried samples, or where it is known that air
dryingdoesnothaveaneffectontestresultsrelativetosamples
Liquid limit 100
prepared in accordance with Practice D 2217.
Plastic limit 15
Centrifuge moisture equivalent 10
Volumetric shrinkage 30
4. Apparatus
Check tests 65
4.1 Balance, sensitive to 0.1 g.
6. Preparation of Test Sample
4.2 Mortar and Rubber-Covered Pestle, suitable for break-
ing up the aggregations of soil particles.
6.1 Select that portion of the air-dried sample selected for
4.3 Sieves—A series of sieves, of square mesh woven wire
purposeoftestsandrecordthemassasthemassofthetotaltest
cloth, conforming to Specification E 11. The sieves required
sample uncorrected for hygroscopic moisture. Separate the test
are as follows:
sample by siev
...
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Sections
Test Method A, using soil material passing a 4.75-mm [No. 4] sieve.
This method shall be used when 100 % of the soil sample passes the 4.75-mm [No. 4] sieve.
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Test Method B, using soil material passing a 19.0 mm [0.75-in.] sieve.
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Note 2: For more information on the effect of treating soils containing water soluble sulfates, refer to the following publication: Little, D.N., Stabilization of Pavement Subgrades and Base Course with Lime, Kendal/Hunt Publishing Co., Dubuque, IA, 1995.
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1.1 These methods determine the water soluble sulfate content of cohesive soils used in construction by using the colorimetric technique. Two methods are presented in this standard. Method A is for use in the field and Method B is for use in the laboratory. The colorimetric technique involves measuring the scattering of a light beam through a solution that contains suspended particulate matter. Measurements of sulfate concentrations in construction soils can be used to guide professionals in the selection of appropriate stabilization methods and to assist in assessment of potential deterioration in concrete structures.
Note 1: These test methods are partially based on the research conducted by Texas A & M University.
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1.3 Ion chromatography is also an acceptable alternative method that can be used to evaluate results, however, it is outside the scope of this standard.
1.4 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this test method.
1.5.1 The procedures used to specify how data are collected/recorded and calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of these test methods to consider significant digits used in analysis methods for engineering data.
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Note 2: The determination of the consolidated, undrained strength of cohesive soils with pore pressure measurement is covered by Test Method D4767.
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1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.
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1.3.1 For purposes of comparing a measured or calculated value(s) with specified limits, the measured or calculated value(s) shall be rounded to the nearest decimal of significant digits in the specified limit.
1.3.2 The procedures used to specify how data are collected/recorded or calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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SIGNIFICANCE AND USE
5.1 Many geotechnical tests require the utilization of intact, representative samples of soil. The quality of these samples depends on many factors. Many of the samples obtained by intact sampling methods have inherent anomalies. Sampling procedures cause disturbances of varying types and intensities. These anomalies and disturbances, however, are not always readily detectable by visual inspection of the intact samples before or after testing. Often test results would be enhanced if the presence and the extent of these anomalies and disturbances are known before testing or before destruction of the sample by testing. Such determinations assist the user in detecting flaws in sampling methods, the presence of natural or induced shear planes, and the presence of natural intrusions, such as gravels or shells at critical regions in the samples, the presence of sand and silt seams, and the intensity of disturbances caused by sampling.
5.2 X-ray radiography provides the user with a picture of the internal massive structure of the soil sample, regardless of whether the soil is X-rayed within or without the sampling tube. X-ray radiography assists the user in identifying the following:
5.2.1 Appropriateness of sampling methods used.
5.2.2 Effects of sampling in terms of the disturbances caused by the turning of the edges of various thin layers in varved soils, large disturbances caused in soft soils, shear planes induced by sampling, or extrusion, or both, effects of overdriving of samplers, the presence of cuttings in sampling tubes, or the effects of using bent, corroded, or nonstandard tubes for sampling.
5.2.3 Naturally occurring fissures, shear planes, etc.
5.2.4 The presence of intrusions within the sample, such as calcareous nodules, gravel, or shells.
5.2.5 Sand and silt seams, organic matter, large voids, and channels developed by natural or artificial leaching of soil components.
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SCOPE
1.1 This practice covers the determination of the quality of soil samples in thin wall tubes or of extruded soil cores by X-ray radiography.
1.2 This practice enables the user to determine the effects of sampling and natural variations within samples as identified by the extent of the relative penetration of X-rays through soil samples.
1.3 This practice can be used to X-ray soil cores (or observe their features on a fluoroscope) in thin wall tubes or liners ranging from approximately 50 to 150 mm [2 to 6 in.] in diameter. X-rays of samples in the larger diameter tubes provide a radiograph of major features of soils and disturbances, such as large scale bending of edges of varved clays, shear planes, the presence of large concretions, silt and sand seams thicker than 6 mm [1/4 in.], large lumps of organic matter, and voids or other types of intrusions. X-rays of the smaller diameter cores provide higher resolution of soil features and disturbances, such as small concretions (3 mm [1/8 in.] diameter or larger), solution channels, slight bending of edges of varved clays, thin silt or sand seams, narrow solution channels, plant root structures, and organic matter. The X-raying of samples in thin wall tubes or liners requires minimal preparation.
1.4 Greater detail and resolution of various features of the soil can be obtained by X-raying extruded soil cores, as compared to samples in metal tubes. The method used for X-raying soil cores is the same as that for tubes and liners, except that extruded cores have to be handled with extreme care and have to be placed in sample troughs (similar to Fig. 2) before X-raying. This practice should be used only when natural water content or other intact soil characteristics are irrelevant to the end use of the sample.
1.4.1 Often it is necessary to obtain greater resolution of features to determine the propriety of sampling methods, the representative nature of soil samples,...
- Standard17 pagesEnglish languagesale 15% off
- Standard17 pagesEnglish languagesale 15% off
SIGNIFICANCE AND USE
5.1 This test method is used to determine the percentage of sand by volume in construction slurry. The significance of this test method mainly relates to construction slurries used for concrete wall and drilled piers construction. The range of measurement is too limited for use in applications where the sand content is intended to be greater than 20 %, such as in the cases of cement bentonite or soil bentonite walls.
5.2 A high sand content in the construction slurry is abrasive for construction plant such as pumps, and is furthermore adverse to the formation of a filter cake in applications where bentonite fluid is used to stabilize an excavation.
Note 1: The quality of the result produced by this standard depends on the competence of the personnel performing it and the suitability of the equipment and facilities being used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 This test method covers the determination of the sand content of bentonitic slurries used in slurry construction techniques. This test method has been modified from API Recommended Practice 13B.
1.2 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.
1.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. Except, the sieve designation is identified using the “alternative” system in accordance with Practice E11 instead of the “standard system,” such that the sieve used is referred to as a No. 200 sieve, instead of a 75 µm sieve.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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