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ASTM D5907-03

(Test Method)

Standard Test Method for Filterable and Nonfilterable Matter in Water

Standard Test Method for Filterable and Nonfilterable Matter in Water

SIGNIFICANCE AND USE
Solids, both as filterable and nonfilterable matter, are important in the treating of raw water and wastewater, and in monitoring of streams.
Waste solids impose a suspended and settleable residue in receiving waters. Suspended and soluble materials provide a matrix for some biological slime and, in sufficient quantity, impair respiration of organisms. These solids may create nuisance slime beds and odors while imposing a long-term biological oxidation load over limited receiving water areas.
Knowledge of suspended and soluble materials is important in treating raw water supplies. Knowledge of solids loading can aid in determining the type or amount of treatment, or both, necessary to make the water acceptable for use. Such information may also be used to determine acceptability of water after treatment. Too little treatment may not be desirable and excess treatment costs money.
Stream monitoring is important for environmental reasons. Stream improvements, water pollution monitoring, mass wasting, algal studies, and sediment loads are but a few of the many reasons streams are monitored.
SCOPE
1.1 This test method covers the determination of filterable and nonfilterable matter in drinking, surface, and saline waters, domestic and industrial wastes. The practical range of the determination of nonfilterable particulate matter is 4 to 20 000 mg/L. The practical range of the determination of filterable matter is 10 to 20 000 mg/L.
1.2 Since the results measured by this test are operationally defined, careful attention must be paid to following the procedure as specified.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see Section 9.

General Information

Status
Historical
Publication Date
09-Jun-2003
ICS
13.060.60 - Examination of physical properties of water
Technical Committee
D19 - Water
Drafting Committee
D19.05 - Inorganic Constituents in Water
Current Stage
Ref Project

Relations

Replaces
ASTM D5907-96a - Standard Test Method for Filterable and Nonfilterable Matter in Water
Effective Date
10-Jun-2003
Replaced By
ASTM D5907-09 - Standard Test Method for Filterable and Nonfilterable Matter in Water
Effective Date
01-May-2009
Referred By
ASTM E2060-22 - Standard Guide for Use of Coal Combustion Products for Solidification/Stabilization of Inorganic Wastes
Effective Date
10-Jun-2003
Referred By
ASTM D5975-17 - Standard Test Method for Determining the Stability of Compost by Measuring Oxygen Consumption
Effective Date
10-Jun-2003
Referred By
ASTM E2635-22 - Standard Practice for Water Conservation in Buildings Through In-Situ Water Reclamation
Effective Date
10-Jun-2003
Referred By
ASTM D8006-16 - Standard Guide for Sampling and Analysis of Residential and Commercial Water Supply Wells in Areas of Exploration and Production (E&P) Operations
Effective Date
10-Jun-2003

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ASTM D5907-03 - Standard Test Method for Filterable and Nonfilterable Matter in Water
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D 5907 – 03
Standard Test Method for
1
Filterable and Nonfilterable Matter in Water
This standard is issued under the fixed designation D5907; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope* E898 Methods of Testing Top-Loading, Direct-Reading
Laboratory Scales and Balances
1.1 This test method covers the determination of filterable
andnonfilterablematterindrinking,surface,andsalinewaters,
3. Terminology
domestic and industrial wastes. The practical range of the
3.1 Definitions: For definitions of other terms used in this
determination of nonfilterable particulate matter is 4 to 20000
test method, refer to Terminology D1129.
mg/L. The practical range of the determination of filterable
3.2 Definitions of Terms Specific to This Standard:
matter is 10 to 20000 mg/L.
3.2.1 filterable matter—also commonly referred to as total
1.2 Since the results measured by this test are operationally
dissolved solids. It is that dissolved matter that is capable of
defined, careful attention must be paid to following the
passingthroughaglassfiberfilteranddriedtoconstantweight
procedure as specified.
at 180°C, as determined by following the procedures outlined
1.3 This standard does not purport to address all of the
in this test method.
safety concerns, if any, associated with its use. It is the
3.2.2 nonfilterable matter—also commonly known as total
responsibility of the user of this standard to establish appro-
suspendedsolids.Itisthatparticulatematterthatisretainedon
priate safety and health practices and determine the applica-
a glass fiber filter and dried to a constant weight at 103 to
bility of regulatory limitations prior to use. For a specific
105°C, as determined by following the procedures outlined in
hazard statement, see Section 9.
this test method.
2. Referenced Documents
4. Summary of Test Method
2
2.1 ASTM Standards:
4.1 A well-mixed sample is filtered through a weighed
D596 Guide for Reporting Results of Analysis of Water
standard glass fiber filter.The suspended solids are retained on
D1129 Terminology Relating to Water
the filter, which is dried at 105°C and weighed. The increased
D1192 Guide for Equipment for Sampling Water and
mass on the filter represents the nonfilterable matter.
Steam in Closed Conduits
4.2 The filtrate from 4.1 may be used to determine the
D1193 Specification for Reagent Water
filterable matter. The filtered sample (liquid phase) is evapo-
D2777 Practice for Determination of Precision and Bias of
rated to dryness and heated to 180°C in a tared vessel to a
Applicable Methods of Committee D-19 on Water
constant weight.
D3370 PracticesforSamplingWaterfromClosedConduits
D3856 Guide for Good Laboratory Practices in Laborato-
5. Significance and Use
ries Engaged in Sampling and Analysis of Water
5.1 Solids, both as filterable and nonfilterable matter, are
D5847 Practice for the Writing Quality Control Specifica-
important in the treating of raw water and wastewater, and in
tions for Standard Test Methods for Water Analysis
monitoring of streams.
E319 PracticefortheEvaluationofSingle-PanMechanical
5.2 Waste solids impose a suspended and settleable residue
Balances
inreceivingwaters.Suspendedandsolublematerialsprovidea
matrix for some biological slime and, in sufficient quantity,
impair respiration of organisms. These solids may create
1
This test method is under the jurisdiction ofASTM Committee D19 on Water
nuisance slime beds and odors while imposing a long-term
and is the direct responsibility of Subcommittee D19.05 on Inorganic Constituents
biological oxidation load over limited receiving water areas.
in Water.
5.3 Knowledge of suspended and soluble materials is im-
Current edition approved June 10, 2003. Published July 2003. Originally
approved in 1996. Last previous edition approved in 1996 as D5907–96a.
portant in treating raw water supplies. Knowledge of solids
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
loadingcanaidindeterminingthetypeoramountoftreatment,
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
or both, necessary to make the water acceptable for use. Such
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. information may also be used to determine acceptability of
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D5907–03
water after treatment.Too little treatment may not be desirable 7. A
...

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5.1 Turbidity is monitored to help control processes, monitor the health and biology of aquatic environments and to determine the impact of environmental events such as storms, floods, runoff, etc. Turbidity is undesirable in drinking water, plant-effluent waters, water for food and beverage production, and for a large number of other water-dependent manufacturing processes. Turbidity is often reduced by coagulation, sedimentation and water filtration. The measurement of turbidity may indicate the presence of particle-bound contaminants and is vital for monitoring the completion of a particle-waste settling process. Significant uses of turbidity measurements include:  
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SCOPE
1.1 This test method covers the in-situ field measurements of turbidity in surface water. The measurement range is greater than 1 TU and the lesser of 10 000 TU or the maximum measurable TU value specified by the turbidimeter manufacturer.  
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4.1 These test methods are applicable for such purposes as impurity detection and, in some cases, the quantitative measurement of ionic constituents dissolved in waters. These include dissolved electrolytes in natural and treated waters, such as boiler water, boiler feedwater, cooling water, and saline and brackish water.  
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SCOPE
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Range  
Sections  
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12 to 18  
Measurement of Static (Non-Flowing) Samples  
μS/cm  
Test Method B—Continuous In-Line Measure  
5 to 200 000  
19 to 23  
ment  
μS/cm  
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This test method covers the apparatus and procedure for the electrometric measurement of oxidation-reduction potential (ORP) in water. The test method described has been designed for the routine and process measurement of oxidation-reduction potential. ORP is defined as the electromotive force between a noble metal electrode and a reference electrode when immersed in a solution. The ORP electrodes are inert and measure the ratio of the activities of the oxidized to the reduced species present. In addition, the ORP electrodes reliably measure ORP in nearly all aqueous solutions and in general are not subject to solution interference from color, turbidity, colloidal matter, and suspended matter. The apparatus to be used in the measurement of ORP includes: pH meter, reference electrode, oxidation-reduction electrode and electrode assembly. Materials necessary in the procedure for ORP measurement include chemical reagents, aqua regia, water, buffer standard salts, phthalate reference buffer solution, phosphate reference buffer solution, chromic acid cleaning solution, detergent, nitric acid, redox standard solution or ferrous-ferric reference solution, and redox reference quinhydrone solutions.
SCOPE
1.1 This test method covers the apparatus and procedure for the electrometric measurement of oxidation-reduction potential (ORP) in water. It does not deal with the manner in which the solutions are prepared, the theoretical interpretation of the oxidation-reduction potential, or the establishment of a standard oxidation-reduction potential for any given system. The test method described has been designed for the routine and process measurement of oxidation-reduction potential.  
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SCOPE
1.1 These practices provide directions for the preparation of the sample for analysis, the preliminary examination of the sample, and methods for dissolving the analytical sample or selectively separating constituents of concern.  
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Sections  
Preparation of the Analytical Sample  
8  
Preliminary Testing of the Analytical Sample  
9  
Dissolving the Analytical Sample  
10  
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5.1 Fe-55 is formed in reactor coolant systems of nuclear reactors by activation of stable iron. The 55Fe is not completely removed by waste processing systems and some is released to the environment by means of normal waste liquid discharges. Power plants are required to monitor these discharges for 55Fe as well as other radionuclides.  
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SCOPE
1.1 This test method covers the determination of 55Fe in the presence of 59Fe by liquid scintillation counting. The a-priori minimum detectable concentration for this test method is 7.4 Bq/L.2  
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1.3 This test method was used successfully with Type III reagent water conforming to Specification D1193. It is the responsibility of the user to ensure the validity of this test method for waters of untested matrices.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific hazard statement, see Section 9.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Test Method for 99Tc in Water by Solid Phase Extraction Disk

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5.1 This test method has not been evaluated for all possible matrices. Test method suitability should be determined on specific waters of interest.
SCOPE
1.1 This test method describes a solid phase extraction (SPE) procedure to separate 99Tc from environmental water (non-process-related or effluent water samples). Technetium-99 beta activity is measured by liquid scintillation spectrometry.  
1.2 This test method is designed to measure 99Tc in the range of approximately 0.037 Bq/L (1.0 pCi/L) or greater for a one litre sample.  
1.3 This test method has been used successfully with tap water. It is the user’s responsibility to ensure the validity of this test method for samples larger than 1 L and for waters of untested matrices.  
1.4 Technetium-99 alternatively can be determined in water samples using Practice D8026.  
1.5 The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard.  
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1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This test method was developed for the purpose of measuring gross alpha radioactivity in water. It is used for the analysis of both process and environmental water to determine gross alpha activity which is often a result of natural radioactivity present in minerals.
SCOPE
1.1 This test method covers the measurement of alpha particle activity of water. It is applicable to nuclides that emit alpha particles with energies above 3.9 MeV and at activity levels above 0.02 Bq/mL (540 pCi/L) of radioactive homogeneous water. This test method is not applicable to samples containing alpha-emitting radionuclides that are volatile under conditions of the analysis.  
1.2 This test method can be used for either absolute or relative determinations. In tracer work, the results may be expressed by comparison with a standard that is defined to be 100 %. For radioassay, data may be expressed in terms of alpha disintegration rates after calibration with a suitable standard. General information on radioactivity and measurement of radiation has been published in Refs (1-3)2 and summarized in Practices D3648.  
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1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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SIGNIFICANCE AND USE
5.1 This test method was developed to measure the concentration of 90Sr in non-process water samples. This test method may be used to determine the concentration of 90Sr in environmental samples.
SCOPE
1.1 This test method covers the determination of radioactive 90Sr in environmental water samples (for example, non-process and effluent waters) in the range of 0.037 Bq/L (1.0 pCi/L) or greater.  
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1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 9.  
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