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ASTM D6203-06(2012)

(Test Method)

Standard Test Method for Thermal Stability of Way Lubricants

Standard Test Method for Thermal Stability of Way Lubricants

SIGNIFICANCE AND USE
Thermal stability characterizes physical and chemical property changes which may adversely affect an oil's lubricating performance. This test method evaluates the thermal stability of a way lubricant in the presence of copper and steel rods at 100°C. Deposits and rod colors are the evaluation criteria. No correlation of the test to field service has been made.
This test method is intended for use in qualifying a way lubricant, rather than for quality control or condition monitoring purposes.
SCOPE
1.1 This test method covers the evaluation of the thermal stability of hydrocarbon–based way lubricants, although oxidation may occur during the test.
1.2 The values stated in SI units are to be regarded as standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
14-Apr-2012
ICS
75.100 - Lubricants, industrial oils and related products
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.L0.01 - Metal Removal Fluids and Lubricants
Current Stage
Ref Project

Relations

Replaces
ASTM D6203-06 - Standard Test Method for Thermal Stability of Way Lubricants
Effective Date
15-Apr-2012

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ASTM D6203-06(2012) - Standard Test Method for Thermal Stability of Way LubricantsASTM D6203-06(2012) - Standard Test Method for Thermal Stability of Way Lubricants
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ASTM D6203-06(2012) - Standard Test Method for Thermal Stability of Way Lubricants
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D6203 − 06 (Reapproved 2012)
Standard Test Method for
Thermal Stability of Way Lubricants
This standard is issued under the fixed designation D6203; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope ing performance. This test method evaluates the thermal
stability of a way lubricant in the presence of copper and steel
1.1 This test method covers the evaluation of the thermal
rods at 100°C. Deposits and rod colors are the evaluation
stability of hydrocarbon–based way lubricants, although oxi-
criteria. No correlation of the test to field service has been
dation may occur during the test.
made.
1.2 The values stated in SI units are to be regarded as
4.2 This test method is intended for use in qualifying a way
standard. The values given in parentheses are for information
lubricant, rather than for quality control or condition monitor-
only.
ing purposes.
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
5. Apparatus
responsibility of the user of this standard to establish appro-
5.1 Gravity Convection Electric Oven, capable of maintain-
priate safety and health practices and determine the applica-
ing the samples at a test temperature of 100 6 2°C.
bility of regulatory limitations prior to use.
5.2 Calibrated Temperature Indicator, suitable for measur-
2. Referenced Documents
ing and controlling the oven temperature.
2.1 ASTM Standards:
5.3 Griffın Beakers, borosilicate glass, 100 mL.
D4057 Practice for Manual Sampling of Petroleum and
5.4 Copper Test Specimens, in accordance with UNS
Petroleum Products
C11000, 99.9 % pure electrolytic tough pitch copper, 6.4 mm
2.2 Other Standards:
in diameter by 7.6 cm in length (0.25 by 3.0 in.).
UNS C11000 Electrolytic Tough Pitch Copper
5.5 Steel Test Specimens, in accordance with AISI W1 1 %
AISI W1 1% Carbon Tool Steel
carbon steel, 6.4 mm in diameter by 7.6 cm in length (0.25 by
3. Summary of Test Method
3.0 in.).
3.1 Abeaker containing test oil and copper and steel rods is
5.6 Silicon Carbide Abrasive, 320 grit with cloth backing.
placed in a gravity convection electric oven for 24 h at a test
5.7 Crocus Cloth.
temperature of 100°C.At the completion of the test, the copper
5.8 Cincinnati Milacron Color Chart.
and steel rods are visually rated for discoloration and the
beaker is visually evaluated for deposits.
5.9 Facial Tissue.
4. Significance and Use
6. Reagents
4.1 Thermal stability characterizes physical and chemical
6.1 Reagent GradeAcetone.(Warning—Flammable,health
property changes which may adversely affect an oil’s lubricat-
hazard.)
6.2 Reagent Grade Heptane. (Warning—Flammable,
This test method is under the jurisdiction of ASTM Committee D02 on
health hazard.)
Petroleum Products and Lubricants and is the direct responsibility of Subcommittee
D02.L0.01 on Metal Removal Fluids and Lubricants.
7. Preparation of Metal Rods
Current edition approved April 15, 2012. Published May 2012. Originally
approved in 1997. Last previous edition approved in 2006 as D6203–06. DOI:
7.1 Handle the rods at all times using forceps, facial tissue,
10.1520/D6203-06R12.
2 or suitable gloves.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
7.2 Clean the iron and copper catalyst rods, whether new or
Standards volume information, refer to the standard’s Document Summary page on
previously used, prior to use. Clean the rods with the 320 grit
the ASTM website.
Available from Copper Development Assoc., 2 Greenwich Office Park, Box silicon carbide abrasive cloth while rotating the rods in a drill
1840, Greenwich, CT 06836.
Available from American Iron and Steel Institute (AISI), 1140 Connecticut
Ave., NW, Suite 705, Washington, DC 20036, http://www.steel.org. Available from Milacron Inc., 2090 Florence Ave., Cincinnati, OH 45206.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
...

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