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ASTM

ASTM D564-87(2002)

(Test Method)

Standard Test Methods for Liquid Paint Driers

Standard Test Methods for Liquid Paint Driers

SIGNIFICANCE AND USE
Driers accelerate the drying of oil, paint, printing ink, and varnish.
These test methods are applicable to liquid driers manufactured for use in paints and related coatings.
The tests for metallic content using ethylenediaminetetraacetic acid dihydrate (EDTA) are intended for concentrated solutions of single metals; two or more metals may cause interference.
SCOPE
1.1 These test methods cover the test procedures to be applied to liquid paint driers used in paints and related coatings. Typical paint driers, listed in Specification D600, are carboxylates of lead, cobalt, manganese, zinc, iron, calcium, and zirconium.  
1.2This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
26-Nov-1987
ICS
87.060.99 - Other paint ingredients
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.21 - Chemical Analysis of Paints and Paint Materials
Current Stage
Ref Project

Relations

Replaces
ASTM D564-87(1996) - Standard Test Methods for Liquid Paint Driers
Effective Date
27-Nov-1987
Replaced By
ASTM D564-87(2008) - Standard Test Methods for Liquid Paint Driers
Effective Date
01-Feb-2008

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ASTM D564-87(2002) - Standard Test Methods for Liquid Paint DriersASTM D564-87(2002) - Standard Test Methods for Liquid Paint Driers
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ASTM D564-87(2002) - Standard Test Methods for Liquid Paint Driers
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D564–87 (Reapproved 2002)
Standard Test Methods for
Liquid Paint Driers
This standard is issued under the fixed designation D564; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope D3804 Test Method for Iron in Paint Driers by EDTA
Method
1.1 These test methods cover the test procedures to be
D3924 Specification for Standard Environment for Condi-
applied to liquid paint driers used in paints and related
tioning and Testing Paint, Varnish, Lacquer, and Related
coatings.Typicalpaintdriers,listedinSpecificationD600,are
Materials
carboxylates of lead, cobalt, manganese, zinc, iron, calcium,
D3969 Test Method for Zirconium in Paint Driers by
and zirconium.
EDTA Method
1.2 This standard does not purport to address all of the
D3970 Test Method for Cerium in Paint Driers by Oxidi-
safety concerns, if any, associated with its use. It is the
metric Determination
responsibility of the user of this standard to establish appro-
D3980 Practice for Interlaboratory Testing of Paint and
priate safety and health practices and determine the applica-
Related Materials
bility of regulatory limitations prior to use.
D3988 TestMethodforVanadiuminPaintDriersbyEDTA
2. Referenced Documents
Method
D3989 Test Method for Total Rare Earth Metals in Paint
2.1 ASTM Standards:
Driers by EDTA Method
D234 Specification for Raw Linseed Oil
D235 Specification for Mineral Spirits (Petroleum Spirits)
3. Significance and Use
(Hydrocarbon Dry Cleaning Solvent)
3.1 Driers accelerate the drying of oil, paint, printing ink,
D600 Specification for Liquid Paint Driers
and varnish.
D1544 Test Method for Color of Transparent Liquids
3.2 These test methods are applicable to liquid driers
(Gardner Color Scale)
manufactured for use in paints and related coatings.
D1640 Test Methods for Drying, Curing, or Film Forma-
4 3.3 The tests for metallic content using ethylenediaminetet-
tion of Organic Coatings at Room Temperature
raacetic acid dihydrate (EDTA) are intended for concentrated
D1644 TestMethodsforNonvolatileContentofVarnishes
solutions of single metals; two or more metals may cause
D2090 Test Method for Clarity and Cleanness of Paint and
interference.
Ink Liquids
D2373 Test Method for Determination of Cobalt in Paint
4. Physical Tests
Driers by EDTA Method
4.1 Sampling—SampleinaccordancewithPracticeD3980.
D2374 Test Method for Lead in Paint Driers by EDTA
4 4.2 Conditioning—Follow Specification D 3924 except
Method
where other temperatures are specified.
D2375 Test Method for Manganese in Paint Driers by
4 4.3 Appearance—After conditioning overnight at room
EDTA Method
temperature (see Specification D3924) examine the drier
D2613 Test Method for Calcium or Zinc in Paint Driers by
4 without aid of magnification for clarity and cleanness and for
EDTA Method
presence of foreign matter, sediment, skins, turbidity or hazi-
ness, in accordance with Test Method D2090.
These test methods are under the jurisdiction of ASTM Committee D01 on 4.4 Sediment or Suspended Matter—If sediment or sus-
Paint and Related Coatings, Materials, and Applications and are the direct
pended matter is observed, proceed as follows:
responsibility of Subcommittee D01.21 on Chemical Analysis of Paints and Paint
4.4.1 Weigh to 1 mg, by difference, 1 to5gof drier into a
Materials.
tared 10 to 15-µm fritted-glass crucible.After most of the drier
Current edition approved Nov. 27, 1987. Published January 1988. Originally
published as D564–40. Last previous edition D564–81.
has passed through wash with mineral spirits conforming to
Annual Book of ASTM Standards, Vol 06.03.
Specification D235 and dry at 50°C until the weight is
Annual Book of ASTM Standards, Vol 06.04.
Annual Book of ASTM Standards, Vol 06.01.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D564
constant to 1 mg. Calculate the difference in weight and report previously evaluated standard of known drying power for
as percent sediment in the drier. comparative purposes.
4.5 Color—Determine color in accordance with Test
NOTE 4—The drying powers or efficiencies of individual metal driers
Method D1544.
may be a function of: (1) the class of carboxylic acids, for example,
octoate versus naphthenate, etc., (2) additives in drier solutions, for
NOTE 1—This scale is useful for yellow and brown organic chro-
example, stabilizers, etc., (3) chemical
...

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SIGNIFICANCE AND USE
3.1 Driers accelerate the drying of oil, paint, printing ink, and varnish.  
3.2 These test methods are applicable to liquid driers manufactured for use in paints and related coatings.  
3.3 The tests for metallic content using ethylenediaminetetraacetic acid dihydrate (EDTA) are intended for concentrated solutions of single metals; two or more metals may cause interference.
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SIGNIFICANCE AND USE
4.1 This test method may be used to confirm in the presence of rare earths the stated cerium content of liquid pure cerium or rare earth driers manufactured for use in the coatings industry.
SCOPE
1.1 This test method covers the titrimetric determination of cerium in liquid cerium and rare earth paint driers and utilizes ferrous ammonium sulfate.  
1.2 This test method is not applicable to dryer blends.  
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ASTM D3988-05(2023)(Test Method)
Standard Test Method for Vanadium in Paint Driers by EDTA Method

SIGNIFICANCE AND USE
4.1 This test method may be used to confirm the stated content of a pure liquid vanadium drier manufactured for use by the coatings industry.
SCOPE
1.1 This test method covers the titrimetric determination of vanadium in liquid vanadium driers and utilizes the disodium salt of ethylenediaminetetraacetic acid dihydrate (EDTA).  
1.2 This test method is limited to the determination of the vanadium content of a liquid vanadium drier that does not contain other drier elements. This test method is not applicable to drier blends.  
1.3 All cations that can be titrated with EDTA in alkaline media interfere and must not be present in the sample.  
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1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Test Method for Calcium or Zinc in Paint Driers by EDTA Method

SIGNIFICANCE AND USE
4.1 This test method may be used to confirm the stated calcium or zinc content of pure liquid calcium or zinc driers soluble in toluene-alcohol and manufactured for use by the coatings industry.
SCOPE
1.1 This test method covers a titrimetric determination of calcium in liquid calcium driers and zinc in liquid zinc driers that can be dissolved in a toluene-alcohol mixture and utilizes the disodium salt of ethylenediaminetetraacetic acid dihydrate (EDTA).  
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4.1 This test method may be used to confirm the stated content of a liquid iron drier soluble in isopropyl alcohol and manufactured for use in the coatings industry. The content determines activity level.
SCOPE
1.1 This test method covers the titrimetric determination of iron in liquid iron driers soluble in isopropyl alcohol and utilizes the disodium salt of ethylenediaminetetraacetic acid dihydrate (EDTA).  
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This specification covers the materials commercially known as gold bronze, pale gold bronze, and rich gold bronze powders. The gold bronze powder shall be made from new ingot metals, shall consist of fine polished flakes containing the prescribed percentage of fatty or oily matter (polishing lubricant), shall have the specified residue content and leafing properties, and shall be suitable for making gold bronze paint. The sampling and test methods to determine conformance to the specified composition and properties are given.
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Standard Specification for Metallic Copper Powder for Use in Antifouling Paints

ABSTRACT
This specification covers metallic copper powder for use in antifouling paints. The pigment shall consist essentially of finely divided copper metal. The copper, and coarse particle shall be tested to meet the requirements prescribed.
SCOPE
1.1 This specification covers copper powder for use in antifouling paints.  
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ASTM D3969-01(2019)e1(Test Method)
Standard Test Method for Zirconium in Paint Driers by EDTA Method

SIGNIFICANCE AND USE
4.1 The amount of zirconium drier used in oxidizing-type coatings significantly affects their drying properties. This test method may be used to confirm the stated content of a pure liquid zirconium drier manufactured for use by the coatings industry.
SCOPE
1.1 This test method covers the titrimetric determination of zirconium in zirconium driers used in the coatings industry and utilizes the disodium salt of ethylenediaminetetraacetic acid dihydrate (EDTA).  
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ASTM D3989-01(2019)e1(Test Method)
Standard Test Method for Total Rare Earth Metals in Paint Driers by EDTA Method

SIGNIFICANCE AND USE
4.1 This test method may be used to confirm the stated content of a pure, liquid rare earth metal drier manufactured for use in the coatings industry.
SCOPE
1.1 This test method covers the titrimetric determination of rare earth metals in liquid rare earth metal driers and utilizes the disodium salt of ethylenediaminetetraacetic acid dihydrate (EDTA).  
1.2 This test method is limited to the determination of the rare earth metal content of a liquid rare earth metal drier that does not contain other drier elements. The method is not applicable to drier blends.  
1.3 This test method has been tested in concentrations of 6 % cerium and 6 % rare earth metals, but there is no reason to believe that it is not suitable for higher or lower drier metal concentrations provided specimen size is adjusted accordingly.  
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ASTM D4140-07(2018)(Guide)
Standard Guide for Determining Volatile and Nonvolatile Content of Driers, Drying Oils, Naval Stores, and Solvents

SIGNIFICANCE AND USE
4.1 The nonvolatile content of raw materials may be used to determine the total nonvolatile content (solids) of paint and related coatings. Such information may be useful to coatings producers and users for the determination of the total solids available for film formation and for the estimation of the volatile organic content.
SCOPE
1.1 This guide is intended to aid in the selection of the proper ASTM test method for determining the volatile and nonvolatile content of driers, drying oils, naval stores, and solvents.  
Note 1: Test methods for determining the composition of the volatile fraction are not covered by this guide.  
1.2 The test methods included are as follows:    
Standard  
Section  
ASTM Designation  
Driers  
5.1  
D1644  
Drying oils  
5.2  
D555
D1960  
Naval stores  
5.3  
D233
D889
D1131  
Solvents  
5.4  
D1353  
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