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ASTM D5439-95(2006)

(Test Method)

Standard Test Method for Determination of Sediment in Moellon

Standard Test Method for Determination of Sediment in Moellon

SIGNIFICANCE AND USE
This test method is intended for use in determining the toluene insoluble sediment contained in Moellon.
SCOPE
1.1 This test method covers the determination of the toluene insoluble sediment contained in Moellon. This test method was derived from Test Method D473.  
1.2 The values stated in SI units are to be regarded as the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Mar-2006
ICS
93.020 - Earthworks. Excavations. Foundation construction. Underground works
Technical Committee
D31 - Leather
Drafting Committee
D31.08 - Fats and Oils
Current Stage
Ref Project

Relations

Replaces
ASTM D5439-95(2001) - Standard Test Method for Determination of Sediment in Moellon
Effective Date
01-Apr-2006
Replaced By
ASTM D5439-95(2012) - Standard Test Method for Determination of Sediment in Moellon
Effective Date
01-Apr-2012

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ASTM D5439-95(2006) - Standard Test Method for Determination of Sediment in MoellonASTM D5439-95(2006) - Standard Test Method for Determination of Sediment in Moellon
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ASTM D5439-95(2006) - Standard Test Method for Determination of Sediment in Moellon
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D5439–95 (Reapproved 2006)
Standard Test Method for
1
Determination of Sediment in Moellon
This standard is issued under the fixed designation D5439; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers the determination of the toluene
insolublesedimentcontainedinMoellon.Thistestmethodwas
derived from Test Method D473.
1.2 The values stated in SI units are to be regarded as the
standard.
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
NOTE 1—Apparatus B shows the water cup in position.
2. Referenced Documents
FIG. 1 Extraction Apparatus for Determination of Sediment
2
2.1 ASTM Standards:
D473 TestMethodforSedimentinCrudeOilsandFuelOils
4.1.2 Condenser, a condenser in the form of a metal coil
by the Extraction Method
approximately 25 mm in diameter and 50 mm in length
D4057 Practice for Manual Sampling of Petroleum and
attached to, and with the ends projecting through a lid of
Petroleum Products
sufficient diameter to cover the neck of the flask as shown in
D4177 Practice for Automatic Sampling of Petroleum and
Fig. 1. The coil should be made from stainless steel, tin,
Petroleum Products
3
tin-plated copper, or tin-plated brass tubing having an outside
2.2 ISO Standard:
diameter of 5 to 8 mm and a wall thickness of 1.5 mm. If
ISO 5272 Toluene for Industrial Use - Specifications
constructed of tin-plated copper or brass, the tin coating shall
3. Significance and Use have a minimum thickness of 0.075 mm. The exposed surface
2
of the coil for cooling purposes is about 115 cm .
3.1 This test method is intended for use in determining the
4.1.3 Extraction Thimble—The extraction thimble should
toluene insoluble sediment contained in Moellon.
be of a refractory porous material, pore size index P15, 25 mm
4. Apparatus
in diameter by 70 mm in height, weighing not less than 15 g
and not more than 17 g. The thimble shall be suspended from
4.1 ExtractionApparatus (see Fig. 1 and Fig. 2), consisting
the condenser coil by means of a basket so that it hangs
of the parts described in 4.1.1-4.1.6.
approximately midway between the surface of the extracting
4.1.1 ExtractionFlask,awide-neckErlenmeyerflaskof1-L
solvent and the bottom of the condenser coil.
capacity.
4.1.4 Thimble Basket—The thimble basket shall be
corrosion-resistant, shall be made of platinum, stainless steel,
nickel-chromium alloy, or similar material, and shall meet the
1
This test method is under the jurisdiction ofASTM Committee D31 on Leather
requirements of Fig. 2.
and is the direct responsibility of Subcommittee D31.08 on Fats and Oils. This test
4.1.5 Water Cup—Awater cup shall be used when testing a
method was developed in cooperation with the American Leather Chemists Assn.
(Method H 23–1957).
samplehavingahigh-watercontent(seeFig.1b).Thecupshall
Current edition approved April 1, 2006. Published April 2006. Originally
be made of glass, shall be conical in shape, shall be approxi-
approved in 1993. Last previous edition approved in 2001 as D5439 – 95(2001).
mately 20 mm in diameter and 25 mm deep, and shall have a
DOI: 10.1520/D5439-95R06.
2
capacity of approximately 3 mL.Aglass hook fused on the rim
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
at one side is so shaped that when hung on the condenser the
Standards volume information, refer to the standard’s Document Summary page on
cup hangs with its rim reasonably level. In this procedure, the
the ASTM website.
3
thimble basket is suspended either as shown in Fig. 1aby
Available from American National Standards Institute, 11 West 42nd St., 13th
Floor, New York, NY 10036. meansofthecorrosion-resistantwireloopedoverthebottomof
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D5439–95 (2006)
NOTE 1—Silver solder should be used on all joints.
FIG. 2 Basket Thimble Support
the condenser coil and attached to the basket supports or as in
_______________
A
Fig. 1b where the wire supports of the basket are attached to
Recorded boiling point 110.6°C.
hooks soldered to the underside of the condenser lid.
6. Sampling
4.1.6 SourceofHeat,asourceofheat,preferablyahotplate,
suitable for vaporizing toluene.
...

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3.1 This test method is intended for use in determining the toluene insoluble sediment contained in Moellon.
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4.1 These test methods are used to determine the resistance of compacted soil-cement specimens to repeated wetting and drying. These test methods were developed to be used in conjunction with Test Methods D560/D560M and criteria given in the Soil-Cement Laboratory Handbook4 to determine the minimum amount of cement required in soil-cement to achieve a degree of hardness adequate to resist field weathering.
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Sections  
Test Method A, using soil material passing a 4.75-mm [No. 4] sieve.
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7  
Test Method B, using soil material passing a 19.0 mm [0.75-in.] sieve.
This method shall be used when part of the soil sample is retained on the 4.75-mm [No. 4] sieve.
This test method may be used only on materials with 30 % or less retained on the 19.0-mm [0.75-in.] sieve.  
8  
1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this test method.  
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SIGNIFICANCE AND USE
5.1 By definition, the tensile strength is obtained by the direct tensile test. However, the direct tensile test is difficult and expensive for routine application. The splitting tensile test appears to offer a desirable alternative because it is much simpler and inexpensive. Furthermore, engineers involved in rock mechanics design usually deal with complex stress fields, including various combinations of compressive and tensile stress fields. Under such conditions, the tensile strength should be obtained with the presence of compressive stresses to be representative of the field conditions.  
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SIGNIFICANCE AND USE
5.1 Where sulfates are suspected, subgrade soils should be tested as an integral part of a geotechnical evaluation because the possibility that sulfate induced heave may occur if calcium containing stabilizers are used to improve the soils and sulfate reactions may also cause deterioration in concrete structures. When planning to treat a soil used in construction with lime, testing the soil for water soluble sulfates prior to treatment becomes very important (Note 2).  
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SCOPE
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SIGNIFICANCE AND USE
5.1 In this test method, the compressive strength of a soil is determined in terms of the total stress, therefore, the resulting strength depends on the pressure developed in the pore fluid during loading. In this test method, fluid flow is not permitted from or into the soil specimen as the load is applied, therefore the resulting pore pressure, and hence strength, differs from that developed in the case where drainage can occur.  
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5.3 If the test specimens are partially saturated, or compacted/reconstituted specimens, where the degree of saturation is less than 100 %, consolidation may occur when the confining pressure is applied and during application of axial load, even though drainage is not permitted. Therefore, if several partially saturated specimens of the same material are tested at different confining stresses, they will not have the same unconsolidated-undrained shear strength.  
5.4 Mohr failure envelopes may be plotted from a series of unconsolidated undrained triaxial tests. The Mohr’s circles at failure based on total stresses are constructed by plotting a half circle with a radius of half the principal stress difference (deviator stress) beginning at the axial stress (major principal stress) and ending at the confining stress (minor principal stress) on a graph with principal stresses as the abscissa and shear stress as the ordinate and equal scale in both directions. The failure envelopes will usually be a horizontal line for saturated specimens and a curved line for partially saturated specimens.  
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SCOPE
1.1 This test method covers determination of the strength and stress-strain relationships of a cylindrical specimen of either intact, compacted, or remolded cohesive soil. Specimens are subjected to a confining fluid pressure in a triaxial chamber. No drainage of the specimen is permitted during the application of the confining fluid pressure or during the compression phase of the test. The specimen is axially loaded at a constant rate of axial deformation (strain controlled).  
1.2 This test method provides data for determining undrained strength properties and stress-strain relations for soils. This test method provides for the measurement of the total stresses applied to the specimen, that is, the stresses are not corrected for pore-water pressure.
Note 1: The determination of the unconfined compressive strength of cohesive soils is covered by Test Method D2166/D2166M.
Note 2: The determination of the consolidated, undrained strength of cohesive soils with pore pressure measurement is covered by Test Method D4767.  
1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
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Standard Practice for X-Ray Radiography of Soil Samples

SIGNIFICANCE AND USE
5.1 Many geotechnical tests require the utilization of intact, representative samples of soil. The quality of these samples depends on many factors. Many of the samples obtained by intact sampling methods have inherent anomalies. Sampling procedures cause disturbances of varying types and intensities. These anomalies and disturbances, however, are not always readily detectable by visual inspection of the intact samples before or after testing. Often test results would be enhanced if the presence and the extent of these anomalies and disturbances are known before testing or before destruction of the sample by testing. Such determinations assist the user in detecting flaws in sampling methods, the presence of natural or induced shear planes, and the presence of natural intrusions, such as gravels or shells at critical regions in the samples, the presence of sand and silt seams, and the intensity of disturbances caused by sampling.  
5.2 X-ray radiography provides the user with a picture of the internal massive structure of the soil sample, regardless of whether the soil is X-rayed within or without the sampling tube. X-ray radiography assists the user in identifying the following:  
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SCOPE
1.1 This practice covers the determination of the quality of soil samples in thin wall tubes or of extruded soil cores by X-ray radiography.  
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1.3 This practice can be used to X-ray soil cores (or observe their features on a fluoroscope) in thin wall tubes or liners ranging from approximately 50 to 150 mm [2 to 6 in.] in diameter. X-rays of samples in the larger diameter tubes provide a radiograph of major features of soils and disturbances, such as large scale bending of edges of varved clays, shear planes, the presence of large concretions, silt and sand seams thicker than 6 mm [1/4 in.], large lumps of organic matter, and voids or other types of intrusions. X-rays of the smaller diameter cores provide higher resolution of soil features and disturbances, such as small concretions (3 mm [1/8 in.] diameter or larger), solution channels, slight bending of edges of varved clays, thin silt or sand seams, narrow solution channels, plant root structures, and organic matter. The X-raying of samples in thin wall tubes or liners requires minimal preparation.  
1.4 Greater detail and resolution of various features of the soil can be obtained by X-raying extruded soil cores, as compared to samples in metal tubes. The method used for X-raying soil cores is the same as that for tubes and liners, except that extruded cores have to be handled with extreme care and have to be placed in sample troughs (similar to Fig. 2) before X-raying. This practice should be used only when natural water content or other intact soil characteristics are irrelevant to the end use of the sample.  
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SIGNIFICANCE AND USE
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Note 2: The agency performing this test method can be evaluated in accordance with Practice D3740. Notwithstanding statements on precision and bias contained in this method: The precision of this test method is dependent on the competence of the personnel performing it and the suitability of the equipment and facility used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing. Users of this test method are cautioned that compliance with Practice D3740 does not, in itself, ensure reliable testing. Reliable testing depends on many factors; Practice D3740 provides a means of evaluating some of these factors.
SCOPE
1.1 This test method covers procedures for preparing, curing, and testing laboratory-compacted specimens of soil-lime and other lime-treated materials (Note 1) for determining unconfined compressive strength. Depending on the diameter to height ratio, two procedures for determining the unconfined compressive strength of compacted soil-lime mixtures have been developed for specimens prepared at the maximum unit weight and optimum water content, or for specimens prepared at other target unit weight and water content levels. Other applications are given in Section 5 on Significance and Use.
Note 1: Lime-based products other than commercial quicklime and hydrated lime are also used in the lime treatment of fine-grained cohesive soils. Lime kiln dust (LKD) is collected from the kiln exhaust gases by cyclone, electrostatic, or baghouse-type collection systems. Some lime producers hydrate various blends of LKD plus quicklime to produce a lime-based product.  
1.2 Cored specimens of soil-lime should be tested in accordance with Test Methods D2166/D2166M.  
1.3 Two alternative procedures are provided:  
1.3.1 Procedure A describes procedures for preparing and testing compacted soil-lime specimens having height-to-diameter ratios between 2.00 and 2.50. This test method provides the standard measure of compressive strength.  
1.3.2 Procedure B describes procedures for preparing and testing compacted soil-lime specimens using Test Methods D698 compaction equipment and molds commonly available in most soil testing laboratories. Procedure B is considered to provide relative measures of individual specimens in a suite of test specimens rather than standard compressive strength values. Because of the lesser height-to-diameter ratio (1.15) of the cylinders, compressive strength determined by Procedure B will normally be greater than that by Procedure A.  
1.3.3 Results of unconfined compressive strength tests using Procedure B should not be directly compared to those obtained using Procedure A.  
1.4 All observed and calculated values shall conform to the guideline...

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ASTM
ASTM D4219-22(Test Method)
Standard Test Method for Short-Term Unconfined Compressive Strength Index of Chemically Grouted Soils

SIGNIFICANCE AND USE
5.1 The purpose of this test method is to obtain values for comparison with other test values to verify uniformity of materials or the effects of controllable variables, in grout-soil compositions.  
5.2 This test method is similar, in principle, to Test Method D2166/D2166M, but is not intended for determination of strength parameters to be used in design. Such values are more properly obtained from long-term triaxial tests.
Note 1: The quality of the result produced by this standard is dependent on the competence of the personnel performing it, and the suitability of the equipment and facilities used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing/sampling/inspection/etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself assure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 This test method covers the determination of the short-term unconfined compressive strength index of chemically grouted soils, using displacement-controlled application of test load.  
1.2 Units—The values stated in SI units are to be regarded as standard. The values given in parentheses are provided for information only and are not considered standard. Reporting of test results in units other than SI shall not be regarded as nonconformance with this standard.  
1.2.1 It is common practice in the engineering/construction profession to concurrently use pounds to represent both a unit of mass (lbm) and of force (lbf). This practice implicitly combines two separate systems of units; the absolute and the gravitational systems. It is scientifically undesirable to combine the use of two separate sets of inch-pound units within a single standard. As stated, this standard includes the gravitational system of inch-pound units and does not use/present the slug unit of mass. However, the use of balances and scales recording pounds of mass (lbm) or recording density in lbm/ft3 shall not be regarded as nonconformance with this standard.  
1.3 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026, unless superseded by this test method.  
1.3.1 For purposes of comparing a measured or calculated value(s) with specified limits, the measured or calculated value(s) shall be rounded to the nearest decimal of significant digits in the specified limit.  
1.3.2 The procedures used to specify how data are collected/recorded or calculated in the standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose for obtaining the data, special purpose studies, or any considerations for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D4381/D4381M-22(Test Method)
Standard Test Method for Sand Content by Volume of Construction Slurries

SIGNIFICANCE AND USE
5.1 This test method is used to determine the percentage of sand by volume in construction slurry. The significance of this test method mainly relates to construction slurries used for concrete wall and drilled piers construction. The range of measurement is too limited for use in applications where the sand content is intended to be greater than 20 %, such as in the cases of cement bentonite or soil bentonite walls.  
5.2 A high sand content in the construction slurry is abrasive for construction plant such as pumps, and is furthermore adverse to the formation of a filter cake in applications where bentonite fluid is used to stabilize an excavation.
Note 1: The quality of the result produced by this standard depends on the competence of the personnel performing it and the suitability of the equipment and facilities being used. Agencies that meet the criteria of Practice D3740 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Practice D3740 does not in itself ensure reliable results. Reliable results depend on many factors; Practice D3740 provides a means of evaluating some of those factors.
SCOPE
1.1 This test method covers the determination of the sand content of bentonitic slurries used in slurry construction techniques. This test method has been modified from API Recommended Practice 13B.  
1.2 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
1.3 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. Except, the sieve designation is identified using the “alternative” system in accordance with Practice E11 instead of the “standard system,” such that the sieve used is referred to as a No. 200 sieve, instead of a 75 µm sieve.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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